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Biomedical subjects

G Vanherle

Publications and source records attributed to G Vanherle.

At least 73 records · Page 4Linked to original sources

Hardness and Young's modulus determined by nanoindentation technique of filler particles of dental restorative materials compared with human enamel.

The recently developed nanoindentation technique was used to measure hardness and Young's modulus of small filler particles in resin composites and other dental restoratives. This technique eliminates the need to visualize indentations. Load and displacement are continuously monitored during a loading-unloading sequence, and hardness as well as Young's modulus are then calculated from the load-displacement curves taking into account the geometry of the indenter. Thirteen posterior composites, 3 dental ceramics for CAD/CAM restorations, 1 sintered porcelain, and 1 amalgam were investigated in this study. The results were compared to the hardness and Young's modulus determined by nanoindentation of human enamel. Of the dental materials tested, only five materials contain inorganic filler particles with a nanohardness not statistically different from that of enamel. The predominant fillers in all other materials, except amalgam and the prepolymerized resin fillers in Bell Firm PX, were found to be significantly harder. The dental restorative materials, except the alloy phase in amalgam, were composed of particles with a Young's modulus significantly lower than that of human enamel. The alloy phase in amalgam had a Young's modulus value comparable to that of enamel.

Dental Amalgam↗

Evaluation of two dentin adhesives in cervical lesions.

The clinical effectiveness of two dentin adhesives, Clearfil New Bond and Scotchbond 2, was evaluated in two different cavity designs. Group A was without enamel bevel or acid etch and with a butt-joint cavity; and group B had enamel bevel, acid etch, and feather-edged cavities. The retentive rate and marginal adaptation were monitored for 2 years. In the Clearfil system, 21% of group A restorations failed after 2 years, whereas virtually all the group B restorations (99%) were retained. In addition, after 2 years, the total of debonded group A restorations in the Scotchbond 2 system expanded to 13%, whereas no restorations from group B were lost. There was clearly marginal deterioration in time irrespective of the bonding system. Nevertheless, the marginal adaptation of cervical lesions restored with Clearfil New Bond adhesive in combination with Clearfil Ray composite resin revealed fewer defects compared with the Scotchbond 2 adhesive with Silux Plus composite resin restorations. SEM evaluation disclosed composite resin remnants on the dentin surface in cavities with lost fillings, which indicates partial cohesive failure of the adhesive joint.

Composite Resins↗

Two-year clinical evaluation of two dentine-adhesive systems in cervical lesions.

Two commercially available dentine-adhesive systems, Tenure and Tripton, were tested in two different cavity designs by placing 132 Class V composite restorations in cervical lesions of 35 patients. In Group A, the cervical restorations were placed totally in dentine without any intentional enamel involvement. In Group B, they were placed in dentine with adjacent enamel margins bevelled and acid etched. The retention rate, the evidence of clinical microleakage, and the marginal integrity were monitored over a 2-year period. The results of this clinical investigation indicate a high failure rate when only dentinal bonding was involved. A loss rate of 30% for Tenure and 55% for Tripton was noted in Group A after 2 years of clinical service. However, both adhesive systems used in combination with micromechanical retention on the enamel border (Group B) performed extremely well with only one restoration each having debonded over the 2-year period. Identically, marginal integrity and evidence of clinical microleakage more severely deteriorated with time for the Group A restorations in comparison with their Group B counterparts. In summary, the overall results were more positive for Tenure than for Tripton. It is concluded that micromechanical retention by acid etching of the enamel margin is still indispensable for the clinical success of cervical Class V composite restorations, primarily for retention and clinical microleakage and also, but to a lesser degree, for marginal adaptation.

Acid Etching, Dental↗

Three-year follow-up of five posterior composites: in vivo wear.

The wear of five posterior composites at occlusal contact areas (OCA) and contact free occlusal areas (CFOA) was evaluated in Class II cavities over a 3-year period with an accurate 3D-measuring technique. A clinical evaluation was also performed. The ultrafine compact-filled composites (Willems et al., 1992) showed acceptable OCA-wear rates ranging from 110 to 149 microns after 3 years. This is very similar to the OCA-wear rate of human enamel on molars, which is about 122 microns after 3 years. The fine compact-filled composite had an unacceptable OCA-wear value of 242 microns after 3 years. The ultrafine midway-filled composite showed an exceptionally high CFOA-wear value of 151 microns after 3 years, which gave the impression of it being gradually washed out of the cavity. Clinically, 70% of the restorations made with the ultrafine midway-filled composite showed excellent colour match after 3 years. For most of the compact-filled composites slightly opaque fillings were noted and 63% of the restorations made with one of these materials were clearly opaque. It can be concluded that the investigated ultrafine compact-filled composites can be considered as amalgam alternatives as far as their wear resistance is concerned.

Adult↗

Three-year follow-up of five posterior composites: SEM study of differential wear.

Assessing the wear of both enamel and composite at a shared occlusal contact area offers the opportunity to determine the differential wear between enamel and composite on the same tooth. Differential wear measurements were carried out on five posterior composite materials with an accurate 3D-measuring technique. The distinct wear step between enamel and composite was visualized by means of scanning electron photomicrographs. Both investigated ultrafine midway-filled and fine compact-filled composites (Willems et al., 1992a) have a considerably higher differential wear value and are, therefore, less suitable for rehabilitation of posterior teeth than are the ultrafine compact-filled composites, which have, in this study, a very satisfactory differential wear rate and appear to be highly wear resistant materials suitable for use in stress-bearing areas.

Adult↗

Dual-cure luting composites: Part I: Filler particle distribution.

Fourteen dual-cure luting composites were analyzed for their filler particle shape, predominant and maximum filler size, and filler weight in function of their clinical use. Polished surfaces were etched with an argon ion beam and studied by means of scanning electron microscopy. The type of filler particles, either inorganic or prepolymerized, could clearly be recognized. Their shapes were angular, rounded or spherical, depending on the product. The maximum filler size varied extremely from less than 1 micron to 250 microns. A particle-size distribution analyser disclosed a bell-shaped filler-size distribution. The predominant filler size for all the products was much smaller than the maximum filler size. The filler weight varied from 36 to 77%. After ion etching, some products showed small areas with a low degree of filler loading. A classification of the luting composites based on the maximum filler size is proposed. Since the particle size varies widely within the group of products analyzed, a standard specification for luting composites is urgently needed.

Adhesives↗

Chemical characterization of the resin-dentin interface by micro-Raman spectroscopy.

The chemical nature of the interface between dentin and adhesive resin materials was characterized by micro-Raman spectroscopy. The resulting chemical profiles were correlated with photomicrographs obtained by SEM after an argon-ion-beam etching treatment of the sample surface. Two commercially available dentin adhesive systems, of which one was also applied with a different conditioning agent, were investigated. Raman spectra, which were recorded along line scans across the interface with a step increment of 1 micron, revealed that resin effectively penetrated 4 to 6 microns deep into the superficially decalcified dentin zone. Across the interface, a gradual transition from resin to dentin over the interdiffusion zone with a mixed contribution of both substances was noticed. Finally, resin appeared to penetrate to the entire decalcification depth of dentin regardless of the aggressiveness of the conditioning procedure.

Boron Compounds↗

Assessment by nano-indentation of the hardness and elasticity of the resin-dentin bonding area.

The hardness and Young's modulus of the successive layers across a resin-dentin bonding area were determined by nano-indentation for four commercially-available dentin adhesive systems, of which two were also applied with a different conditioning agent. With a computer-controlled nano-indentation technique, minute triangular indentations were made within a small area of a few micrometers' diameter at a load of a few milli-Newtons. The load and displacement of the indenter were continuously monitored during the loading-unloading sequence, so hardness and Young's modulus could be computed as a function of the indenter geometry and the applied load. The hardness of the resin-dentin interdiffusion zone was significantly lower than that of unaltered dentin. A gradient of moduli of elasticity was observed from the rather stiff dentin over a more elastic resin-dentin interdiffusion zone and adhesive resin layer to the restorative composite. That gradient was more substantial in those systems that produced relatively thick adhesive resin layers or supplementally provided a filled low-viscosity resin as an intermediate layer between the adhesive resin and the bulk restorative composite. Such an elastic bonding area might have a strain capacity sufficient to relieve stresses between the shrinking composite restoration and the rigid dentin substrate, thereby improving the conservation of the dentin bond and, as a consequence, the marginal integrity and retention of the restoration.

Composite Resins↗

[Amalgam. IV. Metabolism of mercury].

After absorption in the body by four ways, each type of mercury undergoes a specific metabolism. Elementary mercury as mercury vapour becomes rapidly oxidized to Hg2+ and, afterwards, is metabolized as an inorganic mercurial compound. From the blood circulation mercury reaches target organs like the kidneys, the central nervous system, the liver and the hypophysis, in which mercury accumulates. The retention time varies by organ and is longest in the brain. Mercury is mainly eliminated with urine and faeces, to a lesser degree with transpiration and mother's milk and sometimes by respiration.

Absorption↗

[Adhesion of composite to dentin. Mechanical and clinical results].

Although an efficient bond of resin composites to enamel can be realized since quite a long time, reliable dentine bonding is nowadays still a clinical problem. After the failure of the dentine-etch technique, followed by the misfortunes of the chemical dentine adhesion technique, modern dentine adhesive systems are believed to function by a micromechanical attachment mechanism. Based on a morphological study of the resin-dentine interface, a broad selection of dentine adhesive systems was classified following their adhesion-strategy. In a second part, eight dentine adhesive systems were clinically tested in terms of retention.

Acrylic Resins↗

Composite resins in the 21st century.

Human enamel and dentin should be used as the physiologic standards with which to compare composite resins, especially in the posterior region. The intrinsic surface roughness of composite resins must be equal to or lower than the surface roughness of human enamel on enamel-to-enamel occlusal contact areas (Ra = 0.64 microns). Roughness determines the biologic strength of composite resins. The nanoindentation hardness value of the filler particles (2.91 to 8.84 GPa) must not be higher than that of the hydroxyapatite crystals of human enamel (3.39 GPa). Composite resins intended for posterior use should have a Young's modulus at least equal to, and preferably higher than, that of dentin (18.500 MPa). The compressive strength of enamel (384 MPa) and dentin (297 MPa) and the fracture strength of a natural tooth (molar = 305 MPa; premolar = 248 MPa) offer excellent mechanical standards to select the optimal strength for posterior composite resins. The in vivo occlusal contact area wear rate of composite resins must be comparable to the attritional enamel wear rate (about 39 microns/y) in molars. Differential wear between enamel and composite resin on the same tooth is a new criterion for visualizing and quantifying the wear resistance of composite resins in a biologic way. Posterior resins must have a radiographic opacity that is slightly in excess of that of human enamel (198% Al). Based on these standard criteria, it can be concluded that in the 21st century the ultrafine compact-filled composite resins may be the materials of choice for restoring posterior cavities.

Analysis of Variance↗

Stress-induced cervical lesions.

The increasing occurrence of dental lesions at the cervical surfaces requires more knowledge of the causes of the process. Acidic and abrasive mechanisms have clearly been documented as causes but the stress theory by Lee and Eakle is still controversial. This report describes several incidences of possible stress-induced lesions according to the characteristics described by Lee and Eakle. The occurrences of subgingival lesions lend credence to the stress-induction theory by exclusion of other superimposing etiologic factors. With the current concepts, a perceptive approach to the treatment of cervical lesions can be executed.

Bite Force↗

In vitro vibrational wear under small displacements of dental materials opposed to annealed chromium-steel counterbodies.

In vitro vibrational wear tests were performed on 17 composites and one amalgam with human enamel as a reference. The specimens were fixed on a computer-controlled X-Y translation table that generated an oscillatory movement under small displacements. The dental material specimens were in permanent contact with an annealed chromium-steel counterbody. The tests were performed in ambient air of normal humidity at room temperature under non-lubricated sliding conditions. The friction between the counterbody and each of the various materials was measured on-line. After completion of the tests, the wear volumes were determined by contactless profilometry, and the wear pattern was studied with SEM. The simple vibrational test used in this study allowed a fast classification of different dental materials in terms of the relative wear on either the specimen or the counterbody material. The ratio of the wear volume of the counterbody versus the wear volume of the dental material specimen was used to accurately classify the materials according to their in vitro wear behavior, especially when this ratio was related to the total wear volume of the dental material specimen and the counterbody. From an analysis of the wear behavior of the both contacting materials, it became obvious that neither the wear of the dental materials nor of the chromium-steel counterbody appears to correlate with either the inorganic filler hardness, the intrinsic surface roughness, the surface hardness or the Young's modulus of the dental materials.

Chromium Alloys↗

A classification of dental composites according to their morphological and mechanical characteristics.

The on-going search for a biologically acceptable restorative material has brought a confusing variety of composites on the dental market. In the present study, commercially available composites are categorized as a function of their mean particle size, filler distribution, filler content, Young's modulus, surface roughness, compressive strength, surface hardness, and filler morphology. Out of this information, it can be concluded that the materials of choice for restoring posterior cavities at present are the Ultrafine Compact-Filled Composites because their intrinsic surface roughness, Young's modulus and, indirectly, their filler content, compressive strength, and surface hardness are comparable to the same properties of enamel and dentin. The Ultrafine Midway-Filled Composites seem to be very satisfactory materials for anterior use.

Composite Resins↗

Marginal adaptation of four tooth-coloured inlay systems in vivo.

This study investigates the margin quality of four different tooth-coloured inlay systems using computer-aided quantitative margin analysis under scanning electron microscopy. Three types of restorations involved chairside procedures using a commercial CAD-CAM apparatus: one type of inlay restoration was milled from preformed glass ceramic blocks, the other two inlay types were milled from preformed porcelain blocks. The fourth system was based on an experimental indirect composite inlay system. Each inlay type was luted with its respective dual-curing luting composite, which was supplied with the system. After 6 months of clinical service, all four systems revealed a significant percentage of submargination indicating occlusal wear of the luting composite. The porcelain inlays and the composite inlays luted with their respective experimental luting composite showed the best marginal adaptation. Luted glass ceramic inlays, in particular, suffered from a significantly higher percentage of inlay margin fractures (9 per cent) and marginal openings (4 per cent) than the other systems. A possible explanation is that the glass ceramic subsurface structure at the inlay-lute interface was weakened by etching with ammonium bifluoride.

Acid Etching, Dental↗

Marginal accuracy of CAD/CAM inlays made with the original and the updated software.

The software driving the Cerec CAD/CAM system has recently been updated. In this study, the marginal accuracy of computer-machined porcelain inlays was determined using the original and the updated software. Two types of MOD cavities in Frasaco resin teeth were prepared with either sharp or rounded box corners. The distance of the occlusal and proximal marginal interface was determined using a measuring microscope. The mean occlusal interfacial distance was 52 microns for both programs. Only the box corners showed a significantly larger space, of which the mean value was approximately 200 microns. The updated version improved the marginal accuracy at the box corners. Further reduction of the interfacial distance was accomplished by rounding the sharp box corners.

Bicuspid↗