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In vitro friction of stainless steel arch wire-bracket combinations in air and different aqueous solutions.

OBJECTIVES: To investigate the in vitro coefficient of friction of stainless steel arch wire-bracket combinations under fretting contact test conditions performed in air and in different aqueous solutions, like Ringer solution, Ringer with addition of a buffer, Ringer with addition of glucose, and Coca Cola. METHODS: The fretting test set-up used allowed to control on-line the contact configuration and the positioning of the contacting parts. A specific positioning method was used to achieve a parallel alignment of arch wire and bracket slot. The effect of arch wire size, roughness, and test environment were investigated. RESULTS: It was found that the aqueous solutions act as a lubricant compared to air. Friction was affected by the arch wire width while the roughness was found to have a limited effect. Stainless steel 0.018'' x 0.025'' arch wires exhibited higher frictional forces than stainless steel 0.017'' x 0.025'' arch wires on sliding against stainless steel 0.018'' x 0.025'' brackets in the selected test environments when tested under identical fretting test conditions. The wear damage on the arch wire after these in-vitro fretting tests was investigated. It revealed that these in-vitro tests are governed by a competition between oxidational wear and abrasive wear taking place at contact areas between brackets and arch wires. CONCLUSIONS: For all aqueous solutions a lower coefficient of friction was found compared to tests performed in ambient air.

Air↗

A theoretical formulation for boundary friction in articular cartilage.

A theoretical boundary friction model is proposed for predicting the frictional behavior of articular cartilage, including its time-dependent, velocity-dependent, and load-dependent responses. This theoretical model uses the framework of the biphasic theory for articular cartilage, and provides a mathematical formulation for the principle that interstitial fluid pressurization contributes significantly to reduction of the effective friction coefficient. Several examples of the application of this theory are provided, which demonstrate that a variety of experimentally observed cartilage frictional behaviors can now be theoretically predicted.

Cartilage, Articular↗

A two-body frictional wear test.

Enamel abraders used in two-body wear tests suffer the disadvantage that standardization is difficult or impossible to obtain. The aim of this study was to test whether steatite (a ceramic material with a Vickers Hardness similar to that of enamel) could be used as a satisfactory human enamel analogue. The friction and wear characteristics of 'spherical' abraders made from these two materials against composite and amalgam specimens were therefore compared. A two-body wear test for restorative materials was devised which could be carried out in a Universal Testing Machine and which allowed for continuous monitoring of the frictional forces during wear. The results showed that steatite and enamel abraders produced similar coefficients of friction (correlation coefficient, r = 0.98). A linear relationship was found between depth (and volume) of wear and number of cycles (r = 0.98 to 0.99). Wear rate was not affected by the increase in abrader facet area. The wear rate against the steatite abrader was slightly greater than that against enamel, but the two abraders were reasonably correlated (r = 0.94). Friction and wear were correlated for the steatite abrader (P < 0.05, r = 0.88) but not the enamel abrader. The hybrid composites had a high wear rate and wore both the abraders more than did the microfilled composites or amalgam. These findings suggest that steatite is a suitable substitute for enamel in this type of test.

Acrylic Resins↗

Physiologic axial load, frictional resistance, and the football shoe-surface interface.

The purpose of this investigation was to report on the interaction between different types of athletic shoes and playing surfaces using physiologic loads of 40 and 220 lbs. This is a continuation of our previous report using a load of 25 lbs. Nine shoes by three manufacturers were characterized as turf, court, molded cleat, or traditional cleat and tested on both natural grass and synthetic turf. A specially designed pneumatic testing device was used in order to measure translational resistance and rotational torque of the shoe-surface interface. Measurements were acquired for 1) force-X describing translational loading, 2) moment-Y describing the torque generated by linear translation, and 3) moment-Z describing the moment generated by axial rotation, and data were analyzed using repeated measures analysis of variance and Tukey's post-hoc comparison. It was found that increased the axial loads from 40 to 220 lbs significantly increased the frictional resistance (p < .05) between the shoe and the artificial turf surface in a nonlinear fashion. Turf shoes demonstrated the most frictional resistance of any group for this condition. Increases in the forces generated in linear translation from the axial load of 40 to 220 lbs produced the most significant increases of any resistance test on the turf surface. The cleated shoes (both traditional and molded) generated the highest frictional and torsional resistance on the grass surface when compared to the other categories of shoes. Grass generated higher peak moments than turf for the cleated shoes. These results demonstrate the considerable differences between laboratory and physiologic conditions and that the increase in frictional resistance is nonlinear with increasing loads.

Ankle↗

The ex vivo effect of ligation technique on the static frictional resistance of stainless steel brackets and archwires.

This ex vivo investigation compared the effect of various orthodontic ligation techniques on the static frictional resistance of stainless steel brackets and archwires under both dry and wet conditions. The techniques studied were: elastomeric modules tied conventionally and in a 'figure of 8' pattern, stainless steel ligatures, and Teflon-coated ligatures. The first part of the investigation involved the construction of calibration curves for each of the materials, so an estimate of the normal force exerted by the ligatures could be ascertained. Secondly, a pair of ligature locking pliers were modified so that ligatures could be placed with a standardized force. Finally, the four methods of ligation were directly compared on a specially constructed testing apparatus. Results revealed that elastomeric modules tied in a 'figure of 8' pattern produced significantly more friction than any other method tested, under both dry and wet conditions. No significant differences in frictional resistance were found between conventionally tied elastomeric modules and stainless steel ligatures. Teflon-coated ligatures, however, were associated with the lowest frictional forces. The results of the calibration tests indicated that the normal forces exerted by all four methods of ligation may be higher than previously estimated.

Calibration↗

Elimination of the friction effects in unconfined compression tests of biomaterials and soft tissues.

The mechanical properties of biomaterials and soft tissues are determined conventionally using unconfined compression tests. In such tests, frictionless specimen/platen contact in unconfined compression tests has to be assumed in determining the material properties of the materials. Previous theoretical analysis demonstrated, however, that the effects of the friction at the specimen/platen contact interface on the measured stress responses are non-negligible. In this study, a computational approach was proposed to eliminate the effects of friction. The friction coefficient between the specimen and the compression platens is measured first. Using a finite element model, the stress-strain relationship, without the influence of the friction effects, can be derived from the experimental data obtained in conventional unconfined compression tests. In order to validate the proposed approach, unconfined compressive tests of rubber have been performed.

Algorithms↗

The effects of proteins on the friction and lubrication of artificial joints.

The tribological testing of artificial hip and knee joints in the laboratory has been ongoing for several decades. This work has been carried out in an attempt to simulate the loading and motion conditions applied in vivo and, therefore, the potential for the success of the joint. However, several different lubricants have been used in these tests. The work documented in this paper compares results obtained using different lubricants and makes suggestions for future work. Hip joints and knee joints of different material combinations were tested in a friction simulator to determine their friction and lubrication properties. Both carboxymethyl cellulose (CMC) fluids and bovine serum (with CMC fluids added) were used as the lubricants. These were prepared to various viscosities to produce the Stribeck plots. Human synovial fluid, of just one viscosity, was used as the lubricant with some of the joints to give a true comparison with physiological lubricants. The results showed that, in most cases, the lubricant had a significant effect on the friction developed between the joint surfaces. This is thought to be due to the proteins that are present within the bovine serum adsorbing to the bearing surfaces, creating 'solid-like' films which rub together, protecting the surfaces from solid-to-solid contact. This would be beneficial in terms of wear but can either increase or decrease the friction between the contacting surfaces. It is important to simulate the conditions in vivo as closely as possible when testing these joints to try to obtain a better comparison between the joints and to simulate more accurately the way that these joints will operate in the body. In an attempt to simulate synovial fluid, bovine serum seems to be the most popular lubricant used at present. It would be beneficial, however, to develop a new synthetic lubricant that more closely matches synovial fluid. This would allow us to predict more accurately how these joints would operate long-term in vivo.

Body Fluids↗

Friction and lubrication in cushion form bearings for artificial hip joints.

Two hip joint prostheses were designed and constructed to be elastohydrodynamically equivalent producing approximately equal initial contact areas and theoretical film thicknesses. One was made from conventional UHMWPE (ultra-high molecular weight polyethylene) and the other was a cushion component which had a low modulus layer introduced into the joint space. Friction measurements were carried out on a pendulum simulator apparatus and the two joints were compared. In addition the experimental results were compared with theoretical values of friction predicted from elastohydrodynamic lubrication theory. Values for the friction factor at peak load and peak velocity in the cushion cup (0.003-0.009) were much lower than in the UHMWPE cup (0.017-0.042). The low friction values in the cushion cup are consistent with fluid film lubrication in the contact with the thin lubricating film being preserved by microelastohydrodynamic action.

Friction↗

A three-axis hip joint simulator for wear and friction studies on total hip prostheses.

A three-axial, single-station hip joint simulator was designed and built for wear and friction studies on total hip prostheses. The design of the apparatus is described in detail. Continuous level walking is simulated. All three motion components, flexion-extension, abduction-adduction and internal-external rotation, are included. The motions are implemented electromechanically and the uniaxial load pneumatically. The load is measured continuously. For accurate measurement of wear, the apparatus has a loaded control joint, which also renders both the test and control joints self-centering, as they are loaded in series. The frictional torque of the test joint can be measured continuously throughout the wear test, which is an exceptional feature. Four tests of five million cycles each were completed using 32 mm diameter Co-Cr-Mo femoral heads and 5.6 mm thick, metal-backed, ultra-high molecular weight polyethylene acetabular cups as test specimens. Their wear and friction behaviour is described and discussed in relation to previous simulator studies and clinical observations. The lubricant was distilled water, maintained at body temperature. The wear of the cups was measured gravimetrically at intervals. The average wear rate was 3.9 mg/one million cycles, corresponding to 0.03 mm/year, and the average coefficient of friction was 0.01.

Biomechanical Phenomena↗

Air friction and rolling resistance during cycling.

To calculate the power output during actual cycling, the air friction force Fa and rolling resistance Fr have to be known. Instead of wind tunnel experiments or towing experiments at steady speed, in this study these friction forces were measured by coasting down experiments. Towing experiments at constant acceleration (increasing velocity) were also done for comparison. From the equation of motion, the velocity-time curve v(t) was obtained. Curve-fitting procedures on experimental data of the velocity v yielded values of the rolling resistance force Fr and of the air friction coefficient k = Fa/v2. For the coasting down experiments, the group mean values per body mass m (N = 7) were km = k/m = (2.15 +/- 0.32) x 10(-3)m-1 and ar = Fr/m = (3.76 +/- 0.18) x 10(-2)ms-2, close to other values from the literature. The curves in the phase plane (velocity vs acceleration) and the small residual sum of squares indicated the validity of the theory. The towing experiments were not congruent with the coasting down experiments. Higher values of the air friction were found, probably due to turbulence of the air.

Air↗

Friction loss in straight pipes of unplasticized polyvinyl chloride.

In order to design proper ductwork for a local exhaust system, airflow characteristics were investigated in straight pipes of unplasticized polyvinyl chloride (PVC). A linear decrease in static pressure was observed downstream at points from the opening of the VU pipes (JIS K 6741) located at distances greater than 10 times the pipe diameter, for velocities ranging between 10.18-36.91 m/s. Roughness inside pipes with small diameters was found to be 0.0042-0.0056 mm and the friction factor was calculated on the basis of Colebrook's equation for an airflow transition zone. An extended friction chart was then constructed on the basis of the roughness value and the friction factor. This chart can be applied when designing a local exhaust system with the ducts of diameters ranging from 40 to 900 mm. The friction loss of the PVC pipe was found to be approximately 2/3 of that of a galvanized steel pipe.

Equipment Design↗

Evaluation of in vitro properties of films of saliva substitutes in contact with different surfaces. A comparative study with instruments for measurements of friction and rheologic properties.

An instrument based on friction measurement has been developed to evaluate oral mucosal dryness objectively. The purpose of this study was to compare the friction instrument with instruments measuring in vitro rheologic properties. Measurements were performed against steel and irreversible hydrocolloid after application of different concentrations of aqueous solutions of carboxymethylcellulose and chitosan lactate. The results of the measurements were logical, with inversely proportional values for the friction instrument as compared with values obtained using the instrument measuring rheologic properties; that is, increased viscosity led to decreased friction values.

Alginates↗

Frictional behaviour of bovine articular cartilage.

The experimentally measured indentation displacement and friction of normal and degraded (treated with chondroitinase AC) bovine articular cartilage plugs against a smooth steel plate were compared with the predictions based on the biphasic theory using the finite element method. It was found that the measured indentation displacement of both cartilage specimens could be predicted from the biphasic theory and the permeability for the degraded cartilage specimen was increased approximately three times. However, the measured friction coefficient was much lower for short period of loading, and the difference in the finite element prediction of friction coefficient between the normal and degraded cartilage specimens was not observed in the experiment. Therefore, it was concluded that both biphasic and other mechanisms were important in controlling the frictional and lubricating characteristics of articular cartilage in mixed and boundary lubrication regimes.

Animals↗

Does nasal breathing cause frictional trauma in allergic rhinitis?

OBJECTIVES: Frictional stress on the walls of a tube increases with increased air flow and as the diameter of the tube is reduced. High values of frictional stress may occur in the nose during nasal obstruction which could damage the nasal mucosa particularly when the mucosa is inflamed and fragile as in allergic rhinitis. The effect of nasal airflow induced frictional stress on the nasal mucosa was studied in patients with allergic rhinitis. METHODS: We studied nasal peak flow rate in eight patients with allergic rhinitis and nasal obstruction comparing the change in peak expiratory flow after they breathed for 30 minutes through an obstructed and a patent nostril. Patients were studied in the right and left lateral decubitus positions to increase and decrease the resistance in the lower and upper nostril respectively and thus minimize any effects of cyclical changes in nasal resistance. Subjects breathed for 30 minutes through the upper patent nostril (schedule 1) and for a further 30 minutes through the lower obstructed nostril (schedule 2). Nasal peak expiratory flow rate was measured in both nostrils separately in both positions after each schedule. RESULTS: There was a significant reduction in mean (SD) nasal peak flow rate (-12.8 (4.06) L/min) after subjects had breathed for 30 minutes through the obstructed nostril. There was no significant change in nasal peak flow rate after subjects had breathed through the patent nostril, or in the nostril that had no flow for 30 minutes. CONCLUSIONS: These findings are compatible with the hypothesis that frictional stress due to airflow through an obstructed nostril induces trauma and swelling of the nasal mucosa of patients with allergic rhinitis.

Adolescent↗

Subsidence of THA stems due to acrylic cement creep is extremely sensitive to interface friction.

Acrylic cement, used to fixate total hip arthroplasty (THA), creeps under dynamic and static loading conditions. As a result, THA stems which are debonded from the cement, may gradually subside, depending on their shape and surface roughness. The purpose of this study was to evaluate the relationship among dynamic load, creep characteristics, interface friction, and subsidence patterns. A laboratory model consisting of a metal tapered cone, surrounded by a cement mantle, was developed. The cone was gradually compressed in the cement by a dynamic, sinusoidal axial force, cycling between 0 and 7 kN for 1.7 million cycles at a frequency of 1 Hz. Subsidence and cement strain were monitored. Two tapers were tested in this way. The relationships among subsidence, creep properties and interface friction were evaluated from a finite element (FE) model, used to simulate the experiments. In this model, the creep properties obtained in dynamic and static, tension and compression experiments measured earlier, were used. The subsidence patterns of both tapers were similar, but one subsided more than the other (380 vs 630 microns). Both subsided stepwise instead of continuous, with a frequency much smaller than that of the applied load. The characteristics of the subsidence and cement-strain patterns could be reproduced by the FE model, but not with great numerical precision. The stepwise subsidence could be explained by slip-stick mechanisms at the interface starting distally and gradually working towards proximal. Variations in friction from 0.25 to 0.50 reduced the total subsidence and the step frequency by about 50%. It was concluded that FE-models used to simulate the mechanical endurance characteristics of THA reconstructions, extended to incorporate cement creep, produce realistic results. These results showed that prosthetic subsidence under dynamic loads occurs due to cement creep. The extent of the subsidence is extremely sensitive to interface friction, hence to small variations in surface roughness and cement constitution. This may explain the relatively large variation of in vivo prosthetic subsidence rates reported in the literature.

Acrylic Resins↗

Friction properties at the bone-metal interface: comparison of four different porous metal surfaces.

Detailed friction load-displacement response of four distinct metallic surfaces [one beaded porous metal (CTR) and three cast Co-Cr alloy ingrowth mesh surfaces, nonplanar mesh (INX), cast mesh 1 (CM1), and cast mesh 2 (CM2)] on poly-urethane and cancellous bone specimens of six tibiae were measured under different normal stresses (0.1, 0.15, or 0.025 MPa). Bone cubes were obtained from different proximal regions of resurfaced cadaveric tibiae. Both monotonic and cyclic fatigue loadings of up to 4000 cycles at 1 Hz were considered. Comparison of measured results indicated that the friction coefficient was not affected by the magnitude of normal stress and the bone excision site (medial, lateral, anterior, posterior, and central). The CM2 surface showed significantly greater resistance with friction coefficients of more than 0.9 for the bone and 0.8 for the polyurethane. The INX surface yielded the second largest resistance followed by CM1 and CTR surfaces. NO significant difference was found between these latter two surfaces. Fatigue tests of up to 4000 loading-unloading cycles showed about 10% reduction in friction coefficient for CTR and INX surfaces, while negligible reduction was found for CM1 and CM2 surfaces.

Bone Substitutes↗

Surface modification and characterization of some commonly used catheter materials. II. Friction characterization.

The effects of the modification of polystyrene (PS), polyethylene (PE), poly(vinyl chloride) (PVC), silicone rubber (SR), and fluorinated ethylene propylene (FEP) copolymer by radio frequency glow discharge in a helium environment were presented in part I. The hydrated polymer surfaces were characterized by XPS, SEM, visual microscopy, and by contact angle measurements. In general, exposure of the polymers to RFGD produced an oxidized hydrophilic surface, yet the roughness of the surface was unaltered by the relatively mild plasma conditions used. In this article, the frictional behavior of oxidized and unoxidized SR, PE, and FEP in distilled water, isotonic saline, and blood plasma environments is examined experimentally. The results are discussed in relation to the properties generally believed to affect frictional phenomena and to the surface properties as determined in part I. Results indicate that RFGD-treated SR generates less friction than untreated SR when dragged across all untreated and treated polymer surfaces, whether the medium is distilled water or an isotonic saline solution. Friction is consistently lower in a blood plasma medium between all surfaces investigated, most probably because of the presence of adsorbed proteins at the polymer interfaces.

Biocompatible Materials↗

Analysis of tablet compaction. I. Characterization of mechanical behavior of powder and powder/tooling friction.

In this first of two articles on the modeling of tablet compaction, the experimental inputs related to the constitutive model of the powder and the powder/tooling friction are determined. The continuum-based analysis of tableting makes use of an elasto-plastic model, which incorporates the elements of yield, plastic flow potential, and hardening, to describe the mechanical behavior of microcrystalline cellulose over the range of densities experienced during tableting. Specifically, a modified Drucker-Prager/cap plasticity model, which includes material parameters such as cohesion, internal friction, and hydrostatic yield pressure that evolve with the internal state variable relative density, was applied. Linear elasticity is assumed with the elastic parameters, Young's modulus, and Poisson's ratio dependent on the relative density. The calibration techniques were developed based on a series of simple mechanical tests including diametrical compression, simple compression, and die compaction using an instrumented die. The friction behavior is measured using an instrumented die and the experimental data are analyzed using the method of differential slices. The constitutive model and frictional properties are essential experimental inputs to the finite element-based model described in the companion article.

Chemistry, Pharmaceutical↗