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PubMed2004

Infrared antennas coupled to lithographic Fresnel zone plate lenses.

Several designs for Fresnel zone plate lenses (FZPLs) to be used in conjunction with antenna-coupled infrared detectors have been fabricated and tested. The designs comprise square and circular FZPLs with different numbers of Fresnel zones working in transmissive or reflective modes designed to focus infrared energy on a square-spiral antenna connected to a microbolometer. A 163x maximum increase in response was obtained from a 15-zone circular FZPL in the transmissive mode. Sensor measurements of normalized detectivity D* resulted in a 2.67x increase with FZPLs compared with measurements made of square-spiral antennas without FZPLs. The experimental results are discussed and compared with values obtained from theoretical calculations.

Journal Article↗

PubMed2002

An electrospray ionization source for integration with microfluidics.

We have demonstrated a new electrospray ionization (ESI) device incorporating a tip made from a shaped thin film, bonded to a microfluidic channel, and interfaced to a time-of-flight mass spectrometer (TOFMS). A triangular-shaped thin polymer tip was formed by lithography and etching. A microfluidic channel, 20 microm wide and 10 microm deep, was embossed in a cyclo olefin substrate using a silicon master. The triangular tip was aligned with the channel and bonded between the channel plate and a flat plate to create a microfluidic channel with a wicking tip protruding from the end. This structure aided the formation of a stable Taylor cone at the apex of the tip, forming an electrospray ionization source. This source was tested by spraying several solutions for mass spectrometric analysis. Because the components are all made by lithographic approaches with high geometrical fidelity, an integrated array system with multiple channels can be formed with the same method and ease as a single channel. We tested a multichannel system in a multiplexed manner and showed reliable operation with no significant cross contamination between closely spaced channels.

Cytochrome c Group↗