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Biomedical subjects

E C Combe

Publications and source records attributed to E C Combe.

At least 37 records · Page 2Linked to original sources

Properties of gypsum with the addition of gum arabic and calcium hydroxide.

The purpose of this work was to study the effects of adding a mixture of gum arabic and calcium hydroxide to a type III stone and an improved die stone. The effect on the water/powder ratio, compressive and tensile strength, hardness, and setting expansion was determined. Data for mechanical properties were subjected to two-way analysis of variance, followed by the Bonferroni-Dunn procedure to determine any significance (1%) between pairs of means. For the type III material the additives had little effect on setting expansion, but the additives significantly improved surface hardness. The additives did not improve compressive or tensile strength for the type III materials. In contrast, the improved die stone's hardness was not enhanced by the additives, and in some instances a reduction in strength was observed. It was concluded that dental cast materials with superior surface properties can be produced by a simple change of formulation.

Analysis of Variance↗

Colour changes in acrylic teeth--comparison of an objective and subjective method.

Colour changes in four currently used brands of acrylic dental teeth were measured objectively and assessed subjectively following the application of heat, acrylic monomer and light. The data indicated that no clear correlation existed between the results of visual inspection and opto-electronic measurements. It is suggested that visual assessment is an unreliable method of detecting colour change, and an objective colorimetric method is therefore recommended.

Acrylic Resins↗

Development and assessment of an objective method of colour change measurement for acrylic denture base resins.

Current standard specifications for the laboratory evaluation of denture base materials require subjective assessment of colour stability. This study evaluates a new objective measurement technique for translucent denture base materials, by comparing quantitative data with the results obtained from a standard subjective method. Preliminary work on three representative commercial acrylic materials resulted in the selection of a white background for the quantification of colour change of these translucent materials. One half of each sample was exposed to artificial sunlight for 24 h. The colour of both exposed and unexposed resin was measured on the CIE L*a*b* scale using a photo-electric colorimeter. Significant changes in the b* and E* values (P < 0.01) were observed following light exposure. Objective data for a wide range of commercial materials were compared with the results of a subjective evaluation and it was shown that a change in b* of 1.5 units was discernable subjectively by eye for 100% of the cases. It is suggested that this method and limit value could form the basis of a new objective colour change specification for polymeric dental materials.

Acrylic Resins↗

Development of new adhesive pulp capping materials.

The pulp capping materials currently available do not adhere to dentine but cover it and therefore extensive removal of tooth tissue is necessary to expose sufficient dentine for the adhesives used to secure the restoration (the adhesives do not adhere to the capping material). The authors describe how two new pulp capping materials have been developed, which combine the properties required for pulp capping with an ability to adhere to dentine.

Acrylic Resins↗

Pulp response to a novel adhesive calcium hydroxide based cement.

This study compares pulp responses to 3 formulations of calcium hydroxide, namely: a) An experimental adhesive calcium hydroxide cement containing polyacrylic acid, b) Dycal (L.D> Caulk Co, Milford, Delaware) Batch Nos 176970/176990, c) "Analar" calcium hydroxide mixed with sterile distilled water. After 28 days dentine bridges were present in 77% of teeth capped with the test material, 64% of teeth treated with Dycal and in 62% of teeth capped with calcium hydroxide and water. Inflammatory infiltrates were observed in a number of teeth remote from the bridges. Bacteria were detected in these specimens. Exposed rat molar pulp responses to an experimental adhesive calcium hydroxide cement were similar to to those observed with 2 other calcium hydroxide formulations.

Animals↗

Early strength and adaptability of amalgam in relation to coherence time.

The minimum mixing time required to give a coherent mix of a dental amalgam ("coherence time") was determined for eleven representative materials using two different amalgamators. The effect of mixing these amalgams at various multiples of their coherence time on early compressive strength and adaptability was determined. It was found that the two amalgamators gave different coherence time values for the alloys, but that the strength data for any given alloy was similar for a given multiple of coherence time. Longer mixing tended to yield amalgams of greater early strength, but reduced the adaptability of the mixed material.

Analysis of Variance↗

The effect of glass heat treatment on the properties of a novel polyalkenoate cement.

The effect of heat treating the glass component of a novel glass-ionomer (polyalkenoate) cement on cement properties has been determined, with specific reference to the reactivity of the glass, and the mechanical properties of the resultant cement. It has been shown that heat treatment is a suitable method of decreasing the glass reactivity and improving the handling characteristics of the mixed cement. Under some conditions, an increase in compressive strength was found, although the effect on tensile properties was not significant.

Glass Ionomer Cements↗

The use of microwave energy to cure denture acrylic resins.

Experiments have been carried out on the curing of poly(methyl methacrylate) denture base material in a microwave oven, using conventional dental flasks and flask clamps. It has been shown that it is important (a) to maintain sufficient pressure on the materials, (b) to avoid gaseous porosity by not heating too rapidly initially, and (c) to ensure that all metal is protected from exposure to microwaves. When the appropriate conditions of polymerisation were used, microwave-cured samples had satisfactory physical and mechanical properties according to American Dental Association specification number 12.

Acrylic Resins↗

Measurement of the viscosity of irreversible hydrocolloids.

Three techniques have been used to assess the shear rate dependence of the viscosity of mixed alginate impression materials prior to setting. Two methods used a cone-plate viscometer, and one method was a capillary extrusion technique. Data from the three sets of experiments have been critically compared. It has been shown that an unset alginate material exhibits Bingham behaviour.

Alginates↗

Development of novel dental cements. I. Formulation of aluminoborate glasses.

Aluminoborate glasses were formulated as potential novel glass-ionomer cement components, and their reactivity with a polyalkenoic acid was assessed by means of working and setting time measurements. Of the 20 prepared formulations, some containing fluoride, eight were found to have acceptable manipulative characteristics, and three of these formed hard set materials.

Aluminum Silicates↗

Development of novel dental cements. II. Cement properties.

Following earlier work, three novel aluminoborate glasses have been studied as potential cement components. Factors studied include the effect of batch size on composition and manipulative characteristics, and the effect of tartaric acid and conditions of storage on mechanical properties. It was concluded that two materials have potential for application as dental luting agents.

Aluminum Silicates↗

Acoustic evaluation of earmoulds in situ: a comparison of impression and earmould materials.

Laboratory research has been carried out on the accuracy of both ear impression and earmould materials. The present work was undertaken to assess such materials in vivo. An objective clinical method of earmould evaluation was developed, based on estimation of the attenuation in the acoustic feedback path. The method was used to assess the acoustic performance of earmoulds made from three earmould materials of different texture, when prepared from two different impression materials. It was shown that the choice of impression material made a significant difference to earmould performance. For greatest accuracy, addition cured silicone impression materials are recommended.

Adolescent↗

Tin oxide coating of aluminous porcelain by reactive ion plating.

Alumina reinforced dental porcelain has been coated directly with tin oxide by reactive ion plating. Samples were prepared at different distances from the tin source in the ion plating rig. Tensile bond strengths of treated and untreated porcelain discs to a commercially available phosphate-methacrylate based dental cement were determined. Bond strengths of certain coated samples were found to be in excess of the cohesive strength of the porcelain substrates (greater than 7.8 MPa), whereas untreated porcelain achieved an average bond strength of only 3.4 MPa. The microstructures of coatings produced under conditions similar to those which yielded the maximum bond strength were examined in a scanning electron microscope and were found to be approximately 0.5 microns thick. It is believed that ion plating has great potential for rendering inert ceramic surfaces capable of direct bonding to dental cements.

Adhesives↗