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At least 217 records · Page 12Linked to original sources
PubMed2005

Magnetic and transport properties of the magnetic Polaron: application to Eu1-xLaxB6 system.

To understand the role of the magnetic polaron in magnetic and transport properties of Eu(1-x)LaxB6, we investigate the low carrier density ferromagnetic Kondo lattice model by using the Monte Carlo methods. We demonstrate that the magnetic-polaronic (MP) state with the insulating nature is realized in the phase-separated region in between the ferromagnetic and antiferromagnetic (AFM) states in the phase diagram. The insulating behaviors of EuB6 just above T(C) and of Eu(1-x)LaxB6 with 0.05<x<0.2 are well explained by MP states in the paramagnetic and the AFM background, respectively. The Eu vacancy plays a crucial role in forming the bound magnetic polaron and so producing the resistivity peak in EuB6. By applying the weak magnetic field, the AFM metallic ground state is destroyed into the MP state, but the metallic behavior is restored by the strong magnetic field, as is observed for Eu(1-x)LaxB6 with 0.2< x < 0.3.

Journal Article↗
PubMed2005

Spectroscopy of magnetic excitations in magnetic superconductors using vortex motion.

In magnetic superconductors a moving vortex lattice is accompanied by an ac magnetic field which leads to the generation of spin waves. At resonance conditions the dynamics of vortices in magnetic superconductors changes drastically, resulting in strong peaks in the dc I-V characteristics at voltages at which the washboard frequency of the vortex lattice matches the spin wave frequency omegaS(g), where g are the reciprocal vortex lattice vectors. We show that if the washboard frequency lies above the magnetic gap, measurement of the I-V characteristics provides a new method to obtain information on the spectrum of magnetic excitations in borocarbides and cuprate layered magnetic superconductors.

Journal Article↗
PubMed2006

Spin dynamics and magnetic order in magnetically frustrated Tb2Sn2O7.

We report a study of the geometrically frustrated magnetic material Tb2Sn2O7 by the positive muon-spin relaxation technique. No signature of a static magnetically ordered state is detected while neutron magnetic reflections are observed in agreement with a published report. This is explained by the dynamical nature of the ground state of Tb2Sn2O7: the Tb3+ magnetic moment characteristic fluctuation time is approximately 10(-10) s. The strong effect of the magnetic field on the muon-spin-lattice relaxation rate at low fields indicates a large field-induced increase of the magnetic density of states of the collective excitations at low energy.

Journal Article↗
PubMed2001

Study of magnetic materials using helicity-modulated X-ray magnetic circular dichroism.

A new helicity-modulation technique has been applied for recording X-ray magnetic circular dichroism (XMCD) at the K-absorption edge in transition-metal magnetic materials. This technique enables the measurement of the XMCD spectrum with high precision and under extreme conditions. The refined spectrum is presented at the Fe K edge for pure Fe, Fe4N and Co-ferrite. The method is very promising for site-assignment of magnetic cations and for detailed investigation of the magnetic states in a local environment. In Mn3MC perovskites, the dependence of the Mn K-edge XMCD spectrum on temperature and magnetic field demonstrates that the orbital moments are closely associated with the magnetic phase transition. New information obtained from the refined spectrum and novel phenomena observed in temperature and field variations is presented.

Journal Article↗
PubMed1996

Nanoscale Magnetic Domains in Mesoscopic Magnets

The basic magnetic properties of three-dimensional nanostructured materials can be drastically different from those of a continuous film. High-resolution magnetic force microscopy studies of magnetic submicrometer-sized cobalt dots with geometrical dimensions comparable to the width of magnetic domains reveal a variety of intricate domain patterns controlled by the details of the dot geometry. By changing the thickness of the dots, the width of the geometrically constrained magnetic domains can be tuned. Concentric rings and spirals with vortex configurations have been stabilized, with particular incidence in the magnetization reversal process as observed in the ensemble-averaged hysteresis loops.

Journal Article↗
PubMed1999

Enhancement of enzyme reaction of magnetically anisotropic polyacrylamide gel rods immobilized with ferromagnetic powder and beta-D-galactosidase in an alternating magnetic field.

An immobilized polyacrylamide gel containing beta-D-galactosidase and Sr-Ba-ferrite was magnetized in a static magnetic field. The gel rods (10 mm long, O 2 mm) exhibiting magnetic anisotropy could move at lower than 100 Hz but not at higher than 250 Hz in an alternating magnetic field of 200 Oe. In case of immovability of gel rods, the apparent enzymic activity increased 3 times higher under exposure of an alternating magnetic field of 500 Oe (570 Hz). It could be explained that the ferromagnetic powder inside the gel might vibrate under the influence of elasticity of gel in the alternating magnetic field of 100 or 500 Oe and 0.2-12 kHz. This might facilitate faster diffusion of the substance inside the gel and transportation of the substrate and the product through the surface of gel. Consequently, the enzyme reaction was apparently activated.

Acrylic Resins↗
PubMed1991

Use of computed tomography, magnetic resonance imaging, and localized 1H magnetic resonance spectroscopy in Canavan's disease: a case report.

The neuroradiological evaluation of Canavan's disease in a 38-month-old girl is discussed. Computed tomography showed diffuse symmetrical low attenuation values of the subcortical and deep cerebral white matter. Magnetic resonance imaging demonstrated symmetrical diffuse low signal intensity on T1-weighted images and high signal intensity on T2-weighted images. With the use of 1H magnetic resonance spectroscopy, we were able to show elevated levels of N-acetylaspartic acid in the occipital lobe of our patient. The in vivo measurement of N-acetylaspartic acid in the brain by 1H magnetic resonance spectroscopy offers an additional noninvasive diagnostic test for establishing the diagnosis of Canavan's disease. With the increasing availability of magnetic resonance spectroscopy, clinicians may be able to confirm the diagnosis of Canavan's disease immediately after magnetic resonance imaging reveals the typical abnormalities of the white matter.

Amidohydrolases↗
PubMedDate not supplied

TO5 as a magnetization transfer contrast test object: characterization of the gels and determination of the real magnetization transfer.

Following the work of the European concerted action, "Tissue characterization by magnetic resonance spectroscopy and imaging," sets of five test objects (TO) were designed, produced, and distributed among European laboratories. The TO were designed to control the image quality of clincial magnetic resonance imaging in an independent and uniform mode. The fifth test object (TO5) was devoted to relaxation measurements and composed of 18 agarose tubes, inserted in an holder filled with a CuSO4 solution. These gels are subject to magnetization transfer (MT). The purpose of this paper is to characterize their MT parameters. An individual study of each gel was performed in a spectrometer, and an individual fit, as well as a global fit, was done on the two-pool model. The MT parameters found in each case are in agreement with the known properties of the agarose gels and given below. The real MT (transfer of magnetization from water to macromolecules) was computed, taking into account the "bleeding over" (direct saturation of the water magnetization). The maximum real MT ranges from 15 to 35% and can be obtained with almost the same saturation pulse conditions for all the gels. However, the saturating field required to reach the maximum MT is very high (46 microT) and unserviceable on a clinical device.

Biometry↗
PubMed2003

Relationship between magnetic field strength and magnetic-resonance-related acoustic noise levels.

The need for better signal-to-noise ratios and resolution has pushed magnetic resonance imaging (MRI) towards high-field MR-scanners for which only little data on MR-related acoustic noise production have been published. The purpose of this study was to validate the theoretical relationship of sound pressure level (SPL) and static magnetic field strength. This is relevant for allowing adequate comparisons of acoustic data of MR systems at various magnetic field strengths. Acoustic data were acquired during various pulse sequences at field strengths of 0.5, 1.0, 1.5 and 2.0 Tesla using the same MRI unit by means of a Helicon rampable magnet. Continuous-equivalent, i.e. time-averaged, linear SPLs and 1/3-octave band frequencies were recorded. Ramping from 0.5 to 1.0 Tesla and from 1.0 to 2.0 Tesla resulted in an SPL increase of 5.7 and 5.2 dB(L), respectively, when averaged over the various pulse sequences. Most of the acoustic energy was in the 1-kHz frequency band, irrespective of magnetic field strength. The relation between field strength and SPL was slightly non-linear, i.e. a slightly less increase at higher field strengths, presumably caused by the elastic properties of the gradient coil encasings.

Acoustics↗
PubMed1989

Magnetic resonance image degradation from prosthetic magnet keepers.

Eight types of prosthetic magnet keepers were imaged in a water phantom and a living human subject by a 1.5 T magnetic resonance device. Image artifacts were present for all eight samples and ranged from 160 mm to greater than 280 mm in diameter. These artifacts obliterate vital craniocervical areas making their examination by magnetic resonance impossible. Patients with magnetic keepers requiring comprehensive magnetic resonance imaging of the head and neck region must have them removed.

Denture Design↗
PubMed1992

Removable magnetic dental attachment that permits magnetic resonance imaging.

Magnetic dental attachments cause magnetic resonance image (MRI) degradation. A new magnetic dental attachment that allows removal of magnetic parts to exchange them for nonmagnetic parts was developed and tested. It allows high quality MRI with no change in occlusal vertical dimension. A volunteer test subject with combinations of attachments in place was examined by MRI. The images produced showed no degradation or distortion. Magnetic attachments for overdentures or maxillofacial prostheses should be removable to permit use of MRI.

Cobalt↗
PubMedDate not supplied

A novel magnetic adsorbent for immunoglobulin-g purification in a magnetically stabilized fluidized bed.

A novel magnetic poly(ethylene glycol dimethacrylate-N-methacryloly-L-histidinemethylester) [m-poly(EGDMA-(MAH)] support was prepared for purification of immunoglobulin G (IgG) in a magnetically stabilized fluidized bed by suspension polymerization. Elemental analysis of the magnetic beads for nitrogen was estimated as 70 micromol MAH/g polymer. Magnetic poly(EGDMA-MAH) beads were used in the separation of immunoglobulin-G (IgG) from aqueous solutions and/or human plasma in a magnetically stabilized fluidized bed system. IgG adsorption capacity of the beads decreased with an increase in the flow rate. The maximum IgG adsorption was observed at pH 6.0 for MES buffer. IgG adsorption onto the m-poly(EGDMA) was negligible. Higher adsorption values (up to 262 mg/g) were obtained in which the m-poly(EGDMA-MAH) sorbents were used from aqueous solutions. Higher amounts of IgG were adsorbed from human plasma (up to 320 mg/g) with a purity of 87%. IgG molecules could be repeatedly adsorbed and desorbed with these sorbents without noticeable loss in their IgG adsorption capacity.

Adsorption↗
PubMed2001

Conformational isomerism and weak molecular and magnetic interactions in ternary copper(II) complexes of [Cu(AA)L']ClO4.nH2O, where AA = L-phenylalanine and L-histidine, L' = 1,10-phenanthroline and 2,2-bipyridine, and n = 1 or 1.5: synthesis, single-crystal X-ray structures, and magnetic resonance investigations.

Weak molecular and magnetic exchange interactions in ternary copper(II) complexes, viz., [Cu(L-phe)(phen)(H(2)O)]ClO(4) (1), [Cu(L-phe)(bpy)(H(2)O)]ClO(4) (2), and [Cu(L-his)(bpy)]ClO(4).1.5H(2)O (3), where L-phe = L-phenylalanine, L-his = L-histidine, phen = 1,10-phenanthroline, and bpy = 2,2'-bipyridine, have been investigated. Single-crystal X-ray structures reveal that complex 2 crystallizes in a monoclinic space group P2(1), with unit cell parameters a = 7.422(7) A, b = 11.397(5) A, c = 12.610(2) A, beta = 102.10(5) degrees, V = 1043.0(11) A(3), Z = 2, R = 0.0574, and R(w) = 0.1657. Complex 3 crystallizes in a monoclinic space group C2, with a = 18.834(6) A, b = 10.563(4) A, c = 11.039(3) A, beta = 115.23(2) degrees, V = 1986.6(11) A(3), Z = 4, R = 0.0466, and R(w) = 0.1211. Molecules of 2, in the solid state, are self-assembled via weak intra- and intermolecular pi-pi stacking and H-bonding interactions. Molecules of 3 exhibit intermolecular dimeric association with the Cu.Cu separation being 3.811 A. X-ray structures and (1)H NMR studies reveal conformational isomerism in both solid and liquid states of complexes 1 and 2. The aromatic side chain of L-phe in 1 and 2 adopts either a "folded" (A) or an "extended" (B) conformation. Variable-temperature (1)H NMR and spin lattice relaxation measurements point out interconversion between conformations A and B at temperatures above 323 K. The change in molecular conformation induces a change in the electron density at the site of copper and band gap energy between HOMO and LUMO orbitals. Interestingly, in spite of paramagnetic nature, complexes 1 and 2 are amenable for both EPR and (1)H NMR spectroscopic studies. Single-crystal EPR spectra of 2 in three orthogonal planes are consistent with three-dimensional magnetic behavior. Intramolecular exchange dominates the dipolar interactions. The EPR spectra of 3 correspond to weak magnetic interactions between associated dimeric units. The structural and magnetic resonance investigations together reveal that the weak pi-pi stacking interactions are the electronic pathways for magnetic interactions in 1-3.

2,2'-Dipyridyl↗
PubMed2005

Nanoscale size effect of magnetic nanocrystals and their utilization for cancer diagnosis via magnetic resonance imaging.

Since the use of magnetic nanocrystals as probes for biomedical system is attractive, it is important to develop optimal synthetic protocols for high-quality magnetic nanocrystals and to have the systematic understanding of their nanoscale properties. Here we present the development of a synthetically controlled magnetic nanocrystal model system that correlates the nanoscale tunabilities in terms of size, magnetism, and induced nuclear spin relaxation processes. This system further led to the development of high-performance nanocrystal-antibody probe systems for the diagnosis of breast cancer cells via magnetic resonance imaging.

Animals↗
PubMed1997

Magnetic resonance and functional magnetic resonance imaging: tools for the study of human epilepsy.

The development of new magnetic resonance imaging base neuroimaging techniques is increasing the utility and the importance of magnetic resonance imaging in the investigation of patients with epilepsy. Recent advances in magnetic resonance imaging, magnetic resonance spectroscopy and functional magnetic resonance imaging are not only providing relevant clinical information regarding human epilepsy but are also revealing important insights into its basic mechanisms. In the present review the role of these new technologies is discussed in the context of their clinical utility.

Brain Mapping↗
PubMed1984

Magnetic resonance imaging: effects of magnetic field strength.

Magnetic resonance images of the head, abdomen, and pelvis of normal adult men were obtained using varying magnetic field strength, and measurements of T1 and T2 relaxations and of signal-to-noise (SN) ratios were determined. The T1 relaxation of gray matter, white matter, and muscle increases and T2 decreases with field strength, while T1 of fat remains relatively constant and T2 increases. As a consequence, for any one spin echo sequence, gray/white matter contrast decreases and muscle/fat contrast increases with field. SN levels rise rapidly up to 3.0 kgauss and then change more slowly, actually dropping for muscle. The optimum field for magnetic resonance imaging depends on tissue type, body part, and imaging sequence, so that it does not have a unique value. Magnetic resonance systems that operate in the 3.0-5.0 kgauss range achieve most or all of the gains that can be achieved by higher magnetic fields.

Abdomen↗
PubMed2003

Cognitive impairment: assessment with brain magnetic resonance imaging and proton magnetic resonance spectroscopy.

BACKGROUND: In vivo proton magnetic resonance spectroscopy is a safe and noninvasive tool that can be used to study aspects of brain chemistry and metabolism. This study was designed to evaluate its role in routine application to reveal the diagnostic reasons for cognitive impairment. METHOD: 37 Alzheimer's disease patients (NINCDS-ADRDA criteria), 31 patients with subcortical ischemic vascular dementia (Chui et al. criteria), and 13 subjects with subjective cognitive impairment (DSM-IV criteria) were included in this retrospective study. Magnetic resonance images were used for atrophy rating; additionally, proton magnetic resonance spectroscopy was performed. RESULTS: Significantly reduced N-acetylaspartate levels (p <.05) were found in both patients with Alzheimer's disease and patients with subcortical ischemic vascular dementia compared to the group with subjective memory complaints. The ratios of N-acetylaspartate/creatine and N-acetylaspartate/myo-inositol were significantly lower in Alzheimer's disease patients compared to patients with vascular dementia (p =.012) or patients with subjective memory impairment (p =.002). N-acetylaspartate/creatine and N-acetylaspartate/myo-inositol ratios were positively correlated to the degree of cerebral atrophy. Disoriented patients displayed a low N-acetylaspartate/creatine ratio. In contrast, we were not able to relate concurrent psychotic or behavioral symptoms to any spectroscopic parameter. CONCLUSION: This study indicates that proton magnetic resonance spectroscopy parameters could provide additional information in differentiating between Alzheimer's disease, subcortical ischemic vascular dementia, and subjective cognitive impairment. Therefore, this method can contribute to the routine diagnosis of dementia. Psychiatric and behavioral symptoms associated with dementia or due to a major psychiatric disorder cannot be related to changes in the measured proton magnetic resonance spectroscopy parameters.

Aged↗
PubMed1987

[Risks from magnetic fields and radiowaves in equipment for magnetic resonance tomography].

The use of Nuclear Magnetic Resonance Imaging for diagnostic purposes requires a careful analysis of potential risks for workers, patients and public. Aim of this work is a review of the most important biological effects produced by static magnetic fields, radiofrequency fields and field gradients. It's common opinion in fact that the use of magnetic and radiofrequency fields instead of ionizing radiations fields is a safety warranty for patients and workers. Biological experiments in small animals and microorganisms show that also in this case some risks may be expected, due to the trend to employ as much high as possible magnetic fields (and therefore radiofrequency fields). The available data show that the normally used magnetic and radiofrequency fields are below the threshold for somatic effects but denote the necessity of a careful risks/benefit analysis for some patients groups (pacemakers and small surgical metallic implants carriers) and the need of extended and deep studies to specify a possible synergy of different physical agents and incidental oncogenic and teratogenic consequence on the patient.

Animals↗