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PubMed1998

Effect of ion exchange resins on the drug release from matrix tablets.

Ion exchange resins were incorporated into hydroxypropylmethylcellulose (HPMC) matrix tablets to modify the release of oppositely charged drugs. The drug release from HPMC tablets containing drug-resin complexes was significantly slower than from HPMC tablets containing drug without resin. A physical mixture of drug and ion exchange resin (cationic drug, propranolol HCl, with the cation exchange resin, Amberlite IRP 69, or the anionic drug, sodium diclofenac, with the anion exchange resin, cholestyramine (Duolite ATP-143)) resulted in almost the same drug release as tablets containing preformed drug-resin complexes. Upon contact with the dissolution medium, a gel layer formed rapidly around the solid tablet core and the complex between the drug and the resin formed in situ within the gelled regions. No effect of pH of the dissolution medium (0.1 N HCl or pH 7.4 phosphate buffer) or resin counterion was observed with the strong cation exchanger, Amberlite IRP 69. The resin was dissociated at both pH-values, allowing drug binding. With the weak cation exchange resin, Amberlite IRP 88, in situ complex formation and retardation was only observed in pH 7.4 buffer but not in 0.1 N HCl because of the non-ionization of the carboxyl groups. The drug release depended also on the amount and particle size of the resin particles and the type of carrier. The use of smaller resin particles eliminated the burst release seen with larger resin particles. Upon comparing different carrier materials, a rapid formation of the gel layer was important for the in situ complex formation. The drug release was in the order of Gelucire 54/02 (glyceryl palmitostearate) > polyethylene oxide 400K > HPMC K15M.

Adrenergic beta-Antagonists↗

PubMed2002

Comparison of the fracture resistance of six denture base acrylic resins.

Fracture strength of denture base resins is of great concern, and many approaches have been used to strengthen acrylic resin dentures. Fracture resistance of six commercially available acrylic resin denture base materials were compared, through impact and transverse strength tests. Three rapid heat-polymerised resins (QC 20, Meliodent and Trevalon), two high-impact strength resins (Trevalon Hi and Lucitone 199) and a strengthened injection-moulded acrylic resin (SR Ivocap plus) were included in the study. Twenty acrylic resin test specimens were fabricated from each resin. For impact strength test, ten notched specimens were tested in a Charpy-type impact tester. The other ten specimens were used for transverse strength tests, deflection and modulus of elasticity values were also determined, which were assessed with three-point bending tests using an Universal Testing Machine. Impact test values showed significant differences among acrylic resins (F= 4.817 p = 0.0). SR Ivocap resin showed the highest impact strength values, followed by Trevalon Hi and Lucitone 199. The transverse strength test values were not significant when six acrylic resins were compared (F= 1.705 p = 0.151). High-impact resins can be recommended to increase the impact strength of denture base. If the cause of fracture is mechanical or anatomical, strengthened acrylic resins and conventional acrylic resins have similar fracture resistance.

Acrylic Resins↗

PubMed1989

[Dimensional accuracy of microwave-cured denture base resin].

Recently, microwave-cured denture base resin was developed, and the resin solved the problem of internal porosity which had been generated by curing the conventional denture base resins with microwave irradiation. In this study, the dimensional accuracy of microwave-cured denture base resin was compared with that of other denture base resins, such as pour-type resin, heat-cured resin and heat-shock resin. From the experiment, the following results were obtained. 1. Dimensional accuracy of microwave-cured denture base resin was better than that of heat-cured resin and heat-shock resin, and was similar to that of pour-type resin. 2. Dimensional accuracy of microwave-cured denture base resin by slow cooling method and rapid cooling method was almost the same. Those findings suggest that microwave-cured denture base resin is valuable in clinic.

Denture Bases↗

PubMed1990

[Color differences between light-cured composite resin made shade guides and manufactured shade guides].

The purpose of this study was to investigate color differences between shade guides and light-cured composite resins. Resin specimens were made with resins and opaque resins of Silux Plus and Silux (3 M Co.) in a shade-guide metal mold. The resin specimens and the shade guides therefore were identical in shape and size. The sample resin specimens were compared with the shade guides provided with Silux Plus and Silux light-cured composite resins. Color measuring was performed with the Murakami Color Research Laboratory Fast Spectrophotometer C M S -500 and the Flexible Sensor F S -1. Specimens were placed on a plastic disc fixed to the top of the flexible sensor, and identical areas of their incisal, central, and cervical parts were measured. Conclusions. 1) The delta E*ab values between all shade guides and resin specimens showed color differences detectable to the naked eye. 2) Color differences between shade guides and resin specimens were great for the incisal colors (I, X L) and the deep and dark colors (D G, D Y, Y B, D G O, D Y O, Y B O, D D Y O). Color differences were relatively small, however, for the general colors (U, Y, G, U O, Y O, G O). 3) The L* values of shade guides ranged more widely than those of resin specimens. For many colors, L* values of the shade guides were lower than those of the resin specimens. 4) The a* values of shade guides and resin specimens were much more limited. The a* values of all colors showed minus values. The magnitude of a* values of shade guides were lower than those of resin specimens. 5) The b* values of shade guides were higher for some colors and lower for some colors than those of resin specimens.

Bisphenol A-Glycidyl Methacrylate↗

PubMed2001

Orthodontic bracket bonding with a plasma-arc light and resin-reinforced glass ionomer cement.

Developments in light-curing technology have led to the introduction of a plasma-arc light-curing unit that delivers high-intensity output for faster curing. The purposes of this study were to determine the shear bond strengths of light-cured resin-reinforced glass ionomer cement cured with a plasma-arc light-curing unit and to evaluate the durability of the resultant bond strength with thermal cycling. Comparisons were made between light-cured resin-reinforced glass ionomer cement and light-cured composite resin. Two light-curing units were used in this study: a plasma-arc light-curing unit and a conventional light-curing unit. The mean shear bond strengths of light-cured resin-reinforced glass ionomer cement with the plasma-arc and the conventional light-curing units were 20.3 MPa and 26.0 MPa, respectively. An analysis of variance showed no statistically significant differences between the plasma-arc and the conventional light-curing units. Light-cured resin-reinforced glass ionomer cement and light-cured composite resin demonstrated similar bond strengths and exhibited no statistical differences. There was no statistical difference in bond strength between the teeth that were thermal cycled and those that were not. Failure sites for the brackets bonded with light-cured resin-reinforced glass ionomer cement appeared to be predominantly at the bracket-adhesive interface. The SDs of light-cured composite resin were high for both light-curing units. Whereas the coefficients of variation for light-cured resin-reinforced glass ionomer cement ranged from 20% to 30%, those of light-cured composite resin ranged from 40% to 60%. The bond strength of light-cured resin-reinforced glass ionomer cement cured with either a conventional light-curing unit or a plasma-arc light-curing unit surpassed the clinically required threshold. The plasma-arc light-curing unit may be an advantageous alternative to the conventional light-curing unit for orthodontic bracket bonding with both light-cured resin-reinforced glass ionomer cement and light-cured composite resin.

Acrylic Resins↗

PubMed2005

Penetration of bonding resins into fibre-reinforced composite posts: a confocal microscopic study.

AIM: To compare the penetration of two different bonding resins applied for different contact times, on glass reinforced-reinforced composite root canal posts showing an interpenetrating polymer network (IPN) or cross-linked polymer matrix. The research hypothesis was that the bonding resins were equally able to penetrate into the IPN post whereas less penetration was evident into the cross-linked post. In addition, the prolonged contact time of the bonding resin on the surface of post was assumed to increase the resin penetration. METHODOLOGY: A total of 36 posts, comprising 18 IPN posts (everStick Post) and 18 cross-linked posts (C Post Millennium) were divided into 12 groups of three posts. All posts had a diameter of 1.2 mm. Both bonding resins (Scotchbond Multi Purpose Plus and Stick Resin) were labelled with Rhodamine B for determination of the resin penetration into the post. After contact times of 1, 30 and 300 s the bonding resins were light cured for 60 s. Penetration of bonding resins into three sections of each post was measured by confocal scanning light microscope. The influences of post and type of adhesive resin on resin diffusion into the polymer matrix of the post were assessed by nonparametric methods. RESULTS: For C Post Millennium and for 1 s contact time, no penetration of bonding resins into the polymer matrix of posts occurred in any section of any post. For the everStick Post, penetration was always noted after 300 s contact (mean 22.8 microm) and nearly always after 30 s contact (mean 3.5 microm), with very little difference between the two adhesives. The degree of penetration into everStick Posts was invariably greater after 300 s contact than after 30 s (P < 0.001). Both sets of results were highly significantly greater than the zero penetration recorded using C Post Millennium or 1 s contact time (P < 0.001). CONCLUSIONS: The ability of bonding resins to penetrate into everStick Post with IPN polymer matrix may give the opportunity to establish a good link between fibre-reinforced composite posts, luting cements and composite cores.

Composite Resins↗

PubMed1997

Comparative physico-mechanical characterization of new hybrid restorative materials with conventional glass-ionomer and resin composite restorative materials.

The recently developed hybrid restorative materials contain the essential components of conventional glass ionomers and light-cured resins. The objective of this study was to determine several physical and mechanical properties of eight such materials in comparison with two conventional glass ionomers, one micro-filled, and one ultrafine compact-filled resin composite. The two resin composites and two of the three polyacid-modified resin composites could be polished to a higher gloss than the conventional as well as the resin-modified glass ionomers. After abrasion, surface roughness increased for all materials, but not at the same extent, being the least for the conventional resin composites and one polyacid-modified resin composite, Dyract. In contrast to the later resin composites, of which the surface roughness is principally determined by the presence of protruding filler particles above the resin matrix, roughness of conventional and resin-modified glass ionomers results from both protruding filler particles and intruding porosities. The mean particle size of the hybrid restorative materials fell between the smaller mean particle size of the resin composites and the larger one of the conventional glass ionomers. The micro-hardness and Young's modulus values varied substantially among all eight hybrid restorative materials. For all the resin-modified glass-ionomer restorative materials, the Young's modulus reached a maximum value one month after mixing and remained relatively stable thereafter. The Young's modulus of the conventional and the polyacid-modified resin composites decreased slightly after one month. The conventional glass-ionomer materials undoubtedly set the slowest, since their Young's modulus took six months to reach its maximum. The flexural fatigue limit of the hybrid restorative materials is comparable with that of the micro-filled composite. From this investigation, it can be concluded that the physico-mechanical properties vary widely among the eight hybrid restorative materials, indicating that these materials probably have yet to achieve their optimum properties. Their mechanical strength is inadequate for use in stress-bearing areas, and their appearance keeps them from use where esthetics is a primary concern.

Acrylic Resins↗

PubMed1985

Contact allergy to phenol-formaldehyde resins.

Adverse reactions to phenol-formaldehyde resins include depigmentation, irritant dermatitis, chemical burns and allergic contact dermatitis. Allergic contact dermatitis from phenol-formaldehyde resin has mainly been ascribed to resins based on paratertiary-butyl phenol and formaldehyde, and such a resin is included in the ICDRG standard patch test series. When 1220 patients were patch tested with this resin as well as with 2 other phenol-formaldehyde resins, based on phenol and formaldehyde, 26 patients were positive to at least 1 resin. The figures for positive reactions to paratertiary-butyl phenol-formaldehyde resin and the 2 other resins were 0.8%, 1.0% and 3.0% (440 tested subjects), respectively. Therefore, a battery of phenol-formaldehyde resins should be used for screening purposes, since patch testing with the paratertiary-butyl phenol-formaldehyde resin is not sufficient to identify patients with contact allergy to phenol-formaldehyde resins. Several of the 26 patients were patch tested with the basic substances phenol, formaldehyde and paratertiary-butyl phenol, but only 1 positive reaction to formaldehyde was noted. The sensitizing capacity of 2-methylol phenol, 4-methylol phenol and 2,4,6-trimethylol phenol, all 3 compounds being possible ingredients of resins based on phenol and formaldehyde, was demonstrated; 5 of 14 resin positive patients reacted to at least 1 of these methylol phenols.

Chemical Phenomena↗

PubMed2006

Effect of temperature on unpolymerized composite resin film thickness.

STATEMENT OF PROBLEM: Room temperature (RT) composite resins are viscous, and this condition may affect the ability of the material to flow and adapt to preparation walls. PURPOSE: The purpose of this study was to compare the film thickness of a variety of commercial composite resins heated prior to light polymerization. The film thickness of these heated materials was also compared to those of flowable products at RT. MATERIAL AND METHODS: Five flowable and 7 conventional composite resins were used: 2 microfills, a nanofill hybrid, 2 submicron hybrids, a trimodal hybrid, and a packable. Composite resin (0.05 mL) was pressed between 2 Mylar-covered glass plates (15 kg) for 180 seconds, light polymerized, and the thickness measured using a micrometer. When comparing conventional composite resin heated to 54 degrees C or 60 degrees C, the RT value was control, while the RT flowable values were control when compared to heated composite resin. (n=5/group). Data were analyzed using 1- and 2-way analysis of variance and the Tukey-Kramer post hoc test (alpha=.05). Correlation of filler content to flow potential was evaluated. Scanning electron microscopic analysis of polymerized specimens was characterized by filler size and shape. RESULTS: Room temperature conventional composite resin values varied in film thickness. Not all preheated products reduced in thickness. Thickness of the nanofill did not reduce, and one of the submicron hybrids reduced the greatest. No correlation existed between composite resin classification, filler content or shape, and film thickness. No difference in thickness existed between composite resins preheated to 54 degrees C and 60 degrees C. Room temperature and preheated conventional composite resin provided film thickness greater than that of flowable materials. CONCLUSIONS: Preheating conventional composite resin yields lower film thickness for some products, but flow cannot be attributed to composite resin classification, filler content, or shape. Preheated composite resin thickness was greater than that of all flowables.

Acrylic Resins↗

PubMed2001

Repair of denture base resins with visible light-polymerized reline material: effect on tensile and shear bond strengths.

STATEMENT OF PROBLEM: Triad visible light-polymerized (VLP) reline resin has the potential to repair denture bases from other resin systems with the elimination of flasking/deflasking procedures. PURPOSE: This study measured the tensile and shear bond strengths of Triad VLP, PMMA, and glass-fiber-reinforced PMMA (GF-PMMA) acrylic resins before and after repair with Triad VLP reline material. MATERIAL AND METHODS: Fifty-six specimens were fabricated from Triad VLP, PMMA, and GF-PMMA denture base resins. Both Triad VLP reline material and autopolymerizing acrylic resins were used to repair identical laboratory fabricated resin joints. Twenty-eight rectangular specimens (in 4 different groups of 7 each) were prepared to study the shear bond strength of Triad reline material used to repair different denture base resin joints. RESULTS: Statistically significant differences (P< .0001) were found between the tensile strengths of specimens repaired with the Triad VLP reline resin used as a repair agent and those repaired with the autopolymerizing resin. The tensile strength of the Triad VLP denture base resin was found to be higher than that of both the PMMA and GF-PMMA acrylic resins. CONCLUSION: The low tensile and shear bond strengths found after the repair of PMMA and GF-PMMA acrylic resins with Triad VLP reline material were attributed to a lack of cohesion/adhesion between the Triad VLP reline material and the interfaces of the treated sites. The use of Triad VLP reline material to repair Triad VLP denture base resin produced the highest strengths.

Acrylic Resins↗

PubMed2005

Effects of polishing techniques on the surface roughness of acrylic denture base resins.

STATEMENT OF PROBLEM: Rough surfaces of denture bases promote adhesion of microorganisms and plaque formation. It is therefore important to know how different polishing systems affect surface roughness of denture base acrylic resins. PURPOSE: The objective of this study was to compare the effects of 4 chairside polishing kits and 2 conventional laboratory techniques used for polishing 3 different acrylic denture base resins. MATERIAL AND METHODS: Using contact profilometric measurement, the surface texture of 54 specimens (15x30x3 mm) per acrylic material (autopolymerized ProBase Cold, heat-polymerized ProBase Hot, and injection heat-polymerized SR Ivocap plus) was studied before and after cutting with a tungsten carbide bur, and during and after chairside polishing with 4 polishing kits (Exa Technique, Acrylic Polisher HP blue, AcryPoint, Becht Polishing Cream), and after conventional polishing with 2 polishing systems (Universal Polishing Paste for Resins and Metals, Lesk Polishing Liquid). There were 9 specimens for each acrylic resin material and polishing method combination. Conventional lathe polishing with polishing paste served as the control. Mean average surface roughness (Ra) values of each specimen group were analyzed using a 2-way analysis of variance, the Scheffé post-hoc test, and paired t test (alpha=.05) with the Bonferroni adjustment. After testing the polished acrylic resin surfaces were evaluated under a scanning electron microscope. RESULTS: The highest mean average surface roughness (Ra=2.86+/-0.8 microm to 3.99+/-1.31 microm) was measured for surfaces finished with a tungsten carbide bur. The lowest surface roughness values (Ra=0.02+/-0.01 microm) were determined for acrylic resin specimens polished with a lathe and polishing paste. The Ra values of resin specimens after polishing with chairside silicone polishing kits ranged from 0.05+/-0.0 microm to 0.35+/-0.05 microm. Mean average Ra values of specimens polished with a polishing cream alone (Ra=1.01+/-0.17 microm to 1.68+/-0.47 microm) were significantly higher (P<.05) than those obtained with other polishing systems tested, which was confirmed by scanning electron microscope images of acrylic resin surfaces. Significant differences in mean average surface roughness were found between autopolymerizing and injected heat-polymerizing resin specimens. In addition, scanning electron microscopy revealed increased porosity of autopolymerizing resin specimens. CONCLUSIONS: Conventional laboratory polishing was found to produce the smoothest surface of denture base acrylic resin. Chairside silicone polishing kits produced a significantly smoother surface of acrylic resin than specimens polished with a tungsten carbide bur. The presence of large pores was characteristic for the autopolymerizing resin material.

Acrylic Resins↗

PubMed2000

Resin shear bond strength to porcelain and a base metal alloy using two polymerization schemes.

STATEMENT OF PROBLEM: Fractures in ceramometal restorations can occur and need to be repaired because replacements are not an economic solution. PURPOSE: This study evaluated the shear bond strengths of 4 porcelain repair systems (Metabond C&B [ME], Silistor [SI], Clearfil Lustre [CL], and Scotchbond Multipurpose Plus [SQ]) to a base metal alloy and porcelain in relation with the polymerization shrinkage of a visible light-cured composite superstructure and compared with the ceramometal bond strength (Vita VMK 68). MATERIAL AND METHODS: Thirty-two samples were prepared for each bonding system: 16 for resin-metal bond strength test, and 16 for resin-porcelain bond strength test. For each group, bonding agent was applied to 8 substructures and the resin superstructure was polymerized onto the bonding agent; and for the remaining 8 specimens, prepolymerized resin superstructures were bonded with bonding agent. All specimens were subjected to 500 cycles between 5 degrees C and 55 degrees C with 20 seconds dwell time. Tests were performed in a mechanical testing machine with a 0.5 mm/min crosshead speed. RESULTS: All materials showed an increase in shear bond strength when prepolymerized resin superstructures were used. However, the effect of polymerization shrinkage of resin superstructure was statistically significant only for CL group (P <. 05). The highest metal-resin bond was obtained from ME group with prepolymerized resin superstructures (35.27 +/- 2.40 MPa), and the lowest value was obtained for the SI group in which resin superstructures were polymerized in situ (8.71 +/- 1.03 MPa). The highest porcelain-resin bond was obtained from SC group with prepolymerized resin superstructures (20.71 +/- 1.13 MPa) and the lowest was obtained from SI group (9.99 +/- 1.52 MPa). CONCLUSION: Higher bond strength values were obtained with prepolymerized resin superstructures compared to in situ polymerized superstructures. Metabond C&B provided the best results for both prepolymerized and in situ polymerized resin superstructure preparation techniques at the failures where metal was exposed. The best results in situations in which the fracture is limited into porcelain were obtained with the use of Scotchbond Multipurpose Plus material. However, a variety of in vivo and in vitro tests are required before a final judgment is made.

Analysis of Variance↗

PubMed1992

A study of bond strength between light- and self-cured orthodontic resin.

Light-cured orthodontic composite resin has been widely advertised recently for use in bonding. However, the curability of light-cured resin when light waves are diffused through metal, ceramic, or resin brackets is doubtful and questionable. This study evaluated the effectiveness of a visible light source in curing the resin under a solid metal bracket, compared the tensile bond strength at different exposures, and analyzed the broken interface distribution between light-cured resin with various light exposure times and self-cured resin. The bond strength results revealed that the difference between light-cured resin (Transbond) with 60, 40, and 20 seconds of light exposure, respectively, and self-cured resin (Concise) was 1.05, 0.92, 0.61, and 0.71 kg/mm2, respectively. The bond strength of Transbond with 60 and 40 seconds of light exposure was greater than both the bond strength of Transbond with 20 seconds of light exposure and the strength of the self-cured resin of Concise, with statistical significance (p less than 0.01). There were also no statistical differences between Transbond with 60 and 40 seconds of light exposure or Transbond with 20 seconds of light exposure and Concise. The bond failure interfaces were located between the bracket and the resin, within the resin itself, or between the resin and the enamel. Tooth fragmentation was rarely found. There were no statistical differences (p greater than 0.05) among broken interfaces. This indicates that visible light is powerful in curing the visible light-activated composite resin under solid metal brackets.(ABSTRACT TRUNCATED AT 250 WORDS)

Acrylic Resins↗

PubMed2001

Treatment of chromium plating process effluents with ion exchange resins.

The surface treatment industry deals with various heavy metals, including the elements Cr, Zn, Ni, Cd, and Cu. Conventional treatments of effluents generate class I solid residue. The aim of this investigation was to study the viability of ion exchange as an alternative process for treatment of rinse water and to determine the efficacy of two ion exchange systems, System 1: "strong" cationic resin-"strong" anionic resin and System 2: "strong" cationic resin-"weak" anionic resin. Commercial resins and solutions taken from rinse tanks of chromium plating companies were used in this investigation. A two-column system, one for the cationic resin and another for the anionic resin, both with 150 ml capacity was mounted. The solution was percolated at a rate of 10 ml/min. The following solutions were used for regeneration of the resins: 2% H2SO4 for the cationic and 4% NaOH for the anionic. The percolated solutions revealed chromium contents of less than 0.25 mg/l, independent of the system used. The "strong" cationic resin-"weak" anionic resin gave excellent regeneration results. The "strong" cationic-"strong" anionic resin presented problems during regeneration, and did not release the retained ions after percolation of 2000 ml of 4% NaOH solution. It is concluded that for this type of treatment, the system composed of "strong" cationic resin and "weak" anionic resin is more appropriate.

Cations↗

PubMed1996

Impact of the resin blood culture medium on the treatment of critically ill patients.

OBJECTIVE: To assess the relevance, both clinical and bacteriologic, of the use of resin-containing blood culture media in blood cultures taken from critically ill patients receiving antibiotics. DESIGN: A prospective, open clinical trial. SETTING: The mixed medical surgical intensive care unit (ICU) of a 550-bed urban hospital. PATIENTS: All ICU patients admitted during a 3-month period (n = 49) with suspected sepsis requiring blood cultures as part of their laboratory investigations. INTERVENTIONS: The use of an aerobic resin-containing blood culture medium, in addition to the regular aerobic and anaerobic media for all blood cultures taken. MEASUREMENTS AND MAIN RESULTS: Each blood culture result was classified as to its clinical significance. Changes in patient management were recorded. Culture sets in which the resin-containing bottle provided the information central to the change in patient management were identified. Bacteriologically, the results from the resin-containing medium were compared with the results from the aerobic and anaerobic media. Of 266 blood culture sets, 103 (39%) were positive, growing 278 bacterial and fungal isolates. Clinically, the resin-containing medium alone provided relevant data leading to changes in patient management on three occasions. On two of these occasions, cultures from the regular media provided the same data within 72 hrs. Bacteriologically, 77 (29%) aerobic bottles, 55 (21%) anaerobic bottles, and 89 (33%) resin-containing bottles were positive (statistical comparison of percentages: aerobic vs. resin-containing bottles, nonsignificant; aerobic vs anaerobic bottles, p < .046; anaerobic vs. resin-containing bottles, p < .0027). A similar proportion of pathogens was isolated from the resin-containing bottles only (9%) and aerobic bottles only (6%). A higher proportion of contaminants was isolated from the resin-containing bottles only than the aerobic bottles only in the various sets (17% vs. 7%, p < .046). The resin-containing bottle showed a trend toward increased detection of Staphylococcus aureus and Pseudomonas aeruginosa bacteremia. CONCLUSIONS: The resin-containing medium offers little clinical benefit to the majority of ICU patients. Bacteriologically, it seems to have a similar overall sensitivity as the regular aerobic medium (with the possible exception of a higher sensitivity for the isolation of S. aureus and P. aeruginosa), but a lower specificity. The wide-spread use of the resin-containing bottle cannot be recommended.

Anti-Bacterial Agents↗

PubMed1998

Oxidation of resin acids in colophony (rosin) and its implications for patch testing.

Commercial preparations of colophony (rosin) used for patch testing are made from unmodified rosin in pet. and may be stored for some considerable time before being used. This would be satisfactory if the composition and dermatological activity of the preparations were both reproducible and stable, but investigations by the authors have shown that the resin acids undergo progressive and substantial oxidation and that the dermatological activity of the preparations increases significantly with time. This may be a cause of inconsistent patch test results unless the composition can be stabilized. Gas liquid chromatography (GLC) analysis of a raw rosin sample and its commercial patch test preparation has shown that they both contained the same resin acids, but the concentration of the abietic type resin acids was found to be lower in the patch test preparations. The degradation of resin acids is due to their atmospheric oxidation, which may occur during the preparation and storage of the commercial rosin patch test preparation. The susceptibility of individual resin acids to atmospheric oxidation was demonstrated by analysing a sample of raw Portuguese gum rosin, which was then left exposed to air and light. Most of the resin acids were found to undergo oxidation at a rate which gradually diminished. More importantly, it is presumed that the concentration of oxidized resin acids increased correspondingly, and these have been shown to be more dermatologically active than the unoxidised resin acids. The rate of decrease of resin acid concentration was found to be in the following order: neoabietic>levopimaric and palustric>abietic>dehydroabetic acid. The pimaric type resin acids were found to be relatively inert to atmospheric oxidation when compared with the abietic type resin acids. Patch testing with the resulting partly oxidized Portuguese rosin produced positive reactions at a 35% higher frequency than the raw Portuguese rosin. The study demonstrates that the allergic potential of unmodified rosin may increase with exposure to air and light. It is therefore recommended that rosin preparations are analysed routinely as part of a quality control programme, which will enable better validation and comparison of patch test results from different dermatological centres. Since the oxidized resin acids are the main allergens in unmodified rosin, it is important that the concentration of the oxidized resin acids is kept high as well as constant in commercial patch test preparations.

Allergens↗

PubMed2002

Effect of cyclical lateral forces on microleakage in cervical resin composite restorations.

OBJECTIVE: The aim of this study was to assess the effect on microleakage of cyclic lateral fatigue forces in different types of cervical resin composite restorations. METHOD AND MATERIALS: V-notch cavities were prepared at the cementoenamel junction in 60 extracted human premolars and restored with a bonding system along with one of the following resin composites: hybrid resin composite, microfilled resin composite, and flowable resin composite (20 each). Ten specimens from each group of 20 were subjected to 8,400 cycles of lateral fatigue forces (44 N) at the occlusal half of the clinical crown in a machine specifically developed for this purpose. The other 10 specimens of each group served as controls, representing the microleakage that occurred without lateral fatigue forces. All specimens were stained with a 50% silver nitrate solution and sectioned sagittally. A scoring system of 0 to 6 was used to record the amount of die penetration along the restoration-tooth interface. RESULTS: There was leakage in both the fatigued specimens and the nonfatigued control specimens. There were significant differences in the mean values of microleakage for the restorative materials studied. In the nonfatigued groups, hybrid resin specimens exhibited significantly more microleakage at the dentin-resin interface than did microfilled or flowable resin specimens. In the fatigued groups, hybrid resin specimens exhibited significantly more leakage at the dentin-resin interface than did microfilled resin specimens. CONCLUSION: The least elastic resin composite tested, the hybrid material, generally showed the most leakage. This suggests that the elasticity of these resin composite restorative materials may be a factor in the amount of microleakage in cervical restorations.

Barium Compounds↗

PubMed1990

[Physical properties of light-cured opaque resin. (1) Influence of monomer composition].

Light-cured opaque resins with excellent physical properties were prepared using five types of monomer liquid and titanium dioxide as the powder. The five opaque resin monomer liquid had the following monomer compositions. Methyl methacrylate (MMA)/di(methacryloxyethyl) trimethylhexamethylene diurethane (UDMA) = 70/30 (M-U), MMA/neopenthylglycol dimethacrylate (NPG)/UDMA = 45/45/10 (M-N-U), UDMA/MMA = 70/30 (U-M), 2,2-bis (4-methacryloxypolyethoxy phenyl) propane (2.6 E)/2,2-bis [4-(3-methacryloxy-2-hydroxy propoxy) phenyl] propane (Bis-GMA)/triethyleneglycol dimethacrylate (3 G) = 60/35/5(2.6-B-3) and 3 G/UDMA = 70/30 (3-U) by weight. The bond strength, photo-curability and handling properties of the opaque resin were improved. Three MMA-based opaque resins showed nearly the same values in Knoop hardness number, diametral tensile strength and shear bond strength. The depth of cure increased with the decrease in MMA content of monomer composition, while the amount of residual monomer decreased. The 2.6-B-3 opaque resin had nearly the same properties in depth of cure and Knoop hardness number as the 3-U opaque resin. However, the 2.6-B-3 and 3-U opaque resins had a diametral tensile strength more than twice as high as that of the U-M opaque resin. The bond strength of three MMA-based opaque resins showed 0MPa after 5,000 thermocycles, while the 2.6-B-3 opaque resin, about 16 MPa, and the 3-U opaque resin, about 25 MPa. Therefore, the bond strength of the opaque resin was influenced by monomer composition. 3G-UDMA opaque resin showed excellent physical properties and may be clinically acceptable to bond fixed prosthodontic composite.

Bisphenol A-Glycidyl Methacrylate↗