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Flexural properties and impact strength of denture base polymer reinforced with woven glass fibers.

OBJECTIVES: The present investigation was undertaken to determine the reinforcing effect of woven glass fibers on deflection, flexural strength, flexural modulus and impact strength of acrylic denture base polymer. METHODS: Three silanized or unsilanized woven glass fibers were used. Specimens were made by heating the denture cure resin dough containing glass fibers, which were sheathed in the dough. Specimens with four different thicknesses and of five different types were made, incorporating the glass fiber. Three-point flexural test and flywheel type impact test were employed to determine the flexural properties and impact strength. RESULTS: When specimens contained unsilanized glass fiber, the flexural strength in specimens of 1 and 2 mm thickness and the impact strength in specimens of 2 mm thickness were higher than those of specimens without glass fiber (p < 0.01). On the contrary, the flexural strength and deflection in specimens reinforced with silanized glass fiber of 1 mm thickness were significantly higher (p < 0.01, p < 0.05) than those of unreinforced specimens. Further, the impact strength in specimens reinforced with silanized glass fiber of 2 mm thickness was significantly higher (p < 0.01) than that of unreinforced specimens. Statistically significant differences were found in the flexural strength (p < 0.05) and in the impact strength (p < 0.01) when specimens of 4 mm thickness were reinforced with two or three unsilanized glass fibers. SIGNIFICANCE: The reinforcement with glass fiber was effective in thin specimens, and the reinforcing effect increased with the increase of the number of glass fibers in the case of thick specimens.

Acrylic Resins↗

Effect of polyethylene fiber reinforcement on the strength of denture base resins polymerized by microwave energy.

This study investigated the effect of addition of polyethylene fibers on the transverse strength, deflection, and elastic modulus of two denture base acrylic resins polymerized by microwave irradiation. Specimens of each resin, Lucitone 199 and Acron MC, were fabricated with 0.0%, 0.5%, 1.5%, and 3.0% fiber loading. Specimens were tested with use of a three-point flexure apparatus with an Instron universal testing machine after storage in water for 10 days at 37 degrees C. The results showed that polyethylene fibers significantly decreased the transverse strength of Acron MC resin and slightly increased the transverse strength of Lucitone 199 resin at a loading of 0.5% by weight. Fiber loading did not significantly affect the deflection and the elastic modulus of either material.

Acrylic Resins↗

Light-curing reinforcement for denture base resin using a glass fiber cloth pre-impregnated with various urethane oligomers.

The purpose of this study was to investigate the flexural properties of denture base resin reinforced using glass fiber cloth and a urethane oligomer. The five types of oligomer used in this study were S5, S9, S3, U4, and U6, which have varying functional groups and viscosities. The flexural properties of S9 with glass fiber cloth could not be measured because S9 is elastic. In the heat-cured resin reinforced with S9, the reinforcement peeled away from the resin. In the self- and light-cured resins reinforced with S9, the flexural properties increased significantly. When reinforced with the other four oligomers (S5, S3, U4, and U6), the flexural strength and flexural modulus of the self-, heat-, and light-cured resins increased significantly (p<0.01).

Acrylic Resins↗

Bonding properties of heat-polymerized denture base resin to Ti-6Al-7Nb alloy.

The purpose of this study was to evaluate the shear bonding strength and leakage of heat-polymerized denture base resin to titanium-aluminum-niobium (Ti-6Al-7Nb) and cobalt-chromium (Co-Cr) castings using four adhesive systems; three adhesive primers (Metal Primer II, Metal Link, MR. Bond) and one heat-polymerized adhesive resin containing 4-META (Metadent). The resin tab was heat-polymerized directly with or without the primer. Shear bonding strengths and dye penetration distances were determined before and after 10,000 times of thermocycling. The results were analyzed with three-way ANOVA and Tukey's comparison (p<0.05). Thermocycling significantly decreased bonding strength and promoted dye penetration. However, with the application of adhesive systems, post-thermocycling bond strength was significantly improved and dye penetration was inhibited. The bonding strength of Ti-6Al-7Nb was significantly smaller than that of Co-Cr, but the difference was marginal. These results suggested that the examined adhesive systems significantly improved the bonding efficiency of heat-polymerized resin to Ti-6Al-7Nb and Co-Cr alloys.

Acrylic Resins↗

Reinforcement of denture base resin with glass fillers.

PURPOSE: This study evaluated the effect of short glass fibers on the transverse strength of a heat-polymerized acrylic resin denture base material. MATERIALS AND METHODS: Four groups of specimens (n = 10) were fabricated according to the ISO standard for the transverse strength test. E-glass fibers were triturated to produce short fibers of different lengths. Specimens for Group 1 (control) were made of unfilled polymethylmethacrylate (PMMA). For group 2, the PMMA powder was modified with 0.1 g of dry glass fibers. For group 3, the PMMA powder was modified with 0.1 g of silanized glass fibers. For group 4, the PMMA powder was modified with 0.2 g of silanized glass fibers. A three-point loading test was used to determine the transverse strength of the tested specimens. The fracture surface of each specimen was evaluated using SEM. RESULTS: The addition of untreated glass fibers increased the transverse strength by 11% but produced some porosity in the polymeric matrix. The addition of silane-treated glass fibers increased the transverse strength of PMMA by 28% for group 3 and by 26% for group 4, and produced a dense structure for the polymer-fiber composite. CONCLUSION: The transverse strength of PMMA can be slightly increased by the addition of short glass fibers.

Analysis of Variance↗

Repair of acrylic resin denture base reinforced with glass fiber.

STATEMENT OF PROBLEM: The ultimate goal of any denture repair is to restore the original strength of the denture and to avoid further fracture. PURPOSE: This study investigated the strength and deflection of repaired acrylic resin joints reinforced with various glass fiber concentrations. MATERIAL AND METHODS: Transverse strength, maximum deflection, and modulus of elasticity of glass fiber-reinforced polymethyl methacrylate acrylic resin were studied with a 3-point load test on 54 intact specimens. Six concentrations of type B glass fiber specimens were prepared (n = 9 per each fiber group). Fractured joint margins were rounded, a 2-mm gap was placed between them, and then they were repaired with autopolymerizing acrylic resin and retested. RESULTS: Transverse strength, maximum deflection, and the stiffness of all joints were significantly lower after the repair. Among the groups tested, the units treated with 1% glass fiber displayed the highest transverse strength before and after repair. Modulus of elasticity of the repaired 1% fiber concentration units was enhanced by approximately 25% over those repaired but untreated with glass fiber (0% fiber).

Analysis of Variance↗

Relaxation modulus of denture base resin reinforced with woven glass fibers.

This study examined the reinforcing effect of woven glass fibers on the relaxation modulus by three-point loading of denture base resin. Three sandwich-type flexure test specimens polymerized by heating were used, all 3 mm thick: glass fibers in compression (U type); glass fibers in the center (C type); and glass fibers in tension (L type). Unreinforced specimens (ACR) were produced as a control. The relaxation modulus after 8 sec from the start of stress (Er(8)) was calculated from stress relaxation curves. In the glassy state, the Er(8)s of the U and L types were greater than those of the ACR and C types. In the rubbery state (plateau region), the Er(8)s of the U and L types were greater than those of the ACR and C types. The woven glass fibers added to the U and L type specimens increased the relaxation modulus of PMMA near the oral temperature; moreover, they inhibited stress relaxation when the temperature increased.

Algorithms↗

Measurement of residual monomer in denture base material: studies on variations in methodology using gas-liquid chromatography.

It is known that high levels of residual monomer have a deleterious effect on the properties of denture base polymers and may cause irritation or hypersensitivity of the oral tissues. In the present study variations in determination methodology and their influence on residual monomer levels are evaluated. The results demonstrate that filtration of the sample, sealed storage and incorporation of an appropriate volume of internal standard enhanced the accuracy of the technique.

Chromatography, Gas↗

Effect of processing variables (different compression packing processes and investment material types) and time on the dimensional accuracy of polymethyl methacrylate denture bases.

In this study we determined the effect of different compression packing processes, investment materials (a hemihydrate and dental stone) and time on the dimensional accuracy of polymethyl metacrylate denture bases. Square stainless steel plates (15 mm x 15 mm x 5 mm) were prepared to make an acrylic resin specimen. The linear dimensional changes of acrylic resin were determined by measuring the distances of fix points. Measurements were made at 24 hours, 48 hours, 12 days and 30 days after setting with a digital compass. Dimensional changes of test specimens that were obtained with three different flasks and two press techniques were compared by univariate analysis. Measurements of the linear dimensions of specimens cured by different compression packing techniques suggested that differences existed. The time interval differences were not significant. According to the results; flask and investment material types affect the dimensional accuracy of test specimens (p < 0.05). The least dimensional change observed in the specimens was obtained with Type 1 flask-dental stone-manual press combinations.

Acrylic Resins↗

The effect of the addition of different fibres on the transverse and impact strength of acrylic resin denture base material.

The aim of the present study was to investigate the effect of the addition of different types of fibres on the transverse and impact strength of acrylic resin denture base material. The addition of glass fibres (strand) and polyethylene fibres produced a non significant increase in the modulus of elasticity, compared with the control of conventional heat-cured acrylic resin. The addition of glass fibres (woven and strand), polyethylene and carbon fibres to acrylic resin produced a non significant increase in the modulus of rupture. The addition of carbon, glass (strand) and polyethylene fibres produced a significant increase in the impact strength. Within the limitations of this study the addition of silk fibres did not produce an improvement in the mechanical properties.

Acrylic Resins↗