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PubMed · 15157535

A simple, inexpensive, and precise magic angle spinning speed controller.

Eric Hughes·Terry Gullion
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Abstract

Certain magic-angle spinning heteronuclear dipolar recoupling experiments using rotor-synchronized pulse trains require very precise control of the sample-spinning rate. An inexpensive spinning speed controller for use in magic-angle solid-state NMR experiments is described which can control the spinning rate to within +/- 0.2 Hz. The apparatus is based on a simple micro-controller and is self-contained. Experimental results are presented that show the importance of good spinning speed control.

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AlanineAlgorithmsEquipment DesignEquipment Failure AnalysisMagnetic Resonance SpectroscopyReproducibility of ResultsSensitivity and SpecificitySignal Processing, Computer-AssistedComparative StudyEvaluation StudyJournal ArticleResearch Support, U.S. Gov't, Non-P.H.S.Validation Study

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Eric Hughes, Terry Gullion. 2004. A simple, inexpensive, and precise magic angle spinning speed controller.. https://doi.org/10.1016/s0926-2040(03)00063-8

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