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At least 469 records · Page 26Linked to original sources
PubMed2006

Effect of surface coating an acrylic intraocular lens with poly(2-methacryloyloxyethyl phosphorylcholine) polymer on lens epithelial cell line behavior.

PURPOSE: To evaluate the effect of surface coating of an acrylic intraocular lens (IOL) with poly(2-methacryloyloxyethyl phosphorylcholine) (MPC) on the behavior of the lens epithelial cell (LEC) line, alpha-TN4. SETTING: Department of Ophthalmology, Nihon University School of Medicine, Tokyo, Japan. METHODS: A hydrophobic soft acrylic IOL (AF-1, Hoya) was coated with MPC polymer. A noncoated IOL served as control. An IOL from each group was placed on the membrane of collagen I or IV of the cell culture dish. The alpha-TN4 cells were seeded in the insert. Cell behaviors (ie, cell proliferation and spreading) on IOLs and membranes were observed. Cell migration beneath the IOL optic portion was assayed using a computer software program (POCOman system) for posterior capsule opacification (PCO). Type I or IV collagen is the major matrix component of PCO or native lens capsule. RESULTS: Cell proliferation was more marked on the noncoated IOL than on the coated IOL. Type IV collagen accelerated proliferation more than type I collagen. Cell migration to the area beneath the IOL optic was more prominent in the group with the type I collagen membrane and noncoated IOL than in other groups. CONCLUSION: Coating an acrylic IOL surface with MPC polymer suppressed adhesion and proliferation of LECs, suggesting it improves IOL biocompatibility.

Acrylic Resins↗
PubMed2006

Ocular aberrations after cataract surgery with hydrophobic and hydrophilic acrylic intraocular lenses: comparative study.

PURPOSE: To compare tilt and some higher-order aberrations (HOAs) in patients who had cataract surgery and implantation of 2 types of acrylic intraocular lens (IOL), the hydrophobic MA60AC (Alcon) or the hydrophilic XLSTABI (Ioltech). SETTING: Fondation Ophtalmologique Adolphe de Rothschild, Department of Pr Hoang-Xuan, Paris, France. METHODS: Sixty eyes were included in this study. Eyes in group 1 (n = 30) received the acrylic hydrophobic MA60AC IOL, and eyes in group 2 (n = 30) received the acrylic hydrophilic XLSTABI IOL. Optical aberrations were measured with Nidek OPD-Scan at least 1 month after cataract surgery for a 6.0 mm pupil diameter using a 6th-order Zernike polynomials decomposition. RESULTS: In group 1, the mean root-mean-square (RMS) coefficient for the total higher aberration was 0.86 microm +/- 0.38 (SD). The mean RMS of the tilt, coma, trefoil, tetrafoil, spherical aberration, and secondary astigmatism was 0.81 +/- 0.45 microm, 0.38 +/- 0.30 microm, 0.55 +/- 0.18 microm, 0.13 +/- 0.23 microm, 0.30 +/- 0.13 microm, and 0.17 +/- 0.21 microm, respectively. In group 2, the mean RMS coefficient for the total higher aberration was 0.72 +/- 0.31 microm. The mean RMS of the tilt, coma, trefoil, tetrafoil, spherical aberration, and secondary astigmatism was 0.55 +/- 0.30 microm, 0.24 +/- 0.19 microm, 0.50 +/- 0.23 microm, 0.07 +/- 0.22 microm, 0.32 +/- 0.13 microm, and 0.14 +/- 0.14 microm, respectively. There was a statistical difference in aberrations between the 2 groups for the tilt and the coma aberrations (P<.05). There were more aberrations in the MA60AC IOL group. CONCLUSIONS: The design of the IOL influenced ocular aberrations after cataract surgery. There were more tilt and coma aberrations in the MA60AC IOL group.

Acrylic Resins↗
PubMed2007

Effect of ophthalmic solution components on acrylic intraocular lenses.

PURPOSE: To investigate the effect of ophthalmic solution components on the surface of acrylic intraocular lenses (IOLs). SETTING: Department of Opthalmology, Showa University School of Medicine. METHODS: Measurement of the contact angles of ophthalmic solutions on 3 acrylic IOLs was performed. The solutions were diclofenac sodium (Diclod), bromfenac sodium (Bronuck), betamethasone phosphate (Rinderon), dibekacin sulfate (Panimycin), polysorbate 80 (Tween 20), benzalkonium chloride, chlorobutanol, methylparahydroxybenzoate, and propylparahydroxybenzoate. The IOLs were incubated at 35 degrees C for 2 weeks in undiluted ophthalmic solutions and in 1:10 dilutions of ophthalmic solution components. The IOLs were sectioned and observed by scanning electron microscopy. RESULTS: The contact angle of Diclod and Bronuck solutions was the smallest. The contact angle of Rinderon and Panimycin was similar to that of distilled water. Scanning electron microscopy examination of IOLs incubated in ophthalmic solution components showed intralenticular changes. The IOLs immersed in ophthalmic solutions did not show any change, even after extended incubation. CONCLUSION: The chemical components of ophthalmic solutions, such as surfactants and solvents, permeate acrylic IOLs, suggesting the potential for long-term adverse effects of eyedrops in pseudophakic eyes.

Acrylic Resins↗
PubMed2004

Repair strength of autopolymerizing, microwave, and conventional heat-polymerized acrylic resins.

STATEMENT OF PROBLEM: Acrylic resin dentures are susceptible to fracture after clinical use. The repair procedure should be time saving, strong, and should not affect dimensional accuracy. PURPOSE: This study evaluated the transverse repair strength of a conventional heat-polymerized (Lucitone 199, "L") and a microwave-polymerized (Acron MC, "A") acrylic resin that were repaired with these same resins and with an autopolymerizing acrylic resin (Acron MC/R, "AR"). MATERIAL AND METHODS: Twenty-four rectangular specimens (65.0 x 10.0 x 3.3 mm) of L or A and 6 of AR were manufactured according to ISO/FDI 1567 and stored in distilled water at 37 degrees C for 7 days. Eighteen specimens of L or A were selected randomly. Six specimens of each material remained intact (control), each 6 were sectioned in the middle to create a 10-mm gap and repaired with the materials L, A, or AR. After an additional 7 days of storage at 37 degrees C, the transverse strength (MPa) of the repaired and intact specimens was measured using a 3-point bending test. A 2-way ANOVA and a Tukey HSD test were performed to identify significant differences (alpha=.05). The nature of the failure was noted as adhesive, cohesive, or mixed. RESULTS: The intact and repaired specimens showed similar transverse strength values (MPa), except for A-intact (80.6 +/- 2.9), which was significantly stronger (P<.05) than the other materials tested as well as the repaired groups (P<.05). No differences were detected among the repaired groups. Repaired specimens exhibited 3 types of failures: adhesive (interface), cohesive (only in the repair material), and mixed (interface and repair material), with incidences of 2.8, 25, and 72.2%, respectively. CONCLUSION: The autopolymerizing resin exhibited a repair strength similar to those found for the conventional heat- and microwave-polymerized materials.

Acrylic Resins↗
PubMed2005

Water absorption characteristics of two types of acrylic resin obturators.

STATEMENT OF PROBLEM: The mechanisms of water accumulation in the inner space of a closed hollow obturator are not understood, and it is not known whether the porosity of acrylic resin is involved in these mechanisms. PURPOSE: The purpose of this study was to evaluate water absorption by solid and closed hollow obturators and to determine the mechanisms of water accumulation in the inner space of the closed hollow obturator. MATERIAL AND METHODS: Twenty solid and 20 closed hollow spherical specimens (30 mm in diameter) were fabricated from heat-polymerized acrylic resin (Acron Clear). Closed hollow specimens consisted of 2 hemispheres (30 mm in diameter, 1.5 mm in thickness) joined with autopolymerizing resin (Unifast II). Ten solid and 10 closed hollow specimens were immersed in distilled water at 37 degrees C, while the other specimens were stored in an atmosphere of 100% relative humidity at 37 degrees C. Each specimen was weighed every 24 hours for 180 days, and weight changes between each group were compared by 2-way ANOVA and the Tukey HSD test. Split-plot design ANOVA was used to compare the course of the weight change over 180 days (alpha=.05). RESULTS: The weight of the closed hollow specimens increased immediately and became saturated by day 30, with an increase of 1.44% from the initial weight. Water accumulation was not observed inside the closed hollow specimen during the 180-day storage period. The weight of solid specimens increased more slowly than that of closed hollow specimens; by day 180 the weight of the latter had increased by 1.16%. However, no significant difference in changes in mean mass of the same type of specimen was observed between the 2 storage conditions. CONCLUSION: These results suggest that water accumulation inside a closed hollow obturator is unrelated to the water absorption properties of the acrylic resin.

Absorption↗
PubMed2001

Acrylic intraocular lens placement in conjunction with pars plana vitrectomy.

PURPOSE: To report the results of placing a foldable acrylic intraocular lens through a clear cornea incision in eyes undergoing pars plana vitrectomy. METHODS: This interventional case series is a retrospective report of 15 eyes of 15 consecutive patients undergoing foldable (acrylic) intraocular lens insertion in conjunction with pars plana vitrectomy in a single academic institution. Outcome measures included visual acuity and complications. RESULTS: The intraocular lens was successfully implanted and retained in position in all 15 cases. The intraocular lens did not pose difficulty in examining the fundus or cause any vitreoretinal complications. With mean follow-up of 4.5 months (range, 1--10 months), final median postoperative visual acuity range was 20/200 (range, 20/40--2/200) and consistent with the level of vitreoretinal disease. CONCLUSION: Acrylic intraocular lenses may be safely implanted in conjunction with pars plana vitrectomy in selected cases.

Acrylates↗
PubMed1996

Biochemical comparison of plaque fluid on tooth and acrylic surfaces during a sucrose challenge.

Previous studies have investigated variations in dental plaque fluid composition within a single mouth after a sucrose exposure. The purpose of this study was to determine a potential source of calcium and phosphorus in plaque by comparing the pH, calcium and phosphorus concentrations in plaque fluid obtained from an acrylic appliance with samples taken from supragingival tooth surfaces within the same individual after a sucrose challenge. Separate plaque samples from 14 individuals were collected from an acrylic appliance or tooth surfaces within same individual before and 15 min after a 20% sucrose rinse. Each plaque sample was centrifuged and nanolitre samples of plaque fluid were analysed for pH with a pH microelectrode, for total calcium concentration by atomic absorption in a graphite furnace, and for phosphorus concentration by spectrophotometry. There was an increase in the calcium and phosphorus concentration in the plaque after the sucrose challenge and a significant increase in calcium and phosphorus concentrations in the plaque taken from the teeth compared to the acrylic surfaces. The results indicate that the increased total calcium and phosphorus in plaque during a sucrose challenge is probably derived from the demineralization of enamel or extracellular demineralized components.

Acrylic Resins↗
PubMedDate not supplied

Clinical and experimental observation of glistening in acrylic intraocular lenses.

PURPOSE: To determine whether or not glistening particles in implanted acrylic intraocular lenses (IOL) increase with the passage of time. METHODS: Prospective clinical study: Glistenings were evaluated in 31 patients (49 eyes) with implanted acrylic IOL, the emphasis being on when glistening first became evident and subsequent changes in the number of glistening particles. EXPERIMENT: IOLs were monitored for any changes that occurred with the passage of time as they were immersed first in a 50 degrees C saline solution and then in another saline solution with a temperature of 35 degrees C. RESULTS: Prospective clinical study: Glistening phenomenon was observed in 28 IOLs (57%) 2 to 16 months after implantation (mean = 6.6 months). Glistenings reached their peak in number within a few months of formation in all cases, showing no further increase thereafter. EXPERIMENT: Glistening particles first appeared on the 10th day of the experiment in sizes ranging from 3 to 10 microm in diameter. They remained at the same level for the next 60 days without showing any increase. CONCLUSIONS: Glistening formation in acrylic IOLs was found to stabilize within a few months after appearance. The method of our experiment proved reliable in producing, in a relatively short period of time, glistening similar to that found in patients.

Acrylic Resins↗
PubMed2003

Reducing the negative effects of chemical polishing in acrylic resins by use of an additional cycle of polymerization.

STATEMENT OF PROBLEM: The chemical polishing of dentures and orthodontic appliances is an efficient and time-saving technique. However, the process may adversely affect the physical properties of resin. PURPOSE: This study evaluated the effect of an additional polymerization cycle in a microwave or water bath on the physical properties of an autopolymerized acrylic resin submitted to chemical polishing. MATERIAL AND METHODS: Control groups comprised acrylic resin specimens submitted to mechanical (group 1) and chemical (group 2) polishing. Experimental groups comprised chemically polished specimens submitted to an additional cycle of polymerization in a microwave at 450 W for 3 minutes (group 3) or in a hot water bath at 65 degrees C for 1 hour (group 4). For the residual monomer test, 10 standardized half-disc specimens (30 x 3 mm) were fabricated for each of the test groups, and daily ultraviolet spectrophotometric (206 nm) analyses were assessed for 13 days (microg/cm(2)). For transverse strength and internal Knoop hardness (KH) tests, 10 (65 x 10 x 2.5 mm) and 5 (32 x 10 x 2.5 mm) specimens were fabricated for each test group, respectively. Internal Knoop hardness (kg/mm(2)) was assessed at depths of 100, 700, and 1500 microm. Transverse strength (MPa) was measured with a 3-point bending test in a universal testing machine with a 10-kg load cell at a crosshead speed of 5 mm/min. The data were analyzed with 1-way analysis of variance, and the means were compared with Student's t test and Tukey-Kramer intervals (P<.05). RESULTS: At the end of the first day of the test, all groups showed significantly different residual monomer levels (P<.05). The groups in order of decreasing residual monomer were: group 2 (1315.7 +/- 225.5 microg/cm(2)), group 3 (848.2 +/- 150.4 microg/cm(2)), group 4 (295.1 +/- 81.6 microg/cm(2)), and group 1 (136.6 +/- 45.5 microg/cm(2)). After 13 days of water storage, the lowest residual monomer levels were recorded for group 1 (4.6 +/- 1.6 microg/cm(2)). There were no significant differences among group 2 (11.3 +/- 3.1 microg/cm(2)), group 3 (9.6 +/- 1.5 microg/cm(2)), and group 4 (12.3 +/- 1.7 microg/cm(2)). Group 1 demonstrated the highest transverse strength (78.1 +/- 6.1 MPa); the other groups were not significantly different from each other. All groups exhibited lower KH values at the 100-microm depth than at 700- and 1500-microm depths. At the latter depths, group 4 specimens demonstrated the highest hardness values (18.0 +/- 0.5 and 18.8 +/- 0.7 kg/mm(2), respectively). CONCLUSION: Within the limitations of this study, additional polymerization with hot water reduced residual monomer content of chemically polished acrylic resins on the first day. Although additional polymerization increased the internal hardness of the material, however, it did not recover the transverse strength that was decreased by the chemical polishing.

Acrylic Resins↗
PubMed1995

Finite element analysis of stress distribution at the tooth-denture base interface of acrylic resin teeth debonding from the denture base.

Acrylic resin teeth present a problem when they detach unexpectedly from the denture base resin. Detachment is caused by stress concentrations at the tooth/denture base resin interface. In this study, the finite element method was used to examine the stress distribution at this interface when a single static force that resembled incisal bite force was applied. The results indicated that irrespective of the type of acrylic resin teeth used, maximum tensile stresses were found at the palatal aspect of the interface. It is suggested that boxing the tooth in the acrylic resin will help redistribute stress concentrations favorably.

Acrylic Resins↗
PubMed1997

The swelling phenomenon of acrylic resin polymer teeth at the interface with denture base polymers.

PURPOSE: This study examined the interface between acrylic resin polymer teeth and denture base polymers. MATERIAL AND METHODS: An autopolymerized denture base polymer was cured either at 30 degrees C, 50 degrees C, or 70 degrees C, and a heat-cured denture base polymer was cured at 100 degrees C in contact with acrylic resin polymer teeth. The specimens were ground wet and polished to a thickness of 0.21 mm for the examination of the interface with a light microscope. The surface of the specimens was then treated with the solvent tetrahydrofuran, and the specimens were examined with a scanning electron microscope (SEM). RESULTS: As a result of grinding, the inner parts of the beads at the interface of the teeth were exposed to the denture base polymer. The inner part in these polymer beads of the polymer teeth swelled to a depth of 3 microns when the autopolymerized polymer was cured at 30 degrees C. When cured at 70 degrees C, the thickness of the swelled layer was 21 microns (p < 0.001). Microscopically, the interface between the heat-cured denture base polymer and the polymer teeth appeared diffuse in the region of the interpenetrating polymer networks (IPN) and the matrix. The IPN appeared as a separate zone in the outer parts of the beads of the teeth, both with the light microscope and with the SEM. CONCLUSIONS: The results suggest that by increasing the polymerization temperature, the monomers of the denture base polymers diffused more effectively into acrylic resin polymer teeth. This increases the bond strength between the polymer teeth and the denture base polymer.

Acrylic Resins↗
PubMed1997

Retention of Candida albicans on acrylic resin and silicone of different surface topography.

STATEMENT OF PROBLEM: The adhesion of microorganisms to a denture surface is a prerequisite for colonization. PURPOSE: This study compared the retention of Candida albicans on smooth and rough acrylic resin and silicone surfaces after a washing procedure to determine the effect of surface roughness on prosthesis infection and hygiene. MATERIAL AND METHODS: Standardized cell suspensions of C. albicans were incubated with smooth and rough acrylic resin and silicone surfaces for 1 hour at 24 degrees C. After washing, cells that had been retained on the surface were stained with acridine orange and examined with incident beam fluorescent microscopy. RESULTS: There was no significant difference in cell numbers on either of the smooth surfaces. Significantly higher numbers of cells (p > 0.0005) were observed on roughened surfaces (silicone > acrylic resin) than on smooth surfaces. The fitting surface of the maxillary denture was not polished. CONCLUSIONS: Silicones used in prostheses were processed against dental stone. The resultant surface roughness may facilitate microbial retention and infection and should therefore be kept to a minimum.

Acridine Orange↗
PubMed1998

Linear dimensional change of heat-cured acrylic resin complete dentures after reline and rebase.

STATEMENT OF PROBLEM: Relining and rebasing of complete dentures are common procedures to improve the fit of the prostheses. After relining or rebasing, adjustments may be required because of dimensional change that occurs during reprocessing of the denture when new denture base material is polymerized. PURPOSE: This study analyzed the linear dimensional change of heat cured acrylic resin that occurs during reline and rebase procedures for complete dentures. MATERIAL AND METHODS: Twenty-two maxillary and mandibular complete denture bases with artificial teeth were saturated by immersion in distilled water at 37 degrees C +/- 1 degree C. Fine crosses were marked on the incisal edges of the central incisors and the supporting cusps of the second molar teeth. Distances between the marks were measured with a high resolution traveling microscope. Heat-cured acrylic resin was processed by a long curing cycle of 72 degrees C for 6.5 hours, then heated to 100 degrees C for over 30 minutes and kept at 100 degrees C for 1 hour. The relined or rebased denture was allowed to cool slowly in the water bath for 48 hours to reach ambient temperature. The reference-crosses were measured immediately after careful deflasking. RESULTS: In the relining procedure, all incisor-molar and intermolar distances exhibited shrinkage of 0.3%, despite different shapes of maxillary and mandibular dentures. Results of the rebasing procedure were similar to that of the reline expect that only 0.1% intermolar shrinkage was found on the maxillary denture. CONCLUSION: Shrinkage was approximately 0.15 mm for an interarch distance of 50 mm. This degree of change is both clinically undetectable and insignificant. Using this processing cycle for acrylic resin in reline or rebase procedures did not cause clinically significant dimensional changes to complete dentures.

Acrylic Resins↗
PubMed1998

Stress relaxation of heat-activated acrylic denture base resin in the mold after processing.

STATEMENT OF PROBLEM: Stress relaxation of polymethyl methacrylate has been reported, but no studies have investigated residual stress relaxation in heat-activated acrylic denture base resin fabricated by the polymer-monomer mixture method. PURPOSE: This study evaluated the development of residual stress relaxation and clarified how restricted time in the stone mold influenced stress relaxation of heat-activated acrylic denture base resin after processing. MATERIAL AND METHODS: Flat, dumbbell-shaped specimens were used. Thermocouples and strain gauges were embedded in resin for measuring temperature and strain at the dough-stage of resin packing. To clarify the stress relaxation in the stone mold, specimens were removed from the mold by deflasking at 4 hours after from the start of bench cooling (immediately after reaching room temperature; control), and 1 day, 3, 5, and 10 days from the start of bench cooling. RESULTS: Shrinkage strains at deflasking were two thirds for 1 day restriction, one half for 3 and 5 days restriction, as compared with the control. CONCLUSIONS: This study suggested that removing a denture base fabricated by heat-activated acrylic denture base resin from the stone mold only after keeping it in stone mold for at least 1 day or more was effective for reducing deformation of the denture base.

Acrylic Resins↗
PubMed1999

Composite veneered acrylic resin provisional restorations for complete veneer crowns.

Restorations that are remade to improve esthetics, teeth with pronounced gingival-to-incisal color contrast, or high-value translucent teeth can limit the capability of shaded acrylic resin provisional restorations to satisfy the esthetic demands of certain patients. This article describes a procedure to incorporate a composite veneer in an acrylic resin provisional restoration. Improved optical properties of microfilled composite are combined with the excellent marginal seal and contour of acrylic resin. Precise control of color, translucency, and surface texture provide excellent interim esthetics and a better guide for the definitive prosthesis.

Acrylic Resins↗
PubMed1999

Intrinsic 'soft-start' polymerisation shrinkage-kinetics in an acrylate-based resin-composite.

OBJECTIVES: A resin-composite based on multi-acrylate monomers was to be evaluated for any differences in the setting shrinkage-strain kinetics relative to more conventional formulations based on di-methacrylate monomers. METHODS: Four resin-composites were examined for shrinkage-strain over time periods up to 60 min, from initial irradiation, using a 'bonded disk' measurement device. One material was evaluated with a standard and also a two-level (low to high) blue light irradiation regime. The test material (Solitaire), and the other two controls were studied under fixed-(normal) level irradiation by blue light. Measurements were made at 23 and 37 degrees C. RESULTS: The low-high light irradiation applied to one di-methacrylate composite led to a highly significant (p < 0.001) reduction in shrinkage-strain to a minimal level for the initial 0.2 min. The fixed-level irradiation with the acrylate-composite also led to a formally identical, but intrinsic 'soft-start' shrinkage-delay regime; significant at p < 0.001. Di-methacrylate composites under the same fixed-level light regime did not exhibit shrinkage delay. Both di-methacrylate and multi-acrylate composites exhibited increases in the range 18-29% in final equilibrium shrinkage-strain by increase of specimen temperature. SIGNIFICANCE: Reductions in the rate of initial shrinkage of light-cured restoratives may have clinical benefits for restoration bond-integrity nearly as important as reductions in the final equilibrium shrinkage-strain. This may be achieved either by special light irradiation regimes (low to high, or ramped) or in favourable cases by novel monomer-composite formulations and setting chemistry (e.g. Solitaire). The bonded disk shrinkage-strain measurement technique is suitable for the elucidation of such rapid kinetic and temperature-dependent events during photo-polymerisation setting processes.

Acrylic Resins↗
PubMed2002

Acrylic acid grafting and collagen immobilization on poly(ethylene terephthalate) surfaces for adherence and growth of human bladder smooth muscle cells.

In tissue engineering, degradable or non-degradable polymer matrices can act as cell-carrier-scaffolds. Cell adhesion and growth on these scaffolds can be promoted by immobilizing extracellular matrix proteins. Therefore, in this study, polymer poly(ethylene terephthalate) (PET) films were surface modified by graft polymerization of acrylic acid, to subsequently allow collagen (types I and III) immobilization and human smooth muscle cell expansion. The surfaces of PET were activated by plasma, followed by acrylic acid graft polymerization, resulting in covalently bound brushes, containing an average of either 0.22+/-0.1 or 5.93+/-0.87 microg/cm2 of poly(acrylic acid) (PAA). Subsequent electrostatic adsorption of collagen gave a surface concentration of 4.96 and 17.2 microg/cm2, respectively, as determined using radiolabelled 125I collagen. Both PET films grafted with 0.22 microg/cm2 of PAA with or without adsorbed collagen were apt for smooth muscle cell adhesion and proliferation. However, films grafted with 5.93 microg/cm2 were not. PAA-grafted PET films, onto which serum proteins of the culture medium adsorbed spontaneously, proved to be better matrices than films on which collagen has been immobilized. It, therefore, can be speculated that other serum proteins are more important than collagen for the human smooth muscle cell adhesion and growth on surface-modified polymer matrices.

Acrylic Resins↗
PubMed2002

Synthesis and characterization of chitosan-poly(acrylic acid) nanoparticles.

Chitosan (CS)-poly(acrylic acid) (PAA) complex nanoparticles, which are well dispersed and stable in aqueous solution, have been prepared by template polymerization of acrylic acid (AA) in chitosan solution. The physicochemical properties of nanoparticles were investigated by using size exclusion chromatography, FT-IR, dynamic light scattering, transmission electron microscope and zeta potential. It was found that the molecular weight of PAA in nanoparticles increased with the increase of molecular weight of CS, indicating that the polymerization of acrylic acid in the chitosan solution was a template polymerization. It was also found that the prepared nanoparticles carried a positive charge and showed the size in the range from 50 to 400 nm. The surface structure and zeta potential of nanoparticles can be controlled by different preparation processes. The experiment of in vitro silk peptide (SP) release showed that these nanoparticles provided a continuous release of the entrapped SP for 10 days, and the release behavior was influenced by the pH value of the medium.

Acrylic Resins↗