Short-term bond strengths between adhesive cements and dental alloys.
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Biomedical subjects
Publications and source records attributed to J B Moser.
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Corrosion products of amalgam produced in Ringer's solution were compared with products formed in vivo using scanning electron microscopy, X-ray microanalysis, and potentiostatic anodic polarization. The corrosion products in an old amalgam were probably a mixture of tin-oxide and tin oxychloride. In vitro corrosion of fresh amalgam resulted in the buildup of similar products.
An indirect extrusion capillary viscometer has been developed. This has been tested for nonsetting Newtonian fluids and was found to give results close to, but slightly lower than the actual viscosity. The same apparatus has been successfully applied to a non-Newtonian fluid to determine the dependence of viscosity on shear rate. The technique described should meet the requirements for assessing the rheological characteristics important in the mixing and setting of dental materials. The developed viscometer must be coupled with a sensitive mechanical testing machine capable of an adequate range of crosshead speeds that can be changed rapidly. By obtaining force vs time curves at different shear rates for setting materials, viscosity can be calculated as a function of time. Also, the viscosity at any given time during the setting process can be calculated as a function of shear rate. This chould be of aid in the interpretation of changes in rheological properties during setting of dental materials.
The tensile bonding characteristics of five orthodontic cements to etched human enamel with and without a silane primer after storage for 1, 7, and 30 days in artificial saliva at 37 C were compared. The scatter of the data was probably due to the wide variation of surface morphology of etched human enamel. Cement L, a composite resin cement, was significantly stronger than the other cements tested. Cement D, a polycarboxylate cement, was significantly the weakest cement tested. Cements U, O, and N-B were of relatively equal bond strengths. Of the direct-bonding systems commercially available, the N-B system had the fastest setting time. The silane primer used in the research decreased the bond strength of cement O; however, it significantly increased the bond strength of cement L. Storage in artificial saliva at 37 C for 30 days decreased the mean bond strengths of most of the orthodontic cements with and without a silane primer. The exceptions were cement N-B without a silane primer and cements O and D with silane primer.
Color changes resulting from immersion of four composite resins in hot distilled water, coffee and tea were measured by a tristimulus colorimeter. Changes are shown as CIE deltaE values and converted to Munsell deltaH, deltaV and deltaC values.
Solubility and water absorption of eight orthodontic cements were determined as a function of time. Two brands of BIS-GMA and three brands of acrylic cements ranked about equally in solubility and water absorption. Three brands of polycarboxylate cements were appreciably poorer in these properties.