Residue levels of ethyl carbamate in wines and spirits by gas chromatography and mass spectrometry/mass spectrometry.
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Biomedical subjects
Publications and source records attributed to G M Doose.
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The multiresidue procedure of Luke et al., which uses extraction with acetone and partition with petroleum ether and methylene chloride, was simplified and shortened by eliminating the Florisil cleanup. Double concentration with petroleum ether in the Kuderna-Danish evaporator following the initial concentration removed the last traces of methylene chloride. The extract was then injected into a gas chromatograph, using a Hall electrolytic conductivity detector for organohalogen, organonitrogen, and organosulfur pesticides or a flame photometric detector for organophosphorus pesticides. Recoveries of 70 pesticides are presented.