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At least 1,765 records · Page 98Linked to original sources
PubMed2005

Effects of gap size and UV dosage on decolorization of C.I. Acid Orange 7 by UV/H2O2 process.

Wastewater from textile processing plants can be highly colored and difficult to decolorize. During the past few years attention has been drawn to chemical techniques that could be used to textile wastewater decolorization. A crucial feature in designing such systems is the optimization of operating conditions. In the present study, advanced oxidation treatment, the UV/H(2)O(2) process has been applied to decolorization of the azo dye C.I. Acid Orange 7 (AO7) in aqueous solution in a batch photo reactor. The effects of the reactor gap size and UV dosage on decolorization of dye have been investigated. The method of study involved monitoring the rate of dye solution decolorization during irradiation by a low-pressure mercury lamp and varying gap size and volume of the reactor. The rate of color removal was studied by measuring of the absorbance at characteristic wavelength. The gap size of the reactor was adjusted by different depths of the reactor. The results of this study showed that the removal efficiency of AO7 is optimal with 0.3 cm gap size and 83.33 Wl(-1) of UV dosage.

Azo Compounds↗
PubMed2006

Interface pressure and stiffness of ready made compression stockings: comparison of in vivo and in vitro measurements.

OBJECTIVE: It is unknown if the pressure values of compression stockings indicated by the producers correspond to the actual compression pressure exerted in vivo. This study compared pressure and stiffness of ready-made compression stockings (Venosan) of different classes, measured on the leg and by laboratory testing. METHODS: This was an experimental study conducted in a textile laboratory of a company that manufactures compression stockings. Twelve legs from healthy volunteers were fitted with ready-made calf-length compression stockings of the European classes I, II and III. In addition, two class I stockings were applied over each other. The in vivo interface pressure was measured using the medical stocking tester (MST) in position B1, eight cm proximal to the inner ankle. Stiffness was defined by an increase of pressure due to an increase of stretch that reflects the elastic property of the textile and was assessed by measuring the difference of interface pressure between standing and supine position at B1. In the laboratory, the MST was used to check the pressure of these stockings on wooden leg models. Then circular slices were cut out from the stockings at the B1 level and stretched by a Zwick dynamometer in the transverse direction. Force/extension-curves were plotted, from which the pressure and stiffness of each individual stocking was calculated. RESULTS: The pressure profile measured on four positions along the leg by MST showed a degressive gradient on the wooden model but not on the human leg due to the measuring geometry in the ankle region. Pressure values on the leg correspond to the in vitro measurements calculated from the force/extension-curve with a bias (difference of the means) of -2.1 and 4.1 mm Hg. In 95% of the subjects, the difference was between -10.1 and 5.8 mm Hg (Bland Altman plot). The correlation between in vivo and in vitro measurement was highly significant (P < .0001, Spearman correlation coefficient; r = .8161). In vivo and in vitro measurement shows an increase of stiffness with increasing compression classes. The highest values are found for two class I stockings applied over each other. CONCLUSION: Pressure and stiffness can be measured in vivo, correlate well with laboratory findings, and should be used in future studies, especially when different compression devices are to be compared.

Adult↗
PubMed2004

Use of ultrasonic energy for intensification of the bio-preparation of greige cotton.

Raw unscoured cotton contains approximately 90% cellulose and various noncellulosic impurities such as waxes, pectins, proteins, and fats. To remove these hydrophobic noncellulosics and produce a highly absorbent fiber that can be dyed and finished uniformly, the greige cotton is traditionally processed with relatively harsh and environmentally unfriendly chemicals. New bio-preparation processes that utilize highly specific enzymes instead of conventional organic/inorganic chemicals are becoming increasingly popular in the textile industry. The major shortcoming of this new technology is that the processing time is much longer than the conventional method. This limitation was overcome by use of ultrasound energy in combination with enzyme processing. The combined enzyme/ultrasound bio-preparation of greige cotton offers significant advantages such as less consumption of expensive enzymes, shorter processing time, better uniformity of treatment and a notable decrease in the amount and toxicity of the resulting textile wastewater effluents.

Cotton Fiber↗
PubMed2004

Effects of ultrasonic energy on the wash fastness of reactive dyes.

The field of ultrasonic is still making strides towards perfection, but already many applications of ultrasonic energy have been found in science and technology. There is also a field called sonochemistry where ultrasonic energy is used to create some chemical and mechanical effects on matter immersed or solved in liquids. It was presumed that ultrasonic textile washing could be a competitive alternative to conventional textile washing techniques; and as such the following experiments were conducted. In this study, the effects of ultrasonic energy on the wash fastness of reactive dyes, which have three different reactive groups, were investigated. After dyeing with the conventional method, the samples were applied with three types of washing processes simultaneously (conventional, ultrasonic probe and ultrasonic bath) and comparisons were made. Three different fixing agents were used in the washing processes. Colourfastness, staining fastness, magnitude of total colour difference (DeltaE) and lightness difference of the colour (DeltaL) values of dyed samples were measured.

Journal Article↗
PubMed2004

Effect of ultrasonic energy in washing of medical surgery gowns.

Today, the use of medical textiles is very important for health and hygienic purposes. Although some of medical textile materials are disposable, surgery gowns are usually laundered and re-used. After the laundering it is desirable to have these gowns keeping some of their properties such as anti-microbial and tenacity properties. For this in mind, different surgery gowns were washed and compared. In this work, a special blend of polyester carbon anti-microbial and other surgery gowns were stained with blood and later washed with both conventional method and with ultrasonic energy. The results were also analysed spectrophotometrically and the tenacity of the fabrics were determined.

Carbon↗
PubMed1998

Protection against solar ultraviolet radiation.

Interest in protection against solar ultraviolet radiation (UVR) among the general public in Australia has been increasing steadily as a result of the 'SunSmart' campaigns run by the various state cancer councils. This increasing awareness is due in part to the requirements for occupational protection of outdoor workers and to provision of UVR protection for the recreational market. Behaviour outdoors can significantly affect exposure to solar UVR and use of items of personal protection can provide a substantial reduction in the UVR dose received. The protective properties of sunscreens, sunglasses, hats and clothing against UVR have been the subject of considerable research for some time, and over the last few years interest has extended to the provision of shade structures and the UVR protection provided by various commonly used materials. These materials include shadecloth, plastics, glass, windscreens and applicable tints. Australia has rigorous standards covering protection and UVR, in particular for sunscreens [Standards Australia/Standards New Zealand, Sunscreen products-evaluation and classification, Report No. AS 2604, Sydney/Wellington, 1993.], sunglasses [Standards Australia, Sunglasses and fashion spectacles-nonprescription types, Report No. AS 1067.1, Sydney, 1990.], protective eyewear [Standards Australia/Standards New Zealand, Eye protectors for industrial applications, Report No. AS/NZS 1337, Sydney/Wellington, 1992.] and shadecloth [Standards Australia, Synthetic shadecloth, Report No. AS 4174, Sydney, 1994.]. Compliance with the sunglass standard became mandatory in 1988 and UVR protection provided by sunglasses has increased substantially since then. In July 1996 a standard on 'sun protective textiles' [Standards Australia/Standards New Zealand, Sun protective clothing-evaluation and classification, Report No. AS/NZS 4399, Sydney, 1996.] incorporating ultraviolet protection factors (UPFs) and a rating scheme with protection categories, was introduced; this was the first of its kind in the world. Australian Radiation Laboratory (ARL) UPF swing tags with UVR protection advice from the Australian Cancer Society on the reverse side are used to denote the amount of protection against solar UVR provided by clothing. To date in excess of 5 million ARL swing tags have been issued. Work on the various standards is continuing. The maximum allowed 'sun protection factor' (SPF) limit for sunscreens may be increased to SPF 30 + in the near future, and additions to the sun protective textiles standard are also planned. This paper discusses measurement methods, results, the rationale used in formulating the Australian Standards and the current state of UVR protection in Australia.

Australia↗
PubMed2002

Antifeedant activity of an anthraquinone aldehyde in Galium aparine L. against Spodoptera litura F.

The insect antifeedant anthraquinone aldehyde nordamnacanthal (1,3-dihydroxy-anthraquinone-2-al) was identified in Galium aparine L., and isolated from the root powder of akane (Rubia akane), a member of the Rubiaceae. Structure-activity relationship (SAR) studies using a series of anthraquinone analogues suggested that the aldehyde group on the anthraquinone was more important than the quinone moiety for antifeedant activity against the common cutworm (Spodoptera litura). High levels of nordamnacanthal were found in the seed leaf stage and in callus tissue induced from seedlings of G. aparine, but its concentration decreased with plant development. Since these compounds are natural pigments for dying textiles, we also evaluated the antifeedant activity against the carpet beetle (Attagenus japonicus ), a textile pest was also evaluated. While nordamnacanthal had strong antifeedant activity against the common cutworm, it did not show any antifeedant activity against the carpet beetle. The most effective antifeedant against the carpet beetle was the major constituent in the extract of R. trictorum, lucidin-3-O-primeveroside, a food pigment.

Aldehydes↗
PubMed2002

Ozonation of hydrolyzed azo dye reactive yellow 84 (CI).

The combination of chemical and biological water treatment processes is a promising technique to reduce recalcitrant wastewater loads. The key to the efficiency of such a system is a better understanding of the mechanisms involved during the degradation processes. Ozonation has been applied to many fields in water and wastewater treatment. Especially for textile mill effluents ozonation can achieve high color removal, enhance biodegradability, destroy phenols and reduce the chemical oxygen demand (COD). However, little is known about the reaction intermediates and products formed during ozonation. This work deals with the degradation of hydrolyzed Reactive Yellow 84 (Color Index), a widely used azo dye in textile finishing processes with two monochlorotriazine anchor groups. Ozonation of the hydrolyzed dye in ultra pure water was performed in a laboratory scale cylindric batch reactor. Decolorization, determined by measuring the light absorbance at the maximum wavelength in the visible range (400 nm), was almost complete after 60 and 90 min with an ozone concentration of 18.5 and 9.1 mg/l, respectively. The TOC/TOC0 ratio after ozonation was about 30%, the COD was diminished to 50% of the initial value. The BOD5/COD ratio increased from 0.01 to about 0.8. Oxidation and cleavage of the azo group yield nitrate. Cleavage of the sulfonic acid groups of aromatic rings caused increases in the amount of sulfate. Formic acid and oxalic acid were identified as main oxidation products by high performance ion chromatography (HPIC). The concentrations of these major products were monitored at defined time intervals during ozonation.

Azo Compounds↗
PubMed2000

Spatial and temporal regulation of the pesticide dieldrin within industrial catchments

The river catchments of south Yorkshire support a very high density of wool processing industries. Dieldrin was once used as a moth proofing agent, as a sheep dip, and as a pesticide to protect wool fleeces during storage and transport, all of which caused pollution of these catchments due to textile processing. Weekly sampling of four of these rivers revealed two classes of dieldrin contamination: the Aire and Calder (the rivers which support very high concentrations of wool processing industries) had higher concentrations (averaging approximately 3 ng/l) than the Don and Trent (approximately 1 ng/l). The average flux of dieldrin from these rivers into the Humber estuary was 9.8 g/day, with the Aire (of which the Calder is a tributary) and the Trent contributing almost equally, with a smaller contribution from the Don. The Trent has the highest average flow, explaining its large contribution to dieldrin flux. Less detailed sampling of rivers from the north Humber catchment which drain predominantly rural areas had dieldrin concentrations similar to the heavily industrialized southern catchment rivers. This suggests that dieldrin from agronomic and domestic usage may be more persistent than the pollution caused by textile processing industries. Evidence is presented to suggest that the principle dieldrin sources to the Humber catchments are sewage treatment plants, and that the dieldrin sources are in rapid equilibrium with the water column.

Journal Article↗
PubMedDate not supplied

A Sensate Liner for personnel monitoring applications.

This program develops and demonstrates technologies useful for implementing a manageable cost effective systems approach to monitoring the medical condition of personnel by way of an instrumented uniform hereafter referred to as a Sensate Liner (SL). The SL consists of a form fitting garment which contains and interconnects sensing elements and devices to an electronics pack containing a processor and transmitter. The SL prototype requires fiber, textile, garment and sensor development. The SL textile consists of a mesh of electrically and optically conductive fibers integrated into the normal structure (woven or knitted) of fibers and yarns selected for comfort and durability. A suite of SL garment compatible embedded biological and physical sensors are then integrated into the SL. The initial SL sensor suite is selected to improve triage for combat casualties. Additional SL sensor concepts for medical monitoring will be discussed.

Aerospace Medicine↗
PubMed2001

Lactic acid-stabilised albumin for microsphere formulation and biomedical coatings.

Microspheres of ovalbumin (OVA) ranging from 1 to 15 microm were prepared by emulsifying an aqueous solution of albumin in soya oil at room temperature then raising the temperature to 45 degrees C for 30 min, prior to harvesting of the microspheres. Production of OVA nanospheres with size less than 500 nm was achieved by desolvation from aqueous albumin solutions using acetone. In both cases, lactic acid was added to the starting albumin solution to stabilise the resulting particles. Utilisation of an endogenous substance avoids the use of chemical crosslinking agents such as glutaraldehyde and associated toxicological concerns. Protein coating of knitted Dacron vascular grafts was performed by impregnation of the textile structure with lactic acid-stabilised ovalbumin nanospheres thereby providing a surface potentially resistant to blood platelet adhesion but conducive to endothelialisation. Protein release testing carried out in PBS at 37 degrees C revealed that approximately 60% of the original albumin coating was retained by the Dacron graft material after 4 days and remained at this level for upto 4 weeks. Apart from the formulation of albumin microspheres for drug delivery, diagnostic applications and coating of biomedical textiles, the process of albumin stabilisation using lactic acid may be usefully applied to improve protein immobilisation on a wide range of biomaterial surfaces.

Blood Vessel Prosthesis↗
PubMed2001

Use of laccase together with redox mediators to decolourize Remazol Brilliant Blue R.

A pure fungal laccase, obtained from a commercial formulation used in the textile industry, did not decolourize Remazol Brilliant Blue R (RBBR). Decolourization was only observed when a small molecular weight redox mediator was added together with the laccase. Under the conditions specified, violuric acid (5.7 mM) was the most effective mediator studied and almost complete decolourization was observed within 20 min. In contrast, 1-hydroxybenzotriazole (HOBT, 11 mM) decolourized RBBR at about a two-fold slower rate and to a lesser extent. Also, higher concentrations of HOBT were inhibitory which could be due to inactivation of laccase by the toxic HOBT radical. The commercial laccase formulation that contained phenothiazine-10-propionic acid as the mediator was least effective, giving 30% decolourization under equivalent conditions. We suggest that similar laccase plus mediator systems could be used for the detoxification of related anthraquinone textile dyes.

Anthraquinones↗
PubMed2001

Applications of pectinases in the commercial sector: a review.

Pectinases are one of the upcoming enzymes of fruit and textile industries. These enzymes break down complex polysaccharides of plant tissues into simpler molecules like galacturonic acids. The role of acidic pectinases in bringing down the cloudiness and bitterness of fruit juices is well established. Recently, there has been a good number of reports on the application of alkaline pectinases in the textile industry for the retting and degumming of fiber crops, production of good quality paper, fermentation of coffee and tea, oil extractions and treatment of pectic waste water. This review discusses various types of pectinases and their applications in the commercial sector.

Beverages↗
PubMedDate not supplied

The evidential value of black cotton fibres.

Forensic scientists are faced with the problem of estimating the frequency of cotton fibres recovered in casework, in relation to those in the general population. One way of doing this is to consider the degree of spectral variation that occurs within a "block of colour". When a spectral pattern occurs very frequently, the evidential value of the fibres may be so low, that it is not worth considering them as target fibres. Using UV-visible range microspectro-photometry (MSP) spectra were recorded from 88 known black cotton dyes and 225 samples of black cotton taken from various textiles. UV-visible spectra originating from sulphur dyes and from the great majority of reactive and direct dyes can be easily recognised. Vat dyes present a little more difficulty. The degree of spectral variation and consequent discriminating power of MSP varied according to the dye class, from 0.13 for sulphur dyes to 0.93 for reactive dyes. From 99 textiles dyed with reactive dyes, the spectra could be divided into at least 40 varieties showing that these fibres have a high degree of individuality. Within the few direct dyes (11.5%) that were encountered, one basic spectral form predominated, but a number of minor variations were observed. Spectral information below 400 nm (UV-range) is important for making distinctions and is critical in the case of direct dyes.

Clothing↗
PubMed2001

Synthesis of 2-phenylbenzotriazole-type mutagens, PBTA-5 and PBTA-6, and their detection in river water from Japan.

We previously determined the chemical structures of four 2-phenylbenzotriazole mutagens (PBTA-1, -2, -3 and -4) in blue rayon-adsorbed material from the Nishitakase River in Kyoto prefecture and the Nikko River in Aichi prefecture in Japan. On the basis of a synthesis study, these four PBTA derivatives were deduced to have originated from corresponding dinitrophenylazo dyes by reduction and chlorination. 2-[(2-Bromo-4,6-dinitrophenyl)azo]-5-[bis(2-acetoxyethyl) amino]-4-methoxyacetanilide (Color Index Name, Disperse Blue 79:1; CAS Registry Number, 75497-74-4) is a very common dinitrophenylazo dye used in textile dyeing factories. In the present study, we synthesized 2-[4-[bis(2-acetoxyethyl)amino]-2-(acetylamino)-5-methoxyphenyl]-5-amino-7-bromo-4-chloro-2H-benzotriazole (PBTA-5) from Disperse Blue 79:1 by reduction with sodium hydrosulfite and subsequent chlorination with sodium hypochlorite. On hydrolysis of PBTA-5 with alkali, 2-[2-(acetylamino)-4-[bis(2-hydroxyethyl)amino]-5-methoxyphenyl]-5-amino-7-bromo-4-chloro-2H-benzotriazole (PBTA-6) was obtained. Both PBTA-5 and -6 were potent mutagens, inducing 723,000 revertants and 485,000 revertants per microgram of Salmonella typhimurium YG1024, respectively, in the presence of S9 mix. To clarify whether PBTA-5 and -6 exist in the environment, water samples were collected from five rivers flowing through regions where textile dyeing industries are developed. PBTA-6 was detected at levels of 3-134 ng/g blue rayon in all water samples that were examined. On the other hand, the amount of PBTA-5 in the samples was less than the detection limit.

Adsorption↗
PubMed2005

Definition of the M-conotoxin superfamily: characterization of novel peptides from molluscivorous Conus venoms.

Most of the >50,000 different pharmacologically active peptides in Conus venoms belong to a small number of gene superfamilies. In this work, the M-conotoxin superfamily is defined using both biochemical and molecular criteria. Novel excitatory peptides purified from the venoms of the molluscivorous species Conus textile and Conus marmoreus all have a characteristic pattern of Cys residues previously found in the mu-, kappaM-, and psi-conotoxins (CC-C-C-CC). The new peptides are smaller (12-19 amino acids) than the mu-, kappaM-, and psi-conotoxins (22-24 amino acids). One peptide, mr3a, was chemically synthesized in a biologically active form. Analysis of the disulfide bridges of a natural peptide tx3c from C. textile and synthetic peptide mr3a from C. marmoreus showed a novel pattern of disulfide connectivity, different from that previously established for the mu- and psi-conotoxins. Thus, these peptides belong to a new group of structurally and pharmacologically distinct conotoxins that are particularly prominent in the venoms of mollusc-hunting Conus species. Analysis of cDNA clones encoding the novel peptides as well as those encoding mu-, kappaM-, and psi-conotoxins revealed highly conserved amino acid residues in the precursor sequences; this conservation in both amino acid sequence and in the Cys pattern defines a gene superfamily, designated the M-conotoxin superfamily. The peptides characterized can be provisionally assigned to four distinct groups within the M-superfamily based on sequence similarity within and divergence between each group. A notable feature of the superfamily is that two distinct structural frameworks have been generated by changing the disulfide connectivity on an otherwise conserved Cys pattern.

Amino Acid Sequence↗
PubMedDate not supplied

Aerobic degradation of a mixture of azo dyes in a packed bed reactor having bacteria-coated laterite pebbles.

A microbial consortium capable of aerobic degradation of a mixture of azo dyes consisting of two isolated strains (RRL,TVM) and one known strain of Pseudomonas putida (MTCC 1194) was immobilized on laterite stones. The amount of bacterial biomass attached to the laterite stones was 8.64 g per 100 g of the stone on a dry weight basis. The packed bed reactor was filled with these stones and had a total capacity of 850 mL and a void volume of 210 mL. The feed consisted of an equal mixture of seven azo dyes both in water as well as in a simulated textile effluent, at a pH of 9.0 and a salinity of 900 mg/L. The dye concentrations of influent were 25, 50, and 100 microg/mL. The residence time was varied between 0.78 and 6.23 h. It was found that at the lowest residence time 23.55, 45.73, and 79.95 microg of dye was degraded per hour at an initial dye concentration of 25, 50, and 100 microg, respectively. The pH was reduced from 9.0 to 7.0. Simulated textile effluent containing 50 microg/mL dye was degraded by 61.7%. Analysis of degradation products by TLC and HPLC showed that the dye mixture was degraded to nontoxic smaller molecules. The bacteria-coated pebbles were stable, there was no washout even after 2 months, and the reactor was found to be suitable for the aerobic degradation of azo dyes.

Aerobiosis↗
PubMedDate not supplied

Bioengineering of a cellulosic fabric for insecticide delivery via grafted cyclodextrin.

beta-Cyclodextrin (beta-CD) can be easily grafted onto cellulosic textiles through covalent bonds. In such a way beta-CD empty cavities provide an efficient tool for entrapping different kinds of hydrophobic molecules on the surface of the fabric and releasing them slowly in time. The capability of cyclodextrins to include hydrophobic molecules such as fragrances, antimicrobial agents, and other chemicals can be then exploited to produce new grafted textiles with peculiar and useful performances. In this work we report the inclusion of two different products, the pyrethroid insecticide permethrin (PERM) and the insect repellent N,N-diethyl-m-toluamide (DEET), into beta-CD molecules grafted on cotton fabric. UV-vis spectrophotometry and thermal analysis confirmed the presence of the guest molecules on the fabric surface. Bioassays were carried out on two mosquito species of medical importance, Aedes aegypti and Anopheles stephensi; knock down effect and mortality were measured using standard World Health Organization (WHO) cone tests. Repellency and irritancy (blood feeding inhibition) were also measured using cage tests and a baited tunnel device. PERM-treated fabrics kept the insecticidal/irritant efficacy even for a long time after the treatment, whereas DEET activity lasted more shortly.

Aedes↗