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At least 19 recordsLinked to original sources

The shear strength of trabecular bone from the femur, and some factors affecting the shear strength of the cement-bone interface.

The shear strength of trabecular bone from the femur has been studied. In general, the strongest trabecular bone is found close to the cortico-cancellous junction, though its shear strength depends also on the relationship of the trabeculae to the plane of shear. Some factors affecting the shear strength of the cement-bone interface have been investigated. In vitro, maximal cement-bone interface shear strength is obtained by exposing and thoroughly cleaning strong trabecular bone, and then forcing onto it under pressure low viscosity cement.

Adhesiveness↗

Vane shear strength of dewatered sludge from Hong Kong.

The vane shear strength and total solids content of dewatered sludge from Hong Kong were determined in order to evaluate their geotechnical suitability for disposal in landfills. The results obtained indicate that (i) the total solids and vane shear strength of dewatered sludge from different treatment plants varied considerably depending on the type of sludge and dewatering method; and, (ii) percent total solids alone is not sufficient to guarantee geotechnical stability in terms of vane shear strength. The critical state model for soils provided a good fit for the characteristic relationship between vane shear strength and total solids, which can be used to estimate vane shear strength from total solids only. No relationship between volatile solids and vane shear strength was found. The results of the laboratory vane shear test correlated well with those obtained by a pocket shearmeter indicating the usefulness of this method for rapid determination of vane shear strength on site. Some factors that influence vane shear strength were briefly evaluated. Implications of the results for sludge management with special emphasis on dewatering and landfilling were discussed.

Chemical Phenomena↗

Shear strength properties of wet granular materials.

We investigate shear strength properties of wet granular materials in the pendular state (i.e., the state where the liquid phase is discontinuous) as a function of water content. Sand and glass beads were wetted and tested in a direct shear cell and under various confining pressures. In parallel, we carried out three-dimensional molecular dynamics simulations by using an explicit equation expressing capillary force as a function of interparticle distance, water bridge volume, and surface tension. We show that, due to the peculiar features of capillary interactions, the major influence of water content over the shear strength stems from the distribution of liquid bonds. This property results in shear strength saturation as a function of water content. We arrive at the same conclusion by a microscopic analysis of the shear strength. We propose a model that accounts for the capillary force, the granular texture, and particle size polydispersity. We find fairly good agreement of the theoretical estimate of the shear strength with both experimental data and simulations. From numerical data, we analyze the connectivity and anisotropy of different classes of liquid bonds according to the sign and level of the normal force as well as the bond direction. We find that weak compressive bonds are almost isotropically distributed whereas strong compressive and tensile bonds have a pronounced anisotropy. The probability distribution function of normal forces is exponentially decreasing for strong compressive bonds, a decreasing power-law function over nearly one decade for weak compressive bonds, and an increasing linear function in the range of tensile bonds. These features suggest that different bond classes do not play the same role with respect to the shear strength.

Journal Article↗

Shear strength of dentin and dentin bonded composites.

PURPOSE: The objective of this study was to compare the shear strength of dentin with the shear strength of dentin bonded composites, and to determine how variables such as composite strength and blade width used during shear testing influence shear strength values. MATERIALS AND METHODS: Dentin test samples (n = 36) were made by milling the anatomical molar crowns to a shape similar to a composite rod bonded to a flat dentin surface. Dentin bonding was accomplished by bonding composites to flat dentin surfaces (n = 72) using Scotchbond MP and Z100 (n = 36) or Silux Plus (n = 36) composites. Shear testing was conducted using a guillotine-like device with a flat blade embracing half the dentin or composite cylinders. The blade thickness was either 0.25, 0.5, 0.75, 1.0, 1.25, or 1.50 mm. Six samples per material and blade thickness were tested. In addition to the above study, the bond strength of Z100 (n = 6) and Silux (n = 6) bonded with Scotchbond MP and tested with an orthodontic edgewire loop were also tested and compared with the bond strength of the Z100 and Silux samples tested with the 0.5 thick blade. All shear testing was done at a load rate of 0.5 mm/min. The results were analyzed using ANOVA and Duncan's multiple range test. RESULTS: The shear strength values when tested with the blades were: dentin = 39.7 +/- 13.0 MPa, Z100 = 29.3 +/- 7.2 MPa, and Silux = 21.1 +/- 4.9 MPa; each group had significantly different values (p < 0.05). The blade thickness had no significant effect on strength (p = 0.471). Comparing the 0.5-mm-wide blade with the edge wire (width = 0.45 mm) revealed a significant difference (p = 0.0014) favoring the blade. Z100 performed better than Silux (p = 0.0014). CONCLUSION: The shear strength of the tested bonding agent is significantly lower than the shear strength of dentin. The shear strength depends on testing method (blade vs loop) and composite material.

Analysis of Variance↗

Experimental investigation of the shear strengths of teeth in the region of the dentinoenamel junction.

The shear strengths of human incisors, canines, premolars, and molars and bovine incisors in the region of the dentinoenamel junction were tested. The median shear strength of all human teeth, 38.99 MPa, was not significantly different from that of bovine teeth, 37.40 MPa. Among the groups of human teeth, the highest median shear strength was obtained from mandibular premolars (46.15 MPa), and the lowest from mandibular canines (32.63 MPa). Physical treatments (cooling or drying) led to a significant reduction in shear strengths. A similar effect was found after exposure to amino butyrate (a caries-removing agent) but not after exposure to sodium hypochlorite (used in endodontic treatment). In all investigated groups of teeth, the fracture areas were mainly in dentin and never exactly at the dentinoenamel junction; indicating that the cohesion of dentin, not the adhesion between dentin and enamel, is the limiting factor in the shear strength.

Aminobutyrates↗

The effect of irradiation time on the shear strength of composites.

OBJECTIVES: The purpose of this study was to determine the shear strength of composites at a specific depth by a double shear test and to relate it to irradiation time. METHODS: Aluminum molds filled with three different composites were irradiated for the manufacturer's recommended time, as well as for three longer and two shorter times. Fifteen cylindrical specimens were prepared for each combination of material and exposure time and subjected to a double shear test based on the principle of rivets connecting various structural members. The shear planes were symmetrically located 1.5 mm from both outer surfaces. RESULTS: Shear strength vs. irradiation time was directly but nonlinearly related. All test materials attained a maximum shear strength value which was not exceeded by a further increase of the exposure time. Maximum values obtained were 42.5 MPa for Heliomolar (Vivadent) and Durafill (Kulzer) and 66.9 MPa for P-50 (3M). Only the shear strengths using the shortest light activation time were significantly different for each product. SIGNIFICANCE: Shear strength of composites at a specific depth is a function of the combination of light energy and the attenuating power of the specific material. A double shear test might serve as an adjunct to microhardness in determining the extent of cure of composites at a specific depth. The advantage of this testing is the extra information to be gathered regarding the ability of composites to withstand internal stresses at a predetermined distance.

Acrylic Resins↗

Factors influencing shear strength of incrementally cured composite resins.

Factors influencing the shear strength of incremental curing of three different composite resins were examined. The first increment was cured under different surface conditions, in air, or under a coverglass. A separate experiment studied the effect of curing in nitrogen atmosphere. There was no difference in the shear strength of the specimens if the first increment was created in air or under a coverglass. One material (Heliomolar RO) showed higher shear strength when cured in increments and one when bulk-cured (Herculite XR). Curing increments in a nitrogen atmosphere increased the shear strength for two of the three materials tested (P50 and Heliomolar). The results showed that the bond strength between the increments of composites was influenced by the surface properties of the composites themselves after they had been cured under the different conditions; it was also affected by the inherent chemical and physical properties of the materials utilized.

Acrylic Resins↗

Comparison of bone-implant interface shear strength of solid hydroxyapatite and hydroxyapatite-coated titanium implants.

The interface shear strength of uncoated Ti-6Al-4V, dense sintered hydroxyapatite (HA), and HA-coated Ti-6Al-4V were compared. Interface shear strength was determined using a transcortical push-out model in dogs 4 and 12 weeks after implantation. The interface shear strength of dense sintered HA and HA-coated Ti-6Al-4V was significantly higher than that of uncoated Ti-6Al-4V (P < .001). There was no significant difference between the interface shear strength of dense sintered HA and HA-coated Ti-6Al-4V. After the push-out test for HA-coated implants, the regions fractured at the bone-coating interface and at the coating-titanium interface coexisted at 4 weeks after implantation. At 12 weeks, the fracture site was, in all cases, the HA coating-titanium interface, and, in a few samples, fractures inside the coating layer also were visible.

Alloys↗

Shear strength of self-curing acrylic cement.

The average shearing strength of surgical Simplex P bone cement has been experimentally evaluated and found to be 5,762 plus or minus 180 psi. The average shearing strength for compact bone is about 10,000 psi. Therefore surgical Simplex P does not resist shear forces as well as compact bone and should not be used as a substitute for bone whenever possible. The inclusion of 10 per cent barium sulfate U.S.P. for radiographic purposes does not adversely affect the shear strength of the cement. This amount of barium is the same percentage by weight as that found in radiopaque Simplex P in clinical usage today. Varying the loading rate between 0.005 and 0.5 in/min slightly affected the magnitude of the shear force at failure. A comparison of the effect of short term curing times on the magnitude of the shear force at failure reveals that surgical Simplex P strengthens with time. The curing periods varied from 2 to 168 hours.

Acrylic Resins↗

Effect of surface roughness of hydroxyapatite-coated titanium on the bone-implant interface shear strength.

We have investigated the bone-implant interface shear strength of hydroxyapatite (HA)-coated Ti-6Al-4V (HA-coating A) (roughness average, Ra = 3.4 +/- 0.5 microns) and HA-coated Ti-6Al-4V with a rougher surface (HA-coating B) (Ra = 8.4 +/- 1.8 microns). There was no significant difference between HA-coating A and HA-coating B implants with respect to the bone-implant interface shear strength as determined in push-out tests using the transcortical model in adult dogs. The bone-implant interface shear strength of bead-coated porous Ti-6Al-4V was significantly greater than that of both HA-coating A and HA-coating B implants. The failure site, as determined by scanning electron microscopy, was the coating-substrate interface, not the coating-bone interface. This indicates a need to protect the HA coating from the direct shear forces. HA coating enhances early bone growth into the porous surface of the implant. Long-term fixation should depend on bone anchoring to this porous surface. Hydroxyapatite coatings must be developed which do not obstruct the pores of the surface of the implant.

Analysis of Variance↗

Dentin shear strength: effects of tubule orientation and intratooth location.

OBJECTIVES: Dentin has a highly oriented tubule structure, and the tubule number density and area fraction of intertubular dentin vary with distance from the pulp. This investigation sought to determine the influence of tubule orientation on shear strength of dentin from samples derived at various intratooth locations. METHODS: Third molars were sectioned and prepared to provide samples from two locations (center and cusp) and with one of three specific tubule orientations. In series 1, matched pairs of midcoronal samples were tested using two tubule orientations. A paired t-test was used for statistical analysis. In series 2, three samples from central and cuspal areas were tested using three different tubule orientations. A two-day ANOVA was used for statistical analysis. Each sample had dimensions of approximately 1 x 1 x 5 mm and was tested in a hydrated state by a single plane lap shear method. RESULTS: The paired dentin samples of the midcoronal dentin in the two orientations had shear strengths of 72.4 +/- 15.6 MPa and 78.4 +/- 13.2 MPa, and were not significantly different (p > 0.05; paired t-test). In the second series, samples from the center location with tubules parallel to the shear plane with applied force in directions rotated by 90 degrees did not exhibit a significant difference (p > 0.05), with an average value of 53.5 +/- 9.5 MPa. Samples oriented with tubules along the long axis of the specimen and tested with shear force applied perpendicular to the tubule direction had significantly higher (p < 0.05; two-way ANOVA) shear strength (78.0 +/- 8.5 MPa). The specimens from the cusp area did not exhibit a statistically significant difference (p > 0.05; two-way ANOVA) with respect to the three orientations (83.6 +/- 8.4; +/- 13.8; 91.8 +/- 12.7 MPa). Cuspal areas were stronger than central areas in two of the three orientations tested. SIGNIFICANCE: Results indicated that the shear strength differs in central and cusp areas and is dependent on dentin tubule orientation in the central area. Shear strengths were much larger than values reported in shear bond strength tests. This suggests that dentin shear strength is far in excess of dentin bond strengths using shear tests, and that fractures through dentin in such result from flaws or stress concentration in the dentin.

Analysis of Variance↗

Bone-methyl methacrylate interfacial shear strength: an experimental study of dogs.

Bone-methyl methacrylate interfacial shear strength at failure in chronically implanted hip prostheses was studied. Gorman total hip prostheses fixed with methyl methacrylate bone cement were implanted in 6 large dogs. Interface shear strength studies were performed at 8, 16, and 24 weeks. Mechanical testing determined that the mean interfacial shear strength was 15.2 +/- 13.0 kg/cm2. Variability of the data was too great to allow conclusions to be drawn from statistical analysis, but trends in the data were observed. It was concluded that the interfacial bond had sufficient strength to withstand axial loads 3 to 6 times greater than those applied under normal physiologic conditions.

Animals↗

Retentive shear strengths of various bonding attachment bases.

The purpose of this study was to determine whether any of the commercially available attachment bases had significantly better retentive properties. This was determined by their shear strengths after all were bonded to bovine incisors with Auto-Tach. The mean shear strengths of sixteen bases were statistically compared to each other at 24 hours and at 30 days. In addition, the data were converted to pounds per square inch to ascertain if the size of the base significantly influenced the mean shear strength. It was concluded that (1). one of the foil mesh bases tested for shear strength was significantly superior to the two other base designs (indents with undercuts and solid bases with perforations); (2). mechanical retention of the attachment bases to the adhesive was not significantly affected after being placed in distilled water at 37 degrees C. either for 24 hours or for 30 days; (3). smaller foil mesh bases could be used without sacrificing significant shear strength.

Adhesives↗

Shear strength of orthodontic direct-bonding adhesives.

A total of 210 double-width stainless steel edgewise brackets with retentive lip bases were bonded to bovine incisors with seven commercially available direct-bonding materials. Ten samples for each of the seven direct-bonding materials were tested for shear strength using the Instron Universal Testing Instrument. The samples were tested after 1 day, 1 month, and 3 months of immersion in 30 per cent physiologic saline solution. The mean shear strength of each direct-bonding material at each time interval was compared statistically to the mean shear strength of each of the materials at each time interval with a matched 1 test. The same test was used to determine whether there had been a significant change in mean shear strength from start to finish of testing for each material. One product showed a significantly better mean shear strength than any other material at each test interval. The remaining materials were grouped in middle or low ranges, depending upon their final mean shear strengths and degrees of nonsignificance when compared to each other.

Acrylic Resins↗

The role of organic tissue on the punch shear strength of human dentin.

OBJECTIVES: The tendency to fracture of human teeth has been attributed to numerous reasons, including pulpless tooth dehydration, tooth structure degeneration, and excessive spreader loading. To date, however, no consistent data has been gathered to ascertain the effect of organic tissue on the biomechanical properties of human dentin. This study explored the influences of organic tissue removal on the morphological changes and punch shear strength by means of low vacuum wet scanning electron microscope (Wet-SEM) and punch shear apparatus. METHODS: The crown dentin slices with a thickness of 0.45-0.50 mm were prepared from extracted human molars. These specimens were immersed in 5% NaOCl for 1, 3, and 6 h to remove the organic tissue. The dynamic morphological changes of these dentin slices after immersion were observed using Wet-SEM. In addition, the punch shear strength and stiffness of specimens were measured. RESULTS: The removal of organic tissue by 5% sodium hypochlorite treatment caused many cracks on the specimen surfaces. Intertubular and peritubular dentin were also affected, causing an abnormal configuration of dentinal tubule orifices. The 5% sodium hypochlorite treatment for 1, 3, and 6 h significantly reduced the punch shear strength of dentin. As the immersion time increased, the values of punch shear strength also diminished. CONCLUSIONS: The organic tissue loss of human dentin would affect the structure of intertubular and peritubular dentin and cause many cracks on the dentin surface. The punch shear strength of human dentin also reduced after removal of organic tissue.

Chondroitin Sulfates↗

Compression shear strength and tableting behavior of microcrystalline cellulose agglomerates modulated by a solution binder (polyethylene glycol).

PURPOSE: To investigate the possibility of modulating the compression shear strength of agglomerates by the incorporation of a solution binder and to study the subsequent effect on the deformation behavior and tablet forming ability of the agglomerates. METHOD: Various concentrations (0.5 to 10%) of polyethylene glycol were incorporated as a solution binder into microcrystalline cellulose agglomerates of different porosity (10 and 20%) and the shear strength of the agglomerates, as evaluated by the 1/b value of the Kawakita equation, and the permeability to air and tensile strength of tablets formed from them were determined. RESULTS: Increased agglomerate porosity and concentration of polyethylene glycol reduced the 1/b values, which led to the formation of tablets with a lower permeability. A decreased tablet permeability corresponded to an increased tablet tensile strength except that the highest binder content was associated with a drop in the tablet tensile strength. CONCLUSIONS: The solution binder reduced the agglomerate shear strength, which was expressed as an increased degree of agglomerate deformation during compression. The latter seemed to be controlled by both agglomerate porosity and shear strength. The main role of the solution binder in improving the agglomerate compactability was to increase the degree of deformation of agglomerates during compression.

Cellulose↗

Preliminary study of interfacial shear strength between PMMA precoated UHMWPE acetabular cup and PMMA bone cement.

Followed by successful demonstration of high interfacial tensile strength in a new design of cemented all-polyethylene acetabular cup, interfacial shear strength was investigated in this study, with the use of canine-size prototypes of polymethylmethacrylate (PMMA) precoated UHMWPE acetabular cups. In addition to the PMMA precoated prototypes, three different types of controls were also prepared and tested: grooved UHMWPE cups, PMMA (bone cement) cups, and noncoated, plain UHMWPE cups. The interfacial shear strength of the precoated prototypes was 10.1 +/- 0.69 MPa (n = 6), whereas it was 24.3 +/- 0.78 MPa (n = 2) for the PMMA cup, 6.95 +/- 0.21 MPa (n = 2) for the grooved UHMWPE cup, and 0.34 +/- 0.47 MPa (n = 2) for the UHMWPE cup. These results indicate benefits of the PMMA precoating to stabilize the polyethylene acetabular cup securely when applied with bone cement in simulated clinical applications. Analysis of the failed PMMA precoated UHMWPE prototype cups suggested that the chemically induced bonds between precoated PMMA layer and bone cement played a key role in developing high shear strength. After the interfacial shear test of the PMMA precoated prototypes, major disruptions at the interface between treated UHMWPE and precoated PMMA layer were observed by scanning electron microscopy (SEM), which was a unique failure pattern, not found with other prototypes.

Animals↗

Some physical and mechanical factors affecting the simple shear strength of methylmethacrylate.

An investigation of the effect of kneading time on the simple shear strength of cold-cured plain methylmethacrylate bone cement and on the effect of anchor-hole configuration on the load-carrying capabilities of the cement anchor-hole configuration demonstrates that at a strain-rate of 10-3 rad/second, the mean simple shear strength of the cement was 251.65 (plus or minus 3%) for both 30-second and 2-minute kneading times. Increasing the loading rate to 10-1 rad/second increased the simple shear strength of 326.20 kg/cm-2 (plus or minus 2%). The geometric configuration did not significantly affect the maximum shear load-carrying capabilities of the methylmethacrylate.

Acetabulum↗