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T K Murray

Publications and source records attributed to T K Murray.

46 records · Page 3Linked to original sources

Variation in polyunsaturates of special margarines.

Label claims of special margarines offer little information about constituent fatty acids. Nine brands were analyzed with lipoxidase for the cis-methylene-interrupted polyunsaturated fatty acids which are present in unhydrogenated vegetable oils. Although four of these products were advertised as being made from corn oil or containing corn oil, they differed greatly in fatty acid composition. The claim of "polyunsaturates" did not identify those margarines highest in the cis-methylene-interrupted fatty acids. It is noted that regulations are being proposed to set a minimum level for these poly-unsaturated fatty acids in special margarines.

Chromatography, Gas↗

The differentiation and assay of vitamins D2 and D3 by gas-liquid chromatography.

1. A method is described for the differentiation and determination of as little as 0.2mug. of vitamins D(2) and D(3) by gas-liquid chromatography. 2. The vitamins are converted by treatment with antimony trichloride into isovitamins D(2) and D(3), which show single, separate peaks on gas-liquid chromatography, unlike the unmodified vitamins, which give twin peaks due to the formation of pyro and isopyro derivatives. 3. Since isovitamins D(2) and D(3) remain together in all steps of the procedure except during gas-liquid chromatography, one may be used as an internal standard for the other. 4. The use of an internal standard reduces the importance of loss during sample preparation and increases precision. 5. The application of the method to biological materials is demonstrated.

Animals↗

Goitre in Canada.

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Adolescent↗