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A comparison of palatal adaptation in acrylic resin denture bases using conventional and anchored polymerization techniques.

PURPOSE: The study investigated the effects of palatal depth and a resin anchoring system on the adaptation of denture base resin to the master cast after compression molding and heat polymerization. MATERIALS AND METHODS: Forty-eight virtually identical polymethyl methacrylate dentures were fabricated on master casts with either a deep or shallow palatal vault. One half of the master casts of each palate type were altered by the addition of anchoring holes along the posterior land area, as well as perpendicularly in the midsaggital area. Anchoring holes were made with a #8 round bur to a depth of 5 mm. Twenty-four hours after polymerization, the bases on their casts were sectioned at the posterior border and evaluated for degree of adaptation using a traveling microscope. Maladaptation at the interface of the denture base and master cast was measured at predetermined mediolateral locations. A split-plot analysis of variance (alpha = 0.05) was performed followed by a post-hoc Dunn Multiple Comparison Test. RESULTS: In general, depth of the palatal vault did not significantly influence denture palatal discrepancy (p =.0780), but the use of the anchoring system significantly reduced mean gap distances (p =.000). At lateral and midpalate locations, gap distances between the denture bases and their casts were reduced from approximately 0.3 mm to approximately 0.1 mm when the anchoring system was used. CONCLUSIONS: Mean gap distances for steep palate dentures were significantly less than shallow palate dentures at vestibule and lateral palate locations, and anchoring holes placed in an edentulous master cast along the posterior land area and at the midline significantly improved the adaptation of denture bases.

Acrylic Resins↗

The effect of acquired salivary pellicle on the surface free energy and wettability of different denture base materials.

OBJECTIVE: The objective of the present study was to evaluate the effect of salivary coating on the wettability and surface free energy of different denture base materials. METHODS: Five acrylic resin and two metallic denture base materials were investigated. Ten specimens of each material (20 x 15x1.5mm) were fabricated and a standardized method was used for polishing the test specimens. Whole unstimulated saliva was collected from a single healthy donor. The wettability properties of the materials were tested before and after organic layer formation. The wetting forces were determined according to the Wilhelmy Plate Technique. Diiodomethane, ethylene glycol and formamide were used as probe liquids. The contact angles, Lifshitz-van der Waals surface energy components, Lewis acid-base surface energy components and total surface energies were calculated using the equations described in the paper. The significance of the differences in the experimentally determined surface energies of different denture materials are calculated by statistical methods. CONCLUSIONS: Light-cured acrylic resin was the most wettable material with a significant basic character. Organic layers decreased the total surface free energies of all materials and at the same time imparted a more basic character. The coatings had a homogenizing effect in terms of the surface free energy components of the denture materials, nevertheless, their adhesive properties were still influenced by the substrate employed.

Acrylic Resins↗

[Acrylic denture base materials in dentistry. The influence of immersion of bases on the palatal gap].

The method of experimental design, we used, is versatile enough to allow the study of immersion in water at 37 degrees C during 15 days after curing, as a new parameter able to influence the deformation of denture bases, without any additional experiment. According to the experimental conditions used to make up denture bases, this parameter can, in some cases, modify appreciably the deviation in the palate region.

Acrylic Resins↗

Immediate maxillary denture base extension for posterior palatal seal.

A procedure for extension of the maxillary denture base for development of a posterior palatal seal is described. The technique involves provisional extension with paraffin wax and adding direct relining resin supported by a silicone putty core. This simple, quick procedure achieves immediate recovery of retention for underextended maxillary dentures without additional laboratory procedures.

Dental Polishing↗

Denture base materials.

A variety of materials have been used in the fabrication of denture bases. The advantages and disadvantages of these materials are discussed. Special emphasis is placed on polymeric material. particularly poly (methyl methacrylate) (PMMA). The chemical basis for formation of PMMA is provided to facilitate understanding.

Ceramics↗

Fatigue properties of acrylic denture base resins.

Observations were made of fractured surfaces caused by flexural and tensile fatigue tests made in polymethyl methacrylate denture base resins (PMMA). In addition, the changes in dynamic viscoelastic and tensile properties of the materials along with fatigue propagation were investigated. In the tensile and flexural fatigue tests, both the fractured surfaces, which had striations on their surfaces and cracks near the fractured section, closely resembled each other in appearance. On the other hand, all of the tensile properties, such as elastic modulus, toughness and tensile strength, decreased with the increase of the number of stress cycles in the fatigue test. The storage modulus (E') of the material decreased gradually along with fatigue propagation over the whole range of temperatures tested. The loss modulus (E") and mechanical loss tangent (tan delta) increased slightly. The fatigue limit of four commercial denture base resins varied widely from one product to another.

Dental Stress Analysis↗

A denture base resin with low water absorption.

The aim of this study was to investigate poly(isobutyl methacrylate) as a potential denture base material. It was found to have very low water absorption but poor mechanical properties and a low glass transition temperature. The latter features render the material itself unsuitable for use as a denture base material, but indicated that isobutyl methacrylate may be a useful co-monomer for reducing water absorption.

Absorption↗

Determination of residual stresses in denture base polymers using the layer removal technique.

In order to study the influence of residual stresses on dimensional accuracy and mechanical properties of denture bases, an experimental model was devised for measurement of residual stresses in acrylic denture base polymers. Rectangular bar coupons were cut from resin plates heat processed by conventional dental methods. They included samples which had been slow and fast cooled after polymerization and had been stored in dry and wet environments. Uniaxial residual stress distributions for each coupon were disclosed by removing layers of known thicknesses and measuring the ensuing deflection of the specimens. Coupons of a commercial acrylic resin were annealed and used as controls. ANOVA and Scheffe's test were used to compare experimental conditions at the 95% confidence level. Dry specimens exhibited residual surface compressive stresses from 0.43-0.83 MPa (62-120 psi). Water-stored specimens showed higher stress levels, 2.86-3.24 MPa (414-470 psi). Slow cooled pigmented acrylic coupons which were dry showed higher residual stresses compared with other dry but nonpigmented specimens. No significant differences were found between pigmented or clear coupons which contained moisture.

Acrylic Resins↗

Fabrication of an overdenture covering a torus palatinus using a combination of denture base materials: a case report.

A maxillary torus provides a challenge when restoring an edentulous arch. Tori tend to have very thin mucosa and can be intolerant of normal pressures from a denture base. The tori tend to have large undercuts and at times extend to the junction with the soft palate, preventing the creation of a good palatal seal. Triple lamination involves combining 3 materials to fabricate a denture base that utilizes the retentive aspects of the torus. The thermoplastic flange provides a measure of flexibility, allowing the denture to seat over the torus. The resilient liner provides a cushion to diffuse the occlusal load, while the rigid acrylic base provides the support for the denture teeth. Using this approach, a very retentive denture was fabricated using the maxillary torus as a key element in anchoring the prosthesis.

Acrylic Resins↗

Dental abrasion caused by a cobalt-chromium denture base.

A case of abrasive tooth surface loss caused by repeated sliding contact with the tissue surface of a cobalt-chromium denture base is described. The mode of material-tooth contact was brought about by an unusual patient habit which would have been difficult to foresee when the choice of denture base material was made.

Adult↗

Effects of polymerization shrinkage on the interfacial stress at resin-metal joint in denture-base: a non-linear FE stress analysis.

OBJECTIVES: The purpose of this study was to investigate the effects of polymerization shrinkage on stress at the interface between resin and metal in removable dentures. METHODS: Three-dimensional finite element models of a denture-base were studied, which consisted of acrylic occlusal rims with different heights and metal frameworks. A relaxation modulus of 1.5 GPa for the resin and a Young's modulus of 220 GPa for the metal were used as the material properties. Each model was constrained at the edge of the framework on the palatal vault. Surface-to-surface contact elements were used to calculate the interfacial stress in a direction perpendicular to the bond surface under a linear shrinkage ranging from 0.41 to 0.65%. The principal stress within the resin was also calculated. RESULTS: The maximum interfacial and principal stresses within the denture-base increased with resin shrinkage. Under the lowest linear shrinkage, the mean area percentages in the resin-metal joint that showed interfacial tensile stresses over 10 and 20 MPa were 63.4 and 0%, respectively. While under the highest linear shrinkage, these mean area percentages were 98.8 and 38.1%, respectively. Negligible differences in the stresses were shown by occlusal heights. SIGNIFICANCE: The polymerization shrinkage level has a significant influence on the residual stress at the resin-metal interface. Enhancement of the bond strength on the interface can reduce the failure probability at a resin-metal joint.

Acrylic Resins↗

Iodinated methacrylate copolymers as X-ray opaque denture base acrylics.

OBJECTIVES: The purpose of this study was to evaluate novel iodinated methacrylate copolymers as X-ray opaque denture base resins. METHODS: The synthesis of specific monomers and suspension copolymerization with methyl methacrylate to produce copolymer beads. The resulting beads were processed in an identical manner to standard PMMA to produce test-pieces for mechanical testing. RESULTS: Samples prepared from beads containing 25 wt% of the iodinated copolymer exhibited an X-ray opacity equivalent to that exhibited by a similar thickness of aluminium. Furthermore, the appearance and mechanical properties were comparable to standard PMMA, while thermal stability proved superior. CONCLUSION: These novel iodinated methacrylate monomers show promise not only as polymerizable additives to methyl methacrylate to produce an X-ray opaque denture base but also as thermally stable copolymerizable additives to other applications where X-ray opacity would be advantageous.

Contrast Media↗

Residual monomer concentrations in denture-base acrylic resin after an additional, soft-liner, heat-cure cycle.

OBJECTIVES: To determine the effects on methylmethacrylate (MMA) monomer concentration of a second heat-cure cycle introduced for the purpose of processing a denture soft-liner. METHODS: Two denture-base resins (Lucitone199 and Trevalon; Dentsply International, York, PA, USA) were selected. Heat-cure cycles were S (73 degrees C/90 min + 100 degrees C/30 min); L (73 degrees C/9 h); SM (S + 100 degrees C/2 h); LM (L + 100 degrees C/2 h). Cycles SM and LM thus simulated the effect of a further, soft-liner, heat-cure cycle. Groups (n = 6) of the specimens of the denture-base were prepared in the form of thin polymer disks. Monomer was then obtained from the broken fragments of disks by acetone extraction. Concentrations of MMA monomer were determined by reversed-phase high performance liquid chromatography (HPLC). Two-way ANOVA and independent sample t-tests were used to compare the results. RESULTS: The cycle S, applied to Lucitone199, gave a mean concentration of 1.95 wt% MMA (SD 0.24). The cycle L gave the highest level of residual concentration of MMA monomer in both materials. Cycles SM and LM, applied to Trevalon and Lucitone199, gave significant reductions of residual concentration of MMA monomer (p < 0.05). SIGNIFICANCE: The HPLC method was suitable for determining the amount of residual monomer in the denture-base acrylic resin. A further (soft-liner) heat-cure cycle had a statistically significant effect on reducing residual monomer concentrations, and this may have an effect upon mechanical properties.

Acrylic Resins↗

Bonding of synthetic resin teeth to microwave or heat activated denture base resin.

Bonding between acrylic resin teeth and a denture base material was investigated after microwave and hot water-bath curing. The specimens were tested according to the methods of the International Organisation for Standardisation (ISO 3336-1977 Dentistry-Synthetic Resin Teeth) using a universal testing machine. Superior bonding was found after hot water-bath curing. The generation of more porosities during microwave curing is the most likely explanation for the bond failures in this group. This finding is of clinical importance as the choice of curing method could influence the risk of loosening of acrylic teeth from the denture. No statistically significant difference in the fracture load between the two types of curing was found, which was expected as the load at fracture is not only related to the binding forces but also to factors such as the contact area and the fracture type.

Acrylic Resins↗

Impact strength of acrylic denture base resin reinforced with woven glass fiber.

This study investigated the effect of the number and position of woven glass fibers in denture base resin matrix on its impact strength. Test specimens were reinforced with woven glass fiber 0.5, 1.0, or 1.5 mm below the surface. The impact strength was tested using an Izod-type impact tester with an impact speed of 335 cm/s, which simulates dropping the denture, and using a flywheel-type impact tester with a two-point support at 13.5 and 75.0 cm/s, which simulates the chewing. The woven glass fibers had a strengthening effect in all tests, and the impact resistance was further improved when the woven glass fibers were positioned more superficially in the resin. The results suggest that woven glass fiber is an effective reinforcement in denture base resin.

Analysis of Variance↗

The tooth-denture base bond: stress analysis using the finite element method.

Although acrylic resin teeth are the most popular artificial teeth used for denture construction, a high number fracture away at the tooth-denture base interface. Various causes have been documented for this failure; however, it is logical that eventual fracture occurs due to localised tensile stresses at this interface. Examination of these stresses using the finite element method showed that on load application to the upper incisors, the maximum tensile stresses were concentrated within the body of the tooth and not at the tooth-denture base interface. Stresses encountered at the interface were relatively low and introduction of a crack made no significant difference to their magnitude.

Acrylic Resins↗

Effect of the curing cycle on residual monomer levels of acrylic resin denture base polymers.

It has been shown previously that high levels of residual monomer have a deleterious effect on the properties of denture base polymers. Levels of residual monomer were determined on a homopolymer and a copolymer using gas-liquid chromatography. A wide range of recommended and 'short cut' curing cycles were then investigated which produced values ranging from 0.56 to 18.46%. From the ranges examined an optimum cycle of 7 h at 70 degrees C and 1 h at 100 degrees C was established which was used to polymerize 23 currently available synthetic denture base polymers. Only small differences were found between the materials tested with a range from 0.54 to 1.08% of residual monomer.

Acrylic Resins↗