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At least 199 records · Page 11Linked to original sources
PubMed2000

Discrimination between Atlantic and Pacific Subspecies of Northern Bluefin Tuna (Thunnus thynnus) by Magnetic-Capture Hybridization Using Bacterial Magnetic Particles.

The previously developed magnetic-capture hybridization technique employing bacterial magnetic particles was applied to discriminate between Atlantic and Pacific subspecies of the northern bluefin tuna (Thunnus thynnus) using specific DNA sequences. Nucleotide sequences of a 925-bp fragment (ATCO) flanking the mitochondrial ATPase and cytochrome oxidase subunit III genes in these two subspecies were compared. Two regions having single-nucleotide and three-nucleotide differences between the subspecies were adopted to design DNA probes (NR1, 21-mer; NR2, 29-mer), and two internal primer sets were designed to amplify DNA fragments containing these regions. The DNA probes were immobilized on bacterial magnetic particles via streptavidin-biotin conjugation and subjected to magnetic-capture hybridization with the digoxigenin-labeled fragments amplified using the internal primers. The luminescence intensities of DNA on bacterial magnetic particles obtained by hybridization between the probes and the complementary fragments were higher than those obtained by hybridization with noncomplementary fragments. These data suggest that this system employing DNA on bacterial magnetic particles may be useful for discrimination of these two subspecies by recognizing a single-nucleotide difference.

Journal Article↗
PubMed2004

Magnetic field detection for current evaluation by magnetic force microscopy.

A current measurement method through magnetic field detection by magnetic force microscopy was proposed and demonstrated. We observed the magnetic field induced by an AC below 2.2 microA around a GaAs/AlGaAs mesa stripe. To achieve high sensitivity in magnetic field detection, we tuned the AC bias frequency to the torsional resonant frequency of the cantilever. As a result, the sensitivity of the magnetic field detection was much improved and specific features of the magnetic field around the mesa stripe were clearly observed at a current in sub-microA range.

Journal Article↗
PubMed2000

The effect of the rate of magnetic field and temperature changes on the ultrasonic wave absorption coefficient in a magnetic fluid

The rate of external magnetic field changes as well as temperature influences the structure of a magnetic fluid. This work presents experimental results on changes in the ultrasonic wave absorption coefficient of EMG-605 water-based magnetic fluid as a function of the external magnetic field intensity for different rates of magnetic field changes, at different temperatures. On the basis of these studies, radii of spherical clusters formed in the fluid under the influence of an external magnetic field have been determined.

Journal Article↗
PubMed2005

Capillary magnetic field flow fractionation and analysis of magnetic nanoparticles.

This paper reports the purification and analysis of magnetic nanoparticles using capillary magnetic field flow fractionation, which utilizes an applied magnetic field oriented orthogonal to the capillary flow. To validate this approach as a separation method for nanometer-scale particles, samples of magnetic nanoparticles composed of either gamma-Fe2O3 (maghemite) or CoFe2O4 with average diameters ranging from 4 to 13 nm were prepared and characterized by transmission electron microscopy and SQUID magnetometry. Retention of the samples on the capillary was investigated as a function of solvent flow rate and the nanoparticle size and composition; the elution times of the nanoparticles are strongly dependent on their magnetic moments. We demonstrate the use of this method to separate a mixture of nanoparticles into size-monodisperse fractions. The magnetic moments of the particles are calculated based on analysis of the retention parameters and correlate with values obtained in separate SQUID magnetometry measurements.

Journal Article↗
PubMed2006

Static magnetic-field-induced phase lag in the magnetization response of tris(dipicolinato)lanthanides.

Alternating-current (ac) magnetic susceptibility measurements for tris(dipicolinato) complexes with a trivalent heavy lanthanide ion, [N(C2H5)4]3[Ln(dipic)(3)] x nH2O (dipic = pyridine-2,6-dicarboxylate; Ln = Tb, Dy, Ho, Er, Tm, or Yb) are reported. While none of the six complexes showed a magnetization lag from the ac magnetic field of 10-10(3) Hz above 1.8 K, the Dy, Er, and Yb complexes with odd numbers of 4f electrons exhibited the magnetization lag in a static magnetic field. This phenomenon is explained to be caused by the elimination of a fast relaxation path, which is only effective for the Kramers doublet ground states in near zero field. At higher static fields, the remaining paths such as Orbach and/or direct processes govern the dynamics of the two-level systems comprised of spin-up and spin-down states. The non-Kramers complexes were found to have a nondegenerate ground state with large energy gaps from higher states, which is consistent with their fast magnetization relaxation.

Journal Article↗
PubMed2001

Strong supramolecular-based magnetic exchange in pi-stacked radicals. Structure and magnetism of a hydrogen-bonded verdazyl radical:hydroquinone molecular solid.

The X-ray crystal structure and magnetic properties of a molecular crystal consisting of 1,5-dimethyl-3-(2-pyridyl)-6-oxoverdazyl radical and hydroquinone (pyvd:hq) are presented. The structure contains a two-dimensional network of hydrogen bonds involving the hydroquinones and the pyridine ring of the pyvd radical. The radicals adopt an unusual head-over-tail (antiparallel) pi-stacked array perpendicular to the hydrogen-bonded planes. The variable-temperature magnetic susceptibility data can be modeled using a one-dimensional antiferromagnetic chain model, with J = -58 cm(-1). The strength of the magnetic coupling is very unusual because there are no close intermolecular radical-radical contacts to provide conventional pathways for magnetic interactions. A pathway for coupling is proposed involving the mediation of magnetic exchange interactions between radical centers by the pyridine rings. Density functional calculations on the pyvd radical, as well as aggregates thereof based on the X-ray structure, have been employed in attempts to understand the possible mechanisms by which the strong magnetic interactions are achieved.

Journal Article↗
PubMed2004

Single-molecule magnets: a large Mn30 molecular nanomagnet exhibiting quantum tunneling of magnetization.

The largest single-molecule magnet (SMM) to date has been prepared and studied. Recrystallization of known [Mn(12)O(12)(O(2)CCH(2)Bu(t))(16)(H(2)O)(4)] (1; 8Mn(III), 4Mn(IV)) from CH(2)Cl(2)/MeNO(2) causes its conversion to [Mn(30)O(24)(OH)(8)(O(2)CCH(2)Bu(t))(32)(H(2)O)(2)(MeNO(2))(4)] (2; 3Mn(II), 26Mn(III), Mn(IV)). The structure of 2 consists of a central, near-linear [Mn(4)O(6)] backbone, to either side of which are attached two [Mn(13)O(9)(OH)(4)] units. Peripheral ligation around the resulting [Mn(30)O(24)(OH)(8)] core is by 32 Bu(t)CH(2)CO(2)(-), 2 H(2)O, and 4 MeNO(2) groups. The molecule has crystallographically imposed C(2) symmetry. Variable-temperature and -field magnetization (M) data were collected in the 1.8-4.0 K and 0.1-0.4 T ranges and fit by matrix diagonalization assuming only the ground state is occupied at these temperatures. The fit parameters were S = 5, D = -0.51 cm(-1) = -0.73 K, and g = 2.00, where D is the axial zero-field splitting parameter. AC susceptibility measurements in the 1.8-7.0 K range in a zero DC field and a 3.5 G AC field oscillating at frequencies in the 50-997 Hz range revealed a frequency-dependent out-of-phase (chi(M)'') signal below 3 K, indicating 2 to be a single-molecule magnet (SMM), the largest yet obtained. Magnetization versus DC field sweeps show hysteresis loops but no clear steps characteristic of quantum tunneling of magnetization (QTM). However, magnetization decay data below 1 K were collected and used to construct an Arrhenius plot that revealed temperature-independent relaxation below 0.3 K. The fit of the thermally activated region above approximately 0.5 K gave U(eff)/k = 15 K, where U(eff) is the effective relaxation barrier. Resonant QTM was confirmed from the appearance of a "quantum hole" when the recent quantum hole digging method was employed. The combined results demonstrate that SMMs can be prepared that are significantly larger than any known to date and that this new, large Mn(30) complex still demonstrates quantum behavior.

Journal Article↗
PubMed2006

Magnetic resonance imaging of the manipulation of a chemical wave using an inhomogeneous magnetic field.

The effects of applied magnetic fields on the traveling wave formed by the reaction of (ethylenediaminetetraacetato)cobalt(II) (Co(II)EDTA2-) and hydrogen peroxide have been studied using magnetic resonance imaging (MRI) . It was found that the wave could be manipulated by applying pulsed magnetic field gradients to a sample contained in a vertical cylindrical tube in the 7.0 T magnetic field of the spectrometer. Transverse field gradients decelerated the propagation of the wave down the high-field side of the tube and accelerated it down the low-field side. This control of the wave propagation eventually promoted the formation of a finger on the low-field side of the tube and allowed the wave to be maneuvered within the sample tube. The origin of these effects is rationalized by considering the Maxwell stress arising from the combined homogeneous and inhomogeneous magnetic fields and the magnetic susceptibility gradient across the wave front.

Journal Article↗
PubMed2002

Lamellar magnetism in the haematite-ilmenite series as an explanation for strong remanent magnetization.

Magnetic anomalies associated with slowly cooled igneous and metamorphic rocks are commonly attributed to the presence of the mineral magnetite. Although the intermediate members of the ilmenite-haematite mineral series can also carry a strong ferrimagnetic remanence, it is preserved only in rapidly cooled volcanic rocks, where formation of intergrowths of weakly magnetic haematite and paramagnetic ilmenite is suppressed. But the occurrence of unusually large and stable magnetic remanence in rocks containing such intergrowths has been known for decades, and has recently been the subject of intense investigation. These unmixed oxide phases have been shown to contain pervasive exsolution lamellae with thickness from 100 microm down to about 1 nm (one unit cell). These rocks, many of which contain only a few per cent of such oxides, show natural remanent magnetizations up to 30 A m(-1) --too strong to be explained even by pure haematite in an unsaturated state. Here we propose a new ferrimagnetic substructure created by ferrous-ferric 'contact layers' that reduce charge imbalance along lamellar contacts between antiferromagnetic haematite and paramagnetic ilmenite. We estimate that such a lamellar magnetic material can have a saturation magnetization up to 55 kA m(-1) --22 times stronger than pure haematite-- while retaining the high coercivity and thermal properties of single-domain haematite.

Journal Article↗
PubMed2005

Complex magnetic fields enable static magnetic field cue use for rats in radial maze tasks.

Male Wistar rats were trained in an eight-arm radial maze task (two sessions per day, delayed-non-matching-to-sample) that included an intramaze static magnetic field "cue" (185 microT) specific to the entrance point of one of the arms. Rats were exposed daily for 60 min to a complex magnetic field waveform (theta-burst pattern, 200-500 nT), presented with several different interstimulus intervals (ISIs), either immediately following training sessions or immediately preceding testing sessions. Application of the theta-burst stimulus with a 4000 ms ISI significantly improved the rats' memory for the arm of the radial maze whose position was indicated by the presence of a static magnetic field cue. Reference memory errors were homogeneously distributed among all eight arms of the maze for sham-exposed rats, and among the other seven arms of the maze for complex magnetic field-treated rats. These results suggest that static magnetic field cues may be salient orienting cues even in a microenvironment such as a radial maze, but their use as a cue during maze learning in rats is dependent on whole-body application of a specific time-varying complex magnetic field.

Animals↗
PubMed1999

Magnetic flux generation and wave emissions during coalescence of magnetic islands in pair plasmas.

It is shown by using a two-dimensional fully relativistic electromagnetic particle-in-cell code that the tearing instability in a current sheet of pair plasmas is caused by Landau resonances of both electrons and positrons. Strong magnetic flux can be generated during coalescence of magnetic islands in the nonlinear phase of the tearing instability. The magnetic flux produced in an O-type magnetic island is caused by the counterstreaming instability found by Kazimura et al. [Astrophys. J. Lett. 498, L183 (1998); J. Phys. Soc. Jpn. 67, 1079 (1998)]. It is also shown that charge separation with a quadrupole-like structure is generated from the localized strong magnetic flux. During the decay of the quadrupole-like charge structure as well as the magnetic flux, there appear wave emissions with high-frequency electromagnetic waves and Alfvén waves as well as Langmuir waves.

Journal Article↗
PubMed2001

Magnetic-field-induced anisotropic curvature elasticity of a vesicle membrane containing magnetic polyions.

Interaction between a charged membrane and the electrolyte solution containing magnetic polyions is considered. A self-magnetic field, which arises due to the nonhomogeneous magnetic particle distribution near a charged membrane increases the effective charge screening length for the parts of a membrane normal to a magnetic field. The anisotropy of elastic properties of a membrane depending on the screening length is calculated on the basis of the curvature expansion. It is shown that due to diminishing of the spontaneous curvature for the parts of a membrane normal to a magnetic field there are two competing mechanisms of the ferrovesicle shape transformation under the influence of a magnetic field-the formation of a prolate shape orientated along a field due to the diminishing action of the demagnetizing field energy and the deformation to a oblate shape due to the decrease in the spontaneous curvature of the parts of a membrane normal to a field.

Journal Article↗
PubMed2003

Crystal structures of two-dimensional magnetic colloids in tilted external magnetic fields.

The stability of different crystal lattices of two-dimensional superparamagnetic suspensions that are confined to a planar liquid-gas interface and exposed to a tilted external magnetic field is studied theoretically by lattice sum minimizations. The magnetic field induces magnetic dipoles onto the colloidal particles along its direction, whose strength can be controlled by the amplitude of the external field. The mutual interaction between the colloids is governed by dipole-dipole forces and a short-ranged repulsion having its physical origin at the presence of the colloidal cores. If the direction of the magnetic field is perpendicular to the liquid-gas interface, there is a purely repulsive interaction leading to stable triangular crystals. By tilting the external field, the interaction becomes anisotropic and a mutual attraction appears upon a threshold tilt angle. We have calculated the full phase diagram at zero temperature varying the tilt angle, the colloidal density, and the strength of the magnetic field. Apart from the triangular lattice we find a variety of stable crystal lattices including rectangular, oblique, chainlike oblique, and rhombic structures. We also present the accurate derivation of the Hamiltonian of two polarizable particles of finite arbitrary geometries in external magnetic and electric fields.

Colloids↗
PubMed2006

Nonlinear dynamics of semiflexible magnetic filaments in an ac magnetic field.

Flexible spontaneously magnetized filaments exist in the living world (magnetotactic bacteria) and arise in magnetic colloids with large magnetodipolar interaction parameter. We demonstrate that these filaments possess variety of novel nonlinear phenomena in an ac magnetic field: orientation of the filament in the direction perpendicular to the field and the development of the oscillating U-like shapes, which presumably can lead to the formation of rings of magnetic filaments. It is found that these phenomena are determined by the development of the localized boundary modes of the filament deformation. We have illustrated by qualitative estimates that the phenomena found may be useful for insight into the complex pattern formation phenomena in ensembles of magnetic particles under the action of an ac magnetic field.

Journal Article↗
PubMed2000

Low-frequency magnetic noise in micron-scale magnetic tunnel junctions.

We have observed low-frequency noise due to quasiequilibrium thermal magnetization fluctuations in micron-scale magnetic tunnel junctions (MTJs). This strongly field-dependent magnetic noise occurs within the magnetic hysteresis loops, either as 1/f or Lorentzian (random telegraph) noise. We attribute it to the thermally excited hopping of magnetic domain walls between pinning sites. Our results show that magnetic stability is a crucial factor in reducing the low-frequency noise in small MTJs.

Journal Article↗
PubMed2004

Orbital magnetism: pros and cons for enhancing the cluster magnetism.

The discrepancy seen in the experimental and theoretical results on the magnetic moment of a small magnetic cluster has been attributed to the contribution arising from orbital magnetism. In this Letter we show that the magnetic states with large orbital magnetic moment are not always energetically favorable; they could, however, be realizable by coating the cluster or deposing it on appropriate substrates. More importantly, our work shows that the crucial factors that determine the cluster magnetism are found to be the intrinsic, and consequently, the extrinsic properties of the constituent atoms of the cluster.

Journal Article↗
PubMed2004

Magnetic percolation in diluted magnetic semiconductors.

We demonstrate that the magnetic properties of diluted magnetic semiconductors are dominated by short ranged interatomic exchange interactions that have a strong directional dependence. By combining first principles calculations of interatomic exchange interactions with a classical Heisenberg model and Monte Carlo simulations, we reproduce the observed critical temperatures of a broad range of diluted magnetic semiconductors. We also show that agreement between theory and experiment is obtained only when the magnetic atoms are randomly positioned. This suggests that the ordering of diluted magnetic semiconductors is heavily influenced by magnetic percolation, and that the measured critical temperatures should be very sensitive to details in the sample preparation, in agreement with observations.

Journal Article↗
PubMed2004

Temperature dependent magnetic anisotropy in metallic magnets from an ab initio electronic structure theory: L1(0)-ordered FePt.

Using a first-principles, relativistic electronic structure theory of finite temperature metallic magnetism, we investigate the variation of magnetic anisotropy K with magnetization M in metallic ferromagnets. We apply the theory to the high uniaxial K material, L1(0)-ordered FePt, and find its magnetic easy axis perpendicular to the Fe/Pt layers for all M and K to be proportional to M2 for a broad range of values of M. For small M, near the Curie temperature, the calculations pick out the easy axis for the onset of magnetic order. Our ab initio results for this important magnetic material agree well with recent experimental measurements, whereas the single-ion anisotropy model fails to give the correct qualitative behavior.

Journal Article↗