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Effect of some properties of metal strengtheners on the fracture resistance of acrylic denture base material construction.

In this study we investigated the effect of metal wire bonding to acrylic resin on the fracture resistance of an acrylic denture base material construction. Two different bonding methods were tested, and after measuring the resistance, the surface of the wires were examined by a scanning electron microscope. The effect that the placing of metal strengtheners in different positions in the acrylic resin had on the fracture resistance of the denture base material construction was also clarified. When three different positions of the metal wires in the acrylic resin were compared, the results showed that bonding of metal wire to acrylic resin somewhat enhanced the fracture resistance of test specimens, while the different positions of the wires had no effect on the fracture resistance.

Acrylic Resins↗

Determination of doughing and manipulation times of acrylic resin denture base material and a proposal for a specification for a packing plasticity test.

The doughing and manipulation times of a range of acrylic resin denture base polymers are presented in this study. The methods evaluated were: (i) probing following American Society for testing materials specification, F451-76; (ii) hole penetration following British Standard, 2487: 1989 and International Standard Organisation, 1567: 1988; (iii) probing using a penetrometer employing a 20 g load and 1 mm diameter needle; (iv) oscillating rheometer apparatus used at a fixed frequency of 1 Hz by sweeping through a programmed linear increase in strain. The results indicate that each of the methods is capable of evaluating the doughing and manipulation times of the unprocessed polymers. It is concluded that the Bohlin VOR Oscillating Rheometer is excellent for investigating the flow properties of denture base polymers but it cannot be recommended for a standards specification test because of the high cost. The penetrometer method has been shown to be superior to the current standards specification test and would be ideal for a packing plasticity standards test.

Denture Bases↗

Evaluation of mechanical and thermal properties of commonly used denture base resins.

PURPOSE: The purpose of this investigation was to evaluate and compare the mechanical and thermal properties of 6 commonly used polymethyl methacrylate denture base resins. MATERIALS AND METHODS: Sorption, solubility, color stability, adaptation, flexural stiffness, and hardness were assessed to determine compliance with ADA Specification No. 12. Thermal assessments were performed using differential scanning calorimetry and dynamic mechanical analysis. Results were assessed using statistical and observational analyses. RESULTS: All materials satisfied ADA requirements for sorption, solubility, and color stability. Adaptation testing indicated that microwave-activated systems provided better adaptation to associated casts than conventional heat-activated resins. According to flexural testing results, microwaveable resins were relatively stiff, while rubber-modified resins were more flexible. Differential scanning calorimetry indicated that microwave-activated systems were more completely polymerized than conventional heat-activated materials. CONCLUSION: The microwaveable resins displayed better adaptation, greater stiffness, and greater surface hardness than other denture base resins included in this investigation. Elastomeric toughening agents yielded decreased stiffness, decreased surface hardness, and decreased glass transition temperatures.

Adsorption↗

[Dental application of superplastic forming for titanium complete denture bases].

In order to investigate the application of superplastic in forming dental prosthesis, the sheets of titanium and its alloy were deformed to the complete denture bases by using a trial hot press and ceramic die. The results are summarized as follows: 1) By the hot press. It was possible to deform the sheet at a deformation speed ranging from 1 x 10(-3) to 3 x 10(-2) mm/sec at a temperature up to 900 degrees C under a vacuum down to 10(-3) Torr. 2) The trial ceramic die was prepared by sintering the green of the CaO-TiO2-ZrO2-MgCl2 system at 1150 degrees C for 6 hours in the atmosphere. The compressive strength, the thermal expansion, and the surface roughness of the test piece of the die were 11 kg/cm2, 0.8%, Ra = 1.4 microns and Rz = 6.8 microns, respectively. 3) Both the sheet of pure chemical titanium and commercial superplastic titanium alloy Ti-6Al-4V were deformed under the conditions of about 0.1 mm/min, 850 degrees C, and 10(-3) Torr. The deformed surface of the complete denture bases appeared to be nearly the same metallic color of each raw sheet and the pattern was the same as the detail of the die. The oxygen enriched layer of the article determined by EPMA was far thinner than that of a dental cast.

Dental Alloys↗

Effect of tinfoil substitute contamination on adhesion of resin denture tooth to its denture base.

At least one manufacturer claims that contamination of denture teeth with tinfoil substitute during processing is not detrimental. The purpose of this study was to determine whether tinfoil substitute contamination has any significant effect on the bond strength between acrylic resin denture teeth and their processed acrylic resin base. Eighty acrylic resin maxillary central incisors were processed to denture base material. The experimental group had the denture tooth ridgelap area contaminated with tinfoil substitute. The control group was not contaminated. The bond strength of the two groups was tested. The results indicate that contamination with tinfoil substitute significantly reduces the bond strength of acrylic resin denture teeth bonded to their denture base.

Acrylic Resins↗

Comparative evaluation of tensile bond strength of denture base resins to surface pretreated cobalt chromium base metal alloys--an in vitro study.

This study was undertaken to evaluate the tensile bond strength of acrylic resins to surface pretreated Cobalt-chromium base metal alloy. A total of 60 tensile bar specimens were prepared. One half of the bar was cast in cobalt-chromium alloy and the other half made of denture base resins attached to the alloy following surface pretreatment. Two denture base resins and five surface pre-treatments were used which included sandblasting, acid etching, use of metal adhesive primers and the combination of the above mentioned modes. Gradual axial loads were applied on the tensile bar specimen mounted on a Hounsfield tensometer till bond failure was evident. Statistical evaluation was done using Mann-Whitney U test. The study results indicate that the bond strength in those specimens wherein a combination of sandblasting, acid etching and priming was done as surface pretreatment, showed the maximum values as compared to the other groups.

Acid Etching, Dental↗

Influence of a thickness and processing method on the linear dimensional change and water sorption of denture base resin.

The purpose of this study was to evaluate the influence of a thickness and processing method on linear dimension change and water sorption in a denture base resin after storage in water for 24 hours, one week, and four weeks. Sixty wax specimens 65 mm long and 10 mm wide were fabricated in three thicknesses, 1.5, 3, and 4.5 mm. Three dimples were made in each wax specimen. A travelling microscope was used to measure the total distance from the uppermost dimple to the lowest dimple to the nearest 0.01 mm. Acrylic resin blocks were polymerized with 2 processing cycles (short and long-cured). Immediately after processing, all samples were measured by the same investigator. They were then weighed by an electronic precision balance capable of measuring to 0.001 g. Data were analyzed by analysis of variance. Thickness and time of storage were statistically significant on the dimensional change (linear and weight changes) of denture-base resin (p < 0.01), showing the influence of the processing method.

Absorption↗

The effect of pH on the cytotoxicity of eluates from denture base resins.

This in vitro study examined the effects of environmental pH on elution of potentially toxic substances from heat-, light-, and dual- (chemical plus light) polymerized denture base resins. Eluates were prepared by daily transfer of disks to fresh buffers at pH 4.0, 5.0, and 6.8 over a 5-day period. Oral epithelial cells were plated in culture dishes in medium containing the eluate. After 24 hours, cellular RNA synthesis was assessed by measuring tritiated uridine uptake. Effects of materials were compared to identical cultures that contained the appropriate buffer without the eluate. The results indicate that the cytotoxic components leach out of the denture base resins in different amounts and at different rates, and the amount of leaching can be affected by pH.

Acrylic Resins↗

Mechanical properties of reinforced denture base resin: the effect of position and the number of woven glass fibers.

This study examined the effects of the position and the number of woven glass fibers on the flexural strength, flexural modulus, and toughness of reinforced denture base resin. The woven glass fiber consisted of 1-4 laminated sheets. Chemical curing was used to polymerize three types of 4-mm-thick test specimens: fibers in compresrion, fibers in the center, and fibers in tension. Unreinforced specimens were produced as controls. A three-point flexural test was performed and the woven glass fiber content was calculated after the woven glass fiber was fired. The best results were obtained when the woven glass fiber was incorporated outside the base resin under tension, thereby increasing the flexural strength and flexural modulus. Furthermore, the denture base resin reinforced with woven glass fiber was made tougher by increasing the number of woven glass fibers incorporated into the portion under tension.

Analysis of Variance↗

Degree of conversion in denture base materials for varied polymerization techniques.

New processing techniques for denture base acrylic resins have been introduced which have not comparatively quantified the residual monomer content. While proper processing keeps the residual monomer in a tolerable range for most patients, tissue irritation and reaction due to potentially higher residual monomer in these alternative techniques could be a clinical concern. Decreased degree of conversion may influence physical properties as well as biocompatibility. This investigation evaluated the residual monomer content of acrylic resins cured by three different polymerization modes. Materials (polymerization system) evaluated were: Lucitone 199 (conventional process), Accelar 20 (rapid boil-out), and Acron MC (microwave). Fourier transform infrared spectrometry (FTIR) was employed to determine the degree of conversion. All curing methods produced similar results (Lucitone 199 = 92.7% (0.21), Acron MC = 92.6% (0.57), Accelar 20 = 90.9% (0-73). Conversion for Accelar 20 (rapid boil-out technique), though statistically different (P < 0.05, ANOVA) from the other two materials and polymerization techniques, was only slightly less. It is unlikely that the rapid boil-out technique would induce more adverse tissue responses than the other techniques included in this study.

Acrylic Resins↗

Cytotoxicity of denture base resins: effect of water bath and microwave postpolymerization heat treatments.

PURPOSE: This study compared the effect of two postpolymerization heat treatments on the cytotoxicity of three denture base resins on L929 cells using 3H-thymidine incorporation and MTT assays. MATERIALS AND METHODS: Sample disks of Lucitone 550, QC 20, and Acron MC resins were fabricated under aseptic conditions and stored in distilled water at 37 degrees C for 48 hours. Specimens were then divided into three groups: (1) heat treated in microwave oven for 3 minutes at 500 W; (2) heat treated in water bath at 55 degrees C for 60 minutes; and (3) no heat treatment. Eluates were prepared by placing three disks into a sterile glass vial with 9 mL of Eagle's medium and incubating at 37 degrees C for 24 hours. The cytotoxic effect from the eluates was evaluated using the 3H-thymidine incorporation and MTT assays, which reflect DNA synthesis levels and cell metabolism, respectively. RESULTS: The components leached from the resins were cytotoxic to L929 cells when 3H-thymidine incorporation assay was employed. In contrast, eluates from all resins revealed noncytotoxic effects as measured by MTT assay. For both MTT assay and 3H-thymidine incorporation, the heat treatments did not decrease the cytotoxicity of the materials tested. CONCLUSION: Resins were graded by 3H-thymidine incorporation assay as slightly cytotoxic and by MTT assay as noncytotoxic. Cytotoxicity of the denture base materials was not influenced by microwave or water bath heat treatment.

Acrylic Resins↗

Mechanical and thermal properties of hydroxyaptite filled poly (methyl methacrylate) heat processed denture base material.

The aim of this study was to evaluate the effect of powder-to-liquid ratio on the glass transition temperature (Tg) and the tensile properties of denture base material prepared from poly (methyl methacrylate) (PMMA) and hydroxyapatite (HA) previously treated with 3-trimethoxysilylpropyl methacrylate (gamma-MPS). Specimens for mechanical testing were prepared by adding composites powder (PMMA, BPO and HA) to the monomer (MMA and EGDMA) followed by hand mixing as in dental laboratory description usage. The glass transition temperature was studied by using differential scanning calorimetry (DSC). It was observed that the tensile properties and the Tg were affected by the powder-to-liquid ratio. The mechanical characterization of the materials were performed by using single edge notch-tension (SEN-T) specimens; the fracture toughness was slightly higher in formulation which contained HA filler compared to commercial denture base material.

Biomechanical Phenomena↗

Further aspects of design for distal extension removable partial dentures based on the Kennedy classification.

A supplement to the Kennedy classification of partially edentulous arches for restoration with removable partial dentures has been suggested. Factors affecting denture design relating to the position of the abutment teeth, the symmetry of the edentulous distal extensions, the arch form and the cross-sectional shape of the residual ridges have been discussed and classified. An understanding of the movement of the denture bases in relation to the influence of these factors makes for a rational approach to removable partial denture design and the treatment of complications observed clinically in removable partial denture wearers.

Alveolar Process↗

Effect of bench cooling on the dimensional accuracy of heat-cured acrylic denture base material.

OBJECTIVES: In order to obtain an insight on the internal stress caused by both polymerization and thermal shrinkage during the fabrication process of heat-cured denture resin, the effect of bench cooling on the dimensional accuracy of a heat-cured denture base resin was examined. METHODS: A dimensional change of a dumbbell-shaped specimen during the fabrication process was measured directly by using the strain gauge method. After polymerization, the specimens were treated in one of the following two processing methods: (1) rapid cooling: the specimen was removed from a stone mold within a container of boiling water at 100 degrees C and then left to cool in a thermo-stabilized room of 20+/-1 degrees C; (2) bench cooling: the flask was left to cool in a thermo-stabilized room of 20+/-1 degrees C for 140min, after which, the specimen was removed from the stone mold. The strain from deflasking was derived from the difference in the strain, before and after the removal of the specimen from the stone mold. The strain differential, before and after cooling, was determined as the total strain. RESULTS: The bench cooling for the heat-cured denture base resin reduced the strain caused by thermal shrinkage during the fabrication process. The observed reduction in the strain was 26% for the C(L) (direction of center's length), 11% for the E(L) (direction of left-edge's length), and 12% for the E(W) (direction of left-edge's width), when compared with the results obtained from the rapid-cooling method. CONCLUSIONS: The flask should be slowly cooled to room temperature, since the internal stress developed by thermal shrinkage will be relaxed during the cooling process.

Acrylic Resins↗

The effects of various disinfectant solutions on the surface hardness of an acrylic resin denture base material.

There is an increasing awareness of the importance of cross-infection control in dental clinics and laboratories. This study evaluates the effects of various disinfecting solutions on the surface hardness of an acrylic resin denture base material. Hardness was measured as resistance to indentation following the method specified by the British Standards Institute. The results demonstrated that immersion of denture base acrylic resin in disinfecting solution for up to 24 hours resulted in no significant effect on hardness values.

Acrylic Resins↗