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Acrylic resin blockout for interim removable partial dentures.

A technique using autopolymerizing acrylic resin as a blockout material has been described. This technique greatly simplifies the laboratory construction and insertion phases of the complex interim removable partial denture. It is not suggested that the acrylic blockout replace the wax blockout if a heat-cured denture base is not indicated. Wax should be used if a "sprinkle-on" autopolymerizing acrylic resin is used for the denture base.

Acrylic Resins↗

In vivo and in vitro evaluation of the efficacy of a peracetic acid-based disinfectant for decontamination of acrylic resins.

The purpose of this study was to assess the antimicrobial efficacy of a peracetic acid-based disinfectant for decontamination of heat-polymerized, chemically activated and microwave-polymerized acrylic resins. Resin plates were contaminated in vivo upon intraoral use by 10 volunteers for 7 nights and slabs were contaminated in vitro by contact with Bacillus subtilis and Bacillus stearothermophilus. The contaminated acrylic resin specimens were immersed in a 0.2% peracetic acid-based disinfectant (Sterilife; Lifemed) for 5 min or 10 min and placed in a BHI culture medium. After incubation at 37 degrees C for 48 h, bacterial growth was assessed by analyzing turbidity of the medium. For all types of acrylic resin, no turbidity of the medium was observed for any of the resin specimens immersed in the peracetic acid-based disinfectant for either 5 or 10 min. On the other hand, the media with specimens that were not immersed in the disinfectant (control) showed turbidity in 100% of the cases, indicating the presence of microorganisms in both tested conditions. In conclusion, immersion for at least 5 min in a 0.2% peracetic acid-based disinfectant promoted high-level disinfection of heat-polymerized, chemically activated and microwave-polymerized acrylic resins contaminated with either human saliva or Bacillus subtilis or Bacillus stearothermophilus.

Acrylic Resins↗

The swelling phenomenon of acrylic resin polymer teeth at the interface with denture base polymers.

PURPOSE: This study examined the interface between acrylic resin polymer teeth and denture base polymers. MATERIAL AND METHODS: An autopolymerized denture base polymer was cured either at 30 degrees C, 50 degrees C, or 70 degrees C, and a heat-cured denture base polymer was cured at 100 degrees C in contact with acrylic resin polymer teeth. The specimens were ground wet and polished to a thickness of 0.21 mm for the examination of the interface with a light microscope. The surface of the specimens was then treated with the solvent tetrahydrofuran, and the specimens were examined with a scanning electron microscope (SEM). RESULTS: As a result of grinding, the inner parts of the beads at the interface of the teeth were exposed to the denture base polymer. The inner part in these polymer beads of the polymer teeth swelled to a depth of 3 microns when the autopolymerized polymer was cured at 30 degrees C. When cured at 70 degrees C, the thickness of the swelled layer was 21 microns (p < 0.001). Microscopically, the interface between the heat-cured denture base polymer and the polymer teeth appeared diffuse in the region of the interpenetrating polymer networks (IPN) and the matrix. The IPN appeared as a separate zone in the outer parts of the beads of the teeth, both with the light microscope and with the SEM. CONCLUSIONS: The results suggest that by increasing the polymerization temperature, the monomers of the denture base polymers diffused more effectively into acrylic resin polymer teeth. This increases the bond strength between the polymer teeth and the denture base polymer.

Acrylic Resins↗

Bonding of silicone extra-oral elastomers to acrylic resin: the effect of primer composition.

Silicone elastomer is bonded to acrylic resin in many facial or oro-facial prostheses. The silicone elastomer/acrylic resin bond has been reported to be insufficient and primers have been used to enhance the bond. This study investigated the bond strength of silicone elastomer to acrylic resin using different types of primers. The extra-oral silicone elastomers studied were Cosmesil and Ideal. The "overlap-joint" model was used to evaluate the bond strength and the samples were stretched until fracture. The bonding surfaces were treated with a primer. The control primer was Cosmesil and the others a mixture of Cosmesil/Z-6020 and Cosmesil/A-174 in 50/50 v/v ratio. The bond strength ranged from 0.026 MPa to 0.219 MPa. The results obtained in this work led to the conclusion that the most critical parameter allowing the efficient performance of a primer is the compatibility and affinity of its composition with the selected silicone elastomer.

Acrylic Resins↗

[Long-term results of plastic skull repairs with acrylic resins].

In the period from the beginning of 1956 until June 1978, we closed 312 skull gaps with acrylic resin. We used Palacos G (group I) 205 times and Refobacin Palacos R (group II) 107 times. Owing to the antibiotic action of Palacos, the infection rate, which was 6.8 per cent in the first group, could be lowered to 1.07 per cent even with a larger range of indications. The cosmetic results were very satisfactory. Owing to only slight changes in consistency and elasticity, a good protection of the brain was ensured. With the exception of one patient who temporarily showed psychic alterations, the acrylic resin was not felt as a foreign body. Disagreeable sensations, especially in case of the action of heat and cold such as are occasionally mentioned by wearers of metal plates, did not occur in our patients. Formation of neoplasms caused by polymethyl methacrylate has been found in none of the patients during the observation period of 20 years. The plastic repair with acrylic resin can be carried out quickly and in a simple manner. It may be used in all regions of the cranium. Even larger defects can be closed in this way.

Acrylic Resins↗

Porcelain laminate veneer provisionalization using visible light-curing acrylic resin.

Placement of porcelain laminate veneers has become a relatively common procedure. Occasionally it is necessary to fabricate provisional restorations. For these situations, the use of self-curing acrylic resin and composite resin has been described in the literature. Extensive trimming and finishing procedures are often necessary, and, because of the inherent fragility of the materials, the provisional restorations are prone to breakage. To improve the technique, visible light-curing acrylic resin can be used to fabricate direct provisional restorations. The material is available in several shades, has excellent manipulative properties, and does not necessarily require a custom matrix, offering significant advantages over a composite resin or self-curing acrylic resin.

Acrylic Resins↗

Development and application of methods for determination of residual monomer in dental acrylic resins using high performance liquid chromatography.

Two high-performance liquid chromatographic methods for determination of residual monomer in dental acrylic resins are described. Monomers were detected by their UV absorbance at 230 nm, on a Nucleosil C18 (5 microm particle size, 100 A pore size, 15 x 0.46 cm i.d.) column. The separation was performed using acetonitrile-water (55:45 v/v) containing 0.01% triethylamine (TEA) for methyl methacrylate and butyl methacrylate, and acetonitrile-water (60:40 v/v) containing 0.01% TEA for isobutyl methacrylate and 1,6-hexanediol dimethacrylate as mobile phases, at a flow rate of 0.8 mL/min. Good linear relationships were obtained in the concentration range 5.0-80.0 microg/mL for methyl methacrylate, 10.0-160.0 microg/mL for butyl methacrylate, 50.0-500.0 microg/mL for isobutyl methacrylate and 2.5-180.0 microg/mL for 1,6-hexanediol dimethacrylate. Adequate assay for intra- and inter-day precision and accuracy was observed during the validation process. An extraction procedure to remove residual monomer from the acrylic resins was also established. Residual monomer was obtained from broken specimens of acrylic disks using methanol as extraction solvent for 2 h in an ice-bath. The developed methods and the extraction procedure were applied to dental acrylic resins, tested with or without post-polymerization treatments, and proved to be accurate and precise for the determination of residual monomer content of the materials evaluated.

Acrylic Resins↗

Soft acrylic resin materials containing a polymerisable plasticiser I: mechanical properties.

Conventional soft acrylic resin materials depend on the use of plasticisers for their compliance. In aqueous environments the plasticisers leach out causing the material to harden. Use of a polymerisable plasticiser has been shown to solve this problem. One such material was developed but failed mechanically during clinical trial. The aim of this study was to reformulate to produce a material with improved strength. Three different methacrylate monomers were used with two different levels of plasticiser, each monomer mix was used with the same copolymer powder at three powder/liquid ratios. Tensile strength, tear energy and hardness were measured and results compared with 'Supersoft', a proprietary plasticised acrylic resin soft lining material. All the experimental materials had a higher tensile strength than the original Parker/Braden material. The 30% plasticiser materials with the higher powder/liquid level had strength, tear energy and hardness values in the same range as 'Supersoft'. Materials of improved strength have been produced.

Acrylic Resins↗

[Effect of acrylic resin post-pressing time on dimensional change of total denture base].

The dimensional alterations of denture bases were verified in function of the acrylic resin post-pressing time. Twenty stone cast/wax base sets were confected for routine flasking procedure. Thermosetting acrylic resin (Clássico) was prepared according to the instructions of the manufacturer. After final pressing, the acrylic resin was submitted to polymerization in water at 74 degrees C during 9 hours, following the immediate, 6-, 12-, and 24-hour post-pressing times. The resin bases were fixed on the casts with instantaneous adhesive and the sets were laterally sectioned in the regions corresponding to the distal aspect of canines (A), mesial aspect of first molars (B), and posterior palatal zone (C). The gap between the stone cast and the resin base was measured with a comparative microscope at five referential positions for each kind of sectioning. Data submitted to ANOVA and Tukey's test showed that there was no statistically significant difference between the immediate and the 6-hour post-pressing times as well as between the 12- and the 24-hour post-pressing times. However, there was statistically significant difference between the immediate/6-hour groups and the 12-/24-hour groups.

Acrylic Resins↗

A new method of attaching cast gold occlusal surfaces to acrylic resin denture teeth.

Historically, cast gold occlusal surfaces for complete or removable partial dentures have been fabricated with retentive loops or beads and luted to prepared denture teeth with acrylic resin or attached to tooth-colored, heat-processed acrylic resin. At present, alternatives to mechanical retention for attaching resin to metal include chemical bonding of the resin after placement of intermediate ceramic or tin layers and the use of chemically adhesive resin cements. Compared to mechanical retention, the chemical bonding of resin to metal requires less gold and allows more room for properly contoured and esthetic resin. Additionally, this chemical bond limits microleakage at the resin-metal interface. In the following technique, cast gold occlusal surfaces are fitted to onlay preparations of acrylic resin denture teeth set in a processed denture base. The castings are air-abraded, tin plated, and luted to the denture teeth with Panavia dental adhesive. This method is quick, easy, and economical.

Acrylic Resins↗

Assessment of flexural strength and color alteration of heat-polymerized acrylic resins after simulated use of denture cleansers.

The purpose of this study was to assess flexural strength and color alteration of acrylic resins immersed in denture cleansers for different periods of time. Rectangular specimens (65 x 10 x 3mm) made from three heat-polymerized acrylic resins (Lucitone 550, QC-20 and Triplex) were assigned to three denture cleansers groups (Bony Plus, Corega Tabs and Efferdent Plus) and a control group (immersion in water). Soaking trials of 15 min and 8 h simulated 30 days of use. Flexural strength testing was carried out with 105 specimens on a universal testing machine. Color alterations were visually assessed by examination of photographs taken from 21 specimens. Flexural strength means (in MPa) were analyzed statistically by analysis of variance and Tukey's test at 5% significance level. There were significant differences (p<0.01) among the resins Lucitone (89.439 +/- 7.962), Triplex (88.024 +/- 5.167) and QC-20 (83.379 +/- 7.153). No significant differences (p>0.05) were found either among the denture cleansers (Bony Plus = 87.693 +/- 6.943; Corega Tabs = 86.955 +/- 7.114; Efferdent Plus = 86.195 +/- 7.865 and control = 86.536 +/- 7.012) or between the soaking periods (15 min = 86.875 +/- 7.625 and 8 h = 87.432 +/- 7.355) throughout the soaking cycles simulating 30 days of use. No color alterations were identified by visual examination. The findings of this study showed that chemical denture cleansers used according to the manufacturers' specifications did not cause flexural strength alterations or color changes in heat-polymerized acrylic resins submitted to soaking cycles that simulated 30 days of use.

Acrylic Resins↗

The role of denture cleansers on the whitening of acrylic resins.

Dentists and denture wearers have reported that the regular use of a denture cleanser causes whitening of dentures. The whitening effect of denture cleansers on acrylic resin dentures was investigated using four different types of agents on six different types of acrylic resin discs. The color values of the samples were measured using a reflectometer. The greatest whitening effect was seen on autopolymerizing acrylic resins for one of the denture cleansers with all the resins tested.

Acrylic Resins↗

A clinical evaluation of a glass ionomer cement as an orthodontic bonding adhesive compared with an acrylic resin.

Glass ionomer cement (GIC) has been suggested as an alternative to acrylic resin in bracket bonding because of its fluoride release. The aim of this clinical trial was to evaluate further the suitability of GIC as a bonding adhesive compared with an acrylic resin with regard to frequency of bracket failure, fracture modes and clean-up time after debonding. Two commercially available brackets were tested, one with a meshed foil base and the other with an integral base. A total of 60 patients, with a mean age of 13 years 7 months (range 10 years 8 months to 19 years 1 month) were consecutively selected. Brackets were bonded with a GIC (AquaCem, De Trey) and a no-mix diacrylate (Unite, Unitek Corp.) according to random assignment for each jaw. One group of patients (n = 30) was bonded with metal brackets with machine cut grooves in the base (DynaLock, Unitek). In the second group (n = 30) brackets with a meshed foil base (Unitwin, Unitek) were used. Bracket failure location during treatment was recorded as were fracture modes and time required for the clean-up of enamel surfaces at debonding. The frequency of failed brackets was higher with GIC (36 per cent) than with the diacrylate (15 per cent). Bracket failures for the cut groove base type occurred in 50 per cent with GIC and 23 per cent with the acrylic, meshed foil bases failed in 22 per cent GIC and in 7 per cent with the acrylic, respectively. The differences in failure between bracket types were significant at P < 0.001 for both bonding materials. Analysis of the fracture modes showed a small but noticeable difference in the strength of adhesion to the enamel surface, favouring GIC. Time required for the clean-up of enamel surfaces showed a significantly shorter debonding time for GIC. It is concluded that the use of a GIC for orthodontic bonding purposes considerably increases the risk of bond failures during treatment, especially in combination with a cut groove base type. One noticeable advantage with GIC bonding, however, is the shorter clean-up time for the enamel surfaces.

Acrylic Resins↗

The tensile and shear bond strength of a conventional and a 4-meta self-cure acrylic resin to various surface finishes of CoCr alloy.

This study was designed to compare the tensile and shear bond strengths of two self-cure acrylic resins to cobalt-chromium alloy (CoCr) samples, prepared with six surface finishes. The strongest mean tensile bond strength was recorded between the 4-Meta acrylic resin and Silicoated cobalt-chromium alloy. The strongest mean shear bond strengths showed little variation between the 4-Meta acrylic resin and Silicoated, sandblasted and sandblasted/tinplated cobalt-chromium. This laboratory based study may have important implications for the future design of CoCr dentures.

Acrylic Resins↗

Improving interproximal access in direct provisional acrylic resin restorations.

A new technique that improves interproximal access in direct provisional acrylic resin restorations is presented. In this technique a clear Mylar strip is placed interproximally and lifted off with an overimpression prior to the beginning of the tooth preparation procedures. Preparation of the tooth and fabrication of the provisional restorations then continues in the usual direct manner. The Mylar strip, now embedded in the overimpression, becomes incorporated as a separator between the adjacent provisional restorations. The acrylic resin provisional restorations are easily snapped apart and finished individually. The advantages of the technique and the need for marginal perfection around the full perimeter of the tooth are also discussed.

Acrylic Resins↗