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PubMed2005

Formation characterization of hydroxyapatite on titanium by microarc oxidation and hydrothermal treatment.

Microarc oxidation (MAO) was performed on titanium in an electrolyte containing calcium glycerphosphate (Ca-GP) and calcium acetate (CA) using a direct current power supply. It was found that the MAO method is suitable forming a ceramic coating containing Ca and P using titanium, and that films display a porous and rough structure on their surface. Samples with a Ca/P ratio of 1.71 were hydrothermally treated in water solution whose pH was adjusted to 7.0-11.0 by adding NaOH at 190 degrees C for 10 h in an autoclave. Hydroxyapatite crystals were precipitated on the film surface after the hydrothermal treatment, and the amount of hydroxyapatite precipitated increased with increasing pH of water solution. The oxide film composition was semiquantitatively analyzed with an electron probe microanalyzer. The microstructures on the sample surfaces were observed by scanning electron microscopy before and after the hydrothermal treatment. The topography of the oxide film was imaged with an atomic force microscope. Its cross section was observed by scanning electron microscopy after being coated with a thin Au film. The surface structures of the films were analyzed by X-ray diffraction.

Adhesiveness↗
PubMed2003

Hazardous effects of effluent from the chrome plating industry: 70 kDa heat shock protein expression as a marker of cellular damage in transgenic Drosophila melanogaster (hsp70-lacZ).

Hazardous effects of an effluent from the chrome plating industry were examined by exposing transgenic Drosophila melanogaster (hsp70-lacZ) to various concentrations (0.05, 0.1, 1.0, 10.0, and 100.0 micro L/mL) of the effluent through diet. The emergence pattern of adult flies was affected, along with impaired reproductive performance at the higher dietary concentrations of the effluent. Interestingly, the effect of the effluent was more pronounced in male than in female flies. The effect of the effluent on development of adult flies was concurrent with the expression pattern of the heat shock protein 70 gene (hsp70), both in larval tissues and in the reproductive organs of adult flies. We observed a dose- and time-dependent expression of hsp70 in third instar larvae exposed for different time intervals. Absence of hsp70 expression in larvae exposed to 0.1 micro L/mL of the effluent indicated that this is the highest nontoxic concentration for Drosophila. The stress gene assay in the reproductive organs of adult flies revealed hsp70 expression in the testis of male flies only. However, trypan blue dye exclusion tests in these tissues indicate tissue damage in the male accessory gland of adult flies, which was further confirmed by ultrastructural observations. In the present study we demonstrate the utility of transgenic Drosophila as an alternative animal model for evaluating hazardous effects of the effluent from the chrome plating industry and further reveal the cytoprotective role of hsp70 and its expression as an early marker in environmental risk assessment.

Animals↗
PubMed2006

Waveguide analysis of heat-drawn and chemically etched probe tips for scanning near-field optical microscopy.

We analyze two basic aspects of a scanning near-field optical microscope (SNOM) probe's operation: (i) spot-size evolution of the electric field along the probe with and without a metal layer, and (ii) a modal analysis of the SNOM probe, particularly in close proximity to the aperture. A slab waveguide model is utilized to minimize the analytical complexity, yet provides useful quantitative results--including losses associated with the metal coating--which can then be used as design rules.

Computer-Aided Design↗
PubMed1995

A newly-developed electrodeposited diamond scaler with high abrasive resistance.

A diamond scaler on which blade diamond particles were coated by electrodeposition was developed to improve the abrasive resistance of scaler blades. The electrodeposited coating was tested with diamond particles of four different sizes, designated D-4000 with 2 to 4 microns diameter of the particles; D-800 with 12 to 25 microns; D-600 with 20 to 30 microns; and D-400 with 30 to 40 microns. The abrasive resistance of the scalers was examined quantitatively using a recently-developed automatic scaling apparatus that simulated the scaling process of hand instrumentation, as well as SEM observation of the blades. A series of abrasion tests suggested that all the diamond scalers except D-4000 showed better abrasive resistance than the control (D-0), and that D-600 showed the highest abrasive resistance and cutting quality. The SEM observation also suggested that D-600 and D-400 might have higher abrasive resistance. Furthermore, the profilometric evaluation of the surface roughness of the scaled natural dentin after hand instrumentation indicated that the average surface roughness increased in the order of D-4000, D-800, D-600, and D-400, although no marked differences were observed among D-4000, D-800, D-600 and D-0, but not D-400. These results suggested that the electrodeposited diamond scaler with 20 to 30 microns diamond particles (D-600) might have marked abrasive resistance as well as cutting quality without remarkable damage to the tooth surface after conventional scaling procedure.

Adult↗
PubMed1994

Flexural strength of two electro-plated dental ceramics.

This study aimed to investigate the influence on flexural strength of electro-plating two dental porcelains, Vita Omega and Vita Omega 800. The porcelains were treated in accordance with the manufacturer's instructions, and the specimens were produced following the ISO 6872 standard for rectangular bars. Specimens were divided into three groups, of which none, one, or three of the surfaces were plated with a thin layer of gold. Flexural strength was tested with a three-point bending test. Ten specimens were tested for each combination of porcelain and plating, for a total of 60 test pieces. For both porcelains, a significantly higher flexural strength was found for the specimens furnished with a gold layer. The number of covered surfaces did not significantly influence the tested strength. This increase in strength is most likely due to decreased crack initiation and fracture propagation after the covering of random defects in the porcelain. A better stress distribution might also be anticipated and partly explain the results.

Aluminum Silicates↗
PubMed1993

Principles of biotechnological treatment of industrial wastes.

This review includes current information on biodegradation processes of pollutants, digestor biocenosis and bioadditives, sludge production, measurement of pollution, and advances regarding biotechnological treatment of a series of specific industrial effluents.

Biodegradation, Environmental↗
PubMed1994

Effects of titanium nitride coatings on surface and corrosion characteristics of Ni-Ti alloy.

The structure of a titanium nitride film coated by arc ion plating on a Ni-50Ti shape memory alloy was characterized by X-ray photoelectron spectroscopy (XPS). The corrosion behavior of the titanium nitride-coated Ni-50Ti alloy was examined in 0.9% NaCl solution by potentiodynamic polarization measurements and a polarization resistance method. XPS spectra showed that the titanium nitride film consisted of three layers, a top layer of TiO2, a middle layer of TiNx (x > 1), and an inner layer of TiN. The passive current density for the titanium nitride-coated alloy was approximately two orders of magnitude lower than that of the polished alloy in the potential range from the free corrosion potential to +500 mV (vs. Ag/AgCl). Pitting corrosion associated with breakdown of the coated film occurred above this potential. The polarization resistance data also indicated that the corrosion rate of the titanium nitride-coated alloy at the free corrosion potential (+50-+100 mV) was more than one order of magnitude lower than that for the polished alloy.

Corrosion↗
PubMed1996

Effect of temperature on morphology of electrochemically-deposited calcium phosphates.

Calcium phosphates were electrochemically deposited on titanium plates at temperatures from 4 degrees C to 92 degrees C in a solution of NaCl, K2HPO4 and CaCl2 x 2H20. Scanning electron microscopic studies showed that granular deposits formed on the electrode at electrolyte temperatures of 4 degrees C, 22 degrees C, and 37 degrees C; needle-like deposits formed at 52 degrees C-92 degrees C. The width and length of the needles increased with the temperature of the electrolyte. Based on the results of characterization by electron diffractometry. Fourier transform infrared spectroscopy and X-ray diffractometry, the granular deposits were identified as carbonate-containing calcium phosphate with low crystallinity, and the needle-like deposits as carbonate-containing apatite crystals elongated along the c-axis. Crystallinity of the deposits increased with the temperature of the electrolyte, whereas the orientation indices of the apatite increased with temperature up to 82 degrees C and slightly decreased at 92 degrees C.

Apatites↗
PubMed1999

Hydrothermal-electrochemical deposition of calcium phosphates on various metals.

Calcium phosphates were formed on five kinds of substrate metals using a hydrothermal-electrochemical method in an autoclave with two electrodes. The electrolyte dissolving NaCl, K2HPO4, CaCl2.2H2O, tris (hydroxymethyl) aminomethane, and hydrochloric acid was maintained at 100 degrees C, 150 degrees C and 200 degrees C. The counter electrode, the anode, was platinum plate, 20 x 20 x 0.5 mm, and the working electrodes as cathode were pure titanium, pure zinc, pure nickel, pure iron, and stainless steel plates. A constant direct current at 12.5 mA/cm2 was loaded for 1 hr. Hydroxyapatite [Ca10(PO4)6(OH)2] only deposited at three temperatures on pure titanium plate. On pure zinc plate, both parascholzite [CaZn2(PO4)2.2H2O] and hydroxyapatite were formed at 150 degrees C and both parascholzite and ZnO were formed at 200 degrees C. Both hydroxyapatite and beta-TCP [beta-Ca3(PO4)2] were formed on pure nickel, pure iron, and stainless steel plates at 200 degrees C. It seems that the incorporation of the metal ions released from the electrode decreased the Ca/P ratio of the deposit due to the formation of other compounds except hydroxyapatite.

Calcium Phosphates↗
PubMed2002

Calcium-ion incorporation into titanium surfaces accompanied by electrochemical apatite-deposition.

The depths of calcium-ion incorporation into a commercially pure titanium and an experimental beta-type titanium alloy were determined using Auger electron spectroscopy. After the electrochemical deposition of apatite, new compositional gradients appeared in the profiles in which the Ca and P concentrations gradually decreased as a function of the depth up to 6-8 nm. The relative concentration of Ca in the outermost layer was higher than that of P. On the other hand, after the soaking in a simulated body fluid, the relative concentration of P was higher than that of Ca in the outermost layer. These results suggested that Ca ions were well incorporated into the outermost oxide layer of titanium accompanied by the electrochemical apatite-deposition on its surface.

Apatites↗
PubMedDate not supplied

Retention strength of tin plated gold inlays bonded with two resin cements.

Research has shown bonding of restorations to tooth structure to enhance retention of the restoration to increase the fracture resistance of the tooth, and to reduce microleakage. Resin cements have superior physical properties to traditional cements such as zinc phosphate. The purpose of this study was to compare the retention of gold inlays luted with two resin cements to that of those luted with zinc phosphate cement.

Acid Etching, Dental↗
PubMedDate not supplied

Laboratory evaluation of a metal-priming agent for adhesive bonding.

OBJECTIVE: The purpose of this laboratory study was to determine the bond strength of a base metal alloy to a high-noble alloy and amalgam when a new chemical adhesion promoter was used in conjunction with a resin cement. METHOD AND MATERIALS: Specimens of high-noble alloy and amalgam were prepared in epoxy-filled rings. Base metal cylinders were cast. The ends of the cylinders and the metal bonding substrates were wet ground and air abraded with aluminum oxide. The base metal cylinders were cemented with Panavia 21 resin cement after application of 1 of the following to the high-noble and amalgam metal surfaces: (1) Alloy Primer, (2) ED Primer, (3) Alloy Primer and ED Primer, or (4) tin plating. Bond values were determined after 24 hours' storage and after 3 months' storage and thermocycling. RESULTS: At both 24 hours and 3 months, tin plating yielded the highest bond strengths to a high-noble alloy, but the value for the Alloy Primer groups was not significantly lower. There was no statistically significant difference between the 24-hour and 3-month values within the 4 treatment regimens. CONCLUSION: Treatment of amalgam or high-noble alloy with either tin plating or Alloy Primer before bonding with Panavia 21 resin cement yielded equivalent bond strengths to a base metal alloy. ED Primer was not an effective metal primer. There was no advantage to combining Alloy Primer and ED Primer.

Adhesives↗